• Title/Summary/Keyword: 일차 표준

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Taxonomic Study of the Genus Candida by Cellular Fatty Acid Analysis (세포내 지방산 조성 분석에 따른 Candida속의 분류)

  • 신기선;홍순덕;배경숙
    • Korean Journal of Microbiology
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    • v.33 no.2
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    • pp.81-85
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    • 1997
  • Candida속 효모 27종이 표준 균주를 대상으로 세포내 지방산 조성을 기체 크로마토그래피로 분석하여, 함유 지방산의 종류와 함량비를 근거로 27종이 균주를 3개의 분류군으로 나누었다. 이들 지방산 분석에 의한 분류군을 Candida속의 다른 분류학적 결과들인 coenzyme Q 분자종의 종류, DNA 염기함량 분석, ITS 부위의 제한효소 절단 다형질의 양상, 리보좀 소단위 RNA 유전자의 염기배열 보고와 비교 분석하였다. 그 결과 같은 분류군에 위치하는 균주들 사이의 연관 관계가 거의 일치하였다. 다라서 세포내 지방산 분석은 Candida속 규준들을 유전적 동질성을 갖는 균주들로 분류하는 수단으로 사용될 수 있으며, 유전적으로 매우 다양한 균주들의 집단으로 알려진 Candida속에 관한 분류적 고찰에 일차적으로 사용될 수 있는 유용한 수단임을 알 수 있었다.

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A Study for XML DTD Matching Method using Inlining Algorithm (Inlining 알고리즘을 이용한 XML DTD 매칭 방법에 관한 연구)

  • Heo, Bo-Jin;Kim, Hyeong-Seok;Kim, Chang-Suk
    • Proceedings of the Korea Information Processing Society Conference
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    • 2003.11c
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    • pp.1505-1508
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    • 2003
  • XML DTD 매칭은 데이터 통합이나 데이터 웨어하우스, 웹 마이닝, 전자상거래, 의미적 질의 처리등과 같은 데이터베이스 관련 응용분야에서 수행해야 할 근본적인 연구 분야이다. 웹이 발전됨에 따라 웹 상의 데이터 교환의 표준인 XML로 많은 데이터를 표현하게 되었고, 이 XML DTD에 대한 매칭이 주된 연구 분야로 대두되었다. XML 스키마는 플랫 구조인 기존의 관계형 데이터베이스 스키마와는 달리 계층적인 트리 구조로 이루어져 DTD를 직접 비교하기가 어렵다. 본 논문에서는 계층적 구조인 XML DTD의 계층적 구조 정보와 무결성 제약조건을 추출하여 일차원적인 직렬 구조로 변환한 후, 유사한 DTD를 매칭하는 방법을 제안한다.

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A study on the metadata of the sports video record (스포츠 동영상 기록물 메타데이터에 관한 연구)

  • Park, In-Woo;Nam, Young-Joon
    • Proceedings of the Korean Society for Information Management Conference
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    • 2018.08a
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    • pp.127-132
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    • 2018
  • 본 연구는 스포츠 동영상 기록물의 체계적 보존과 관리, 이를 적극적으로 활용할 수 있는 스포츠 동영상 메타데이터 제안을 연구목적으로 설정하였다. 스포츠 동영상이 지닌 특성을 분석하고, 현재 스포츠 관련 기록물을 소장한 관리 주체에서 운영하고 있는 관리시스템을 분석하였다. 각 사례와 표준에서 추출한 메타데이터 요소를 상호 비교하여 공통 요소와 특성 요소를 일차적으로 추출하였다. 추출된 요소의 타당성에 대하여 전문가 의견을 수렴, 검증받은 후 7개의 상위요소와 12개의 하위요소를 지닌 관리적(administrative) 요소와 9개의 상위요소와 11개의 하위요소로 구성한 기술적(descriptive) 요소로 제안하였다.

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Intercomparison of the KAERI Reference Photon and Beta Radiation Measurements (한국원자력연구소 기준 광자 및 베타선장 측정의 국제상호비교)

  • Chang, Si-Yeong;Kim, Bong-Hwan;Kim, Jang-Lyul;McDonald, J.C.;Murphy, M.K.
    • Journal of Radiation Protection and Research
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    • v.21 no.4
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    • pp.255-262
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    • 1996
  • This paper describes the results of intercomparison measurements of KAERI reference photon and beta radiation fields between the KAERI and the PNNL(Pacific Northwest National Laboratory), recently performed at KAERI radiation calibration and dosimetry laboratory on the basis of the ANSI N13.11 criteria for personal dosimeter performance test. Each laboratory used her own radiation detectors or measurement devices traceable to her national primary standard in measuring the exposure rates for photon fields, the absorbed dose rates for beta radiation fields. The agreements in reference radiation measurements between two laboratories were found to be less than ${\pm}2.0%$ for photon fields, ${\pm}1.0%$ for beta radiation fields. Therefore, it could be concluded that KAERI reference radiation fields comply well with the international standard and thus can further serve as a national basis for the researches and developments in radiation protection dosimetry in Korea.

