• Title/Summary/Keyword: 이종접합체

Search Result 53, Processing Time 0.025 seconds

TEM and Raman Spectrum Characterization of 3C-SiC/Si(001) Heterostructure Grown by Chemical Vapor Deposition (화학증착 방법으로 Si(001)기판 상에 성장된 3C-SiC 이종접합 박막의 투과전자현미경 및 라만 특성분석)

  • Kim, Dong-Geun;Lee, Byeong-Taek;Mun, Chan-Gi;Kim, Jae-Geun;Jang, Seong-Ju
    • Korean Journal of Materials Research
    • /
    • v.7 no.8
    • /
    • pp.654-659
    • /
    • 1997
  • HMDS[Si$_{2}$(CH$_{3}$)$_{6}$]단일 선구체를 이용하여 화학증착 방법으로 성장된 3C-SiC/Si(001) 이종접합박막의 특성을 XRD, 라만 스펙트럼 및 투과전자현미경(TEM)등을 이용하여 조사하였으며 시판되고 있는 상용 3C-SiC/Si 시편을 같은 방법으로 분석하여 특성을 비교검토하였다. $C_{3}$H$_{8}$-SiH$_{4}$-H$_{2}$혼합가스를 선구체로 이용하여 5$\mu\textrm{m}$두께로 성장된 상용 3C-SiC/Si 이종접합박막 시료의 XRD스펙트럼에서는 강한 3C-SiC(002)피크 만이 관찰되었으며, 라만 스펙트럼의 LO피크는 970nm$^{-1}$ 정도에서 강하게 나타났다. TEM 관찰 결과 다수의 전위, 쌍정, 적층결함 및 APB와 같은 결정결함들이 3C-SiC/Si 계면 근처에 집중적으로 분포되어 있었으며 성장된 박막은 단결정임을 확인할 수 있었다. 선구체로 HMDS를 사용하여 0.3$\mu\textrm{m}$ 및 2$\mu\textrm{m}$ 두께로 성장시킨 3C-SiC/Si 박막 시료의 XRD 스펙트럼은 다소 완만한 3C-SiC(002) 피크와 함께 3C-SiC(111)피크가 관찰되었으며, TEM으로 확인한 결과 소경각 결정립들이 약 5˚-10˚ 정도 방위차를 가지고 성장하여 기둥구조(columnar structure)를 이루고 있기 때문임을 알 수 있었다. 라만 스펙트럼 분석 결과 박막의 LO 피크가 967-969nm$^{-1}$정도로 다소 낮은 wavenumber쪽으로 이동되어 박막 내에 상당한 응력이 존재함을 확인할 수 있었다. 이와 같은 HMDS 3C-SiC박막의 특성은 성장 온도가 낮고 박막 성장용 가스로 사용한 HMDS 선구체에서 탄소가 과잉으로 공급되기 때문으로 제안되었다.다.

  • PDF

An Evaluation Method of fracture Toughness on Interface Cracks in Bonded Dissimilar Materials (이종 접합체의 계면균열에 대한 파괴인성의 평가방법)

  • 정남용
    • Transactions of the Korean Society of Automotive Engineers
    • /
    • v.11 no.4
    • /
    • pp.110-116
    • /
    • 2003
  • In this paper, an evaluation method of fracture toughness on interface cracks has been investigated under various mixed-mode conditions of the bonded scarf joints. Two types of the bonded scarf joints with an interface crack were prepared to analyze the stress intensity factors using boundary element method(BEM) and to perform the fracture toughness test. From the results of fracture toughness experiments and BEM analysis, an evaluation method of fracture toughness on interface cracks in the bonded dissimilar materials has been proposed and discussed.

Dry Compaction of Nanosize TiO$_2$Powders (산화 티타늄 나노분말의 건식가압성형)

  • 이해원;임건자;전형우;박종구;이종호
    • Journal of the Korean Ceramic Society
    • /
    • v.37 no.12
    • /
    • pp.1146-1149
    • /
    • 2000
  • 표면윤활층 처리와 540 MPa 까지의 진공가압성형을 통하여 나노 TiO$_2$과립 분말의 가압성형공정에서 나타나는 접합압력을 확인하였으며, 접합압력 상하에서 제조된 시편의 소결특성을 $700^{\circ}C$ 등온 소결을 통하여 분석하였다. 접합압력 이상에서 가압성형한 성형체를 $700^{\circ}C$에서 48시간 소결하여 96%의 높은 소결밀도와 112 nm의 평균 결정립 크기를 얻었다.

  • PDF

Stress Analysis of Brazed Interface in Dissimilar Materials by BEM (이종접합재 접합계면의 응력해석)

  • 오환섭;김시현;김성재;양인수
    • Journal of the Korean Society for Precision Engineering
    • /
    • v.20 no.7
    • /
    • pp.171-176
    • /
    • 2003
  • In this study, stress analysis using Boundary Element Method (BEM) was carried to investigate stress distribution in the brazing joint between a Hardmetal and a HSS. The two models were proposed to analyze the stress singularity in the interfaces of the brazing joint. The material type, thickness of the filler metal and the length of the vertical brazing adhesive are considered in the BEM analysis. As results, the peak point of the stress is founded to be in the lower interface of the brazed joint. It should be noted that the maximum stress of the peak point is being affected by the thickness and length of the brazing joint.

The Stress Analysis of Dissimilar Materials in Brazed Interface by BEM (이종재 브레이징 접합계면의 응력해석)

  • 오환섭;김시현;김성재
    • Proceedings of the Korean Society of Precision Engineering Conference
    • /
    • 1997.10a
    • /
    • pp.769-772
    • /
    • 1997
  • In this study, By employing two dimensional(2-D) Boundary Element Method(BEM) stress analysis was carried to investigate stress distributions on the brazing joint of a Hardmetal and a HSS. Two model was proposed to analyze stress singularity in brazed interface. The stress results from the BEM were considered influence of the kind of materials , thickness of filled metal and length of vertical brazing adhesive. From those obtained results , the peak point of stress was founded in the lower part of two interface was made by brazing. As the thickness and length changed, the maximum stress tended to change in the peak point.

  • PDF

Influence of Circular Hole for Fracture Criteria of Interface Crack in Bonded Dissimilar Materials (이종접합 계면균열의 파괴기준에 대한 원공의 영향)

  • 정남용
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
    • /
    • 1999.10a
    • /
    • pp.301-306
    • /
    • 1999
  • Application of bonded dissimilar materials in various industries are increasing. When these materials are used in structures, it needs to investigate strength evaluation applying fracture mechanics. Al/Epoxy bonded dissimilar materials with an interface crack and an interface crack emanating from an edge semicircular hole were prepared for the static tests so that experiment of fracture toughness were carried out. Stress intensity factors of interface cracks in bonded dissimilar materials were computed with boundary element method(BEM) and the fracture criteria of mixed mode crack were analyzed. From the results, the fracture criteria and the method of strength evaluation by the fracture toughness in Al/ Epoxy bonded dissimilar materials were proposed.

  • PDF

The Structural Performance of PSC Frame System with GerberCs beam (게르버 보 형식의 PSC 골조시스템의 구조성능)

  • Kim, Sang-Sik;Choi, Kwang-Ho;Lee, Jong-Gyu;Song, Hun
    • Proceedings of the Korea Concrete Institute Conference
    • /
    • 2002.10a
    • /
    • pp.341-346
    • /
    • 2002
  • 이 연구는 게르버 보 형식의 