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Studies on the Standardization of pH Measurement System (pH 측정 시스템의 표준화에 관한 연구)

  • Lee, Hwa Shim;Kim, Myung Soo;Kim, Jin Bok;Oh, Sang Hyup
    • Journal of the Korean Chemical Society
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    • v.42 no.4
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    • pp.432-442
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    • 1998
  • Since the definition of pH, $pH=-Ioga_H$ is based on a single ion activity, pH values can not be determined with measurement itself, but require an approximation method. They are derived from EMF measurement of a liquid junction free cell using hydrogen and Ag/AgCl electrodes. Primary standard materials with certified pH values can be obtained with this approximation method. Standard buffer solutions are used to calibrate pH meters. Thus the accuracy of the pH values of standard buffer solutions limits the reliability of measured pH values can be obtained with this approximation method. Standard buffer solution are used to calibrate pH meters. Thus the accuracy of the pH values of standard buffer solutions limits the reliability of measured pH values of sample solutions. To certify the pH values, we have established the system for the primary standard measurement and certified the pH of buffer solutions in the range of 1.6∼12.5 pH unit within uncertainty of ${\pm}0.005$ pH unit.

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Quantification of cholesterol in human serum by isotope dilution liquid chromatography/mass spectrometry (동위원소희석 액체크로마토그래피/질량분석법에 의한 혈청 내 콜레스테롤의 정량)

  • Shin, Hyesun;Lee, Hwashim;Lee, Gaeho
    • Analytical Science and Technology
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    • v.21 no.6
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    • pp.502-509
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    • 2008
  • An ID LC/MS (isotope dilution liquid chromatography/mass spectrometry) was used as a primary method for the quantitative analysis of cholesterol in human serum. The separation of cholesterol was carried out by Thermo ODS hypersil $C^{18}$ column. The mobile phase was 100% methanol, and flow rate was $0.3m{\ell}/min$. Cholesterol and cholesterol-$3,4-13C_2$ were monitored at m/z 369.4 and 371.3, which correspond to $[M-H_2O+H]^+$ respectively. In order to verify the measurement method, NIST SRM 909b was analyzed. The results agreed well with certified values within uncertainty. The four kinds of serum certified reference material were prepared and certified. The repeatabilities of measurement were ranged from 0.1 to 0.8% (RSD), which were relatively good. The reproducibility between independent measurement run was below 0.24% (RSD). The expanded uncertainty was about 1.43% within the 95% confidence interval.

Development of Lead Free Shielding Material for Diagnostic Radiation Beams (의료영상용 방사선방호를 위한 무납차폐체 개발)

  • Choi, Tae-Jin;Oh, Young-Kee;Kim, Jin-Hee;Kim, Ok-Bae
    • Progress in Medical Physics
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    • v.21 no.2
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    • pp.232-237
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    • 2010
  • The shielding materials designed for replacement of lead equivalent materials for lighter apron than that of lead in diagnostic photon beams. The absorption characteristics of elements were applied to investigate the lead free material for design the shielding materials through the 50 kVp to 110 kVp x-ray energy in interval of 20 kVp respectively. The idea focused to the effect of K-edge absorption of variable elements excluding the lead material for weight reduction. The designed shielding materials composited of Tin 34.1%, Antimon 33.8% and Iodine 26.8% and Polyisoprene 5.3% gram weight account for 84 percent of weight of lead equivalent of 0.5 mm thickness. The size of lead-free shielder was $200{\times}200{\times}1.5\;mm^3$ and $3.2\;g/cm^3$ of density which is equivalent to 0.42 mm of Pb. The lead equivalent of 0.5 mm thickness generally used for shielding apron of diagnostic X rays which is transmitted 0.1% for 50 kVp, 0.9% for 70 kVp and 3.2% for 90 kVp and 4.8% for 110 kVp in experimental measurements. The experiment of transmittance for lead-free shielder has showed 0.3% for 50 kVp, 0.6% for 70 kVp, 2.0% for 90 kVp and 4.2% for 110 kVp within ${\pm}0.1%$. respectively. Using the attenuation coefficient of experiments for 0.5 mm Pb equivalent of lead-free materials showed 0.1%. 0.3%, 1.0% and 2.4%, respectively. Furthermore, the transmittance of lead-free shielder for scatter rays has showed the 2.4% in operation energy of 50 kVp and 5.9% in energy of 110 kVp against 2.4% and 5.1% for standard lead thickness within ${\pm}0.2%$ discrepancy, respectively. In this experiment shows the designed lead-free shielder is very effective for reduction the apron weight in diagnostic radiation fields.

Functional MRI ofThe Supplementary Motor Area in Hand Motor Task: Comparison Study with The Primary Motor Area (수지운동자극을 사용한 부운동중추의 기능적 MR연구: 일차운동중추와의 비교)

  • 이호규;김진서;최충곤;임태환
    • Investigative Magnetic Resonance Imaging
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    • v.1 no.1
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    • pp.103-107
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    • 1997
  • Purpose: To investigate the localization and functional lateralization of the supplementary motor area (SMA) in motor activation tests in comparison to that of the primary motor area. Materials and Methods: Seven healthy volunteers obtained echoplanar imaging blood oxygen level dependent technique. This study was carried on 1.5T Siemens Magnetom Vision system with the standard head coil. Parameters of EPI were followed as; TR/TE : 1.0/66.0msec, flip angle: $90^{\circ}$, field of view: $22cm{\times}22cm,{\;}matrix:{\;}128{\times}128$, slice number/slice thickness/gap: 1O/4mm/0.8mm with fat suppression technique. Motor task as finger opposition in each hand consisted of 3 sets of alternative rest and activation periods. Postprocessing were done on Stimulate 5.0 by using cross-correlation statistics. To compare the functional lateralization of the SMA in the right and left hand tests, each examination was evaluated for the percent change of signal intensity and the number of activated voxels both in the SMA and in the pri¬mary motor area. Hemispheric asymmetry was defined as difference of summation of the activted voxels between each hemisphere. Results: Percent change of signal intensity in the SMA (2.49 -3.06%) is lower than that of primary motor area(4.4 -7.23%). Percent change of signal intensity including activated voxels were observed almost equally in the right and left SMA. As for summation of activated voxels, primary motor area had significant difference between each hemisphere but not did the SMA. Conclusion: Preferred contralateral dominant hemisphere and hemispheric asymmetry were detected in the primary motor area but not in the SMA.

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Adsorption Kinetic and Thermodynamic Studies of Tricyclazole on Granular Activated Carbon (입상 활성탄에 대한 트리사이크라졸의 흡착동력학 및 열역학적 연구)

  • Lee, Jong-Jib;Cho, Jung-Ho;Kim, H.T.
    • Journal of Korean Society of Environmental Engineers
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    • v.33 no.9
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    • pp.623-629
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    • 2011
  • The adsorption characteristics of tricyclazole by granular activated carbon were experimently investigated in the batch adsorption. Kinetic studies of adsorption of tricyclazole were carried out at 298, 308 and 318 K, using aqueous solutions with 250, 500 and 1,000 mg/L initial concentration of tricyclazole. It was established that the adsorption equilibrium of tricyclazole on granular activated carbon was successfully fitted by Freundlich isotherm equation at 298 K. The pseudo first order and pseudo second order models were used to evaluate the kinetic data and the pseudo second order kinetic model was the best with good correlation. Values of the rate constant ($k_2$) have been calculated as 0.1076, 0.0531, and 0.0309 g/mg h at 250, 500 and 1,000 mg/L initial concentration of tricyclazole, respectively. Thermodynamic parameter such as activation energy, standard enthalpy, standard entropy and standard free energy were evaluated. The positive value for enthalpy, -66.43 kJ/mol indicated that adsorption interaction of tricyclazole on activated carbon was an exothermic process. The estimated values for standard free energy were -5.08~-8.10 kJ/mol over activated carbon at 200 mg/L, indicated toward a exothermic process.

A study on the development of phthalate plasticizers CRM in ABS resin (ABS 중 phthalates 가소제 CRM 개발에 대한 연구)

  • Jung, Jung-Sul;Park, Jung-Woo;Yoo, Seok;Kweon, Seong-Il;Hong, Sung-Taeg;Sun, Yle-Shik;Park, Cheon-Min;Choi, Chang-Hyoo
    • Analytical Science and Technology
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    • v.25 no.5
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    • pp.273-283
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    • 2012
  • Phthalate plasticizers are regulated by RoHS, REACH and CPSC as hazardous substances. Responding to these international environmental restrictions, we developed ABS certified reference material (CRM) for determination of phthalate plasticizers such as DMP, DEP, DBP, BBP, DEHP and DnOP. The candidate material has been made with ABS resin widely used in electric and electronic products and 6 kinds of phthalate plasticizers. The making of the material involved a series of processes like extruding, cooling, pelletizing, and drying using twin screw extruder. Then it has been certified according to ISO Guide 35. Using isotope dilution-gas chromatography/mass spectrometry (ID-GC/MS), homogeneity, short-term stability, and long-term stability were evaluated. The certified values were determined by using primary reference material (PRM) of KRISS for traceability. From now on, we will provide ABS CRM to national and international companies and research institutes after certification as certified reference material and registering on COMAR (code of reference material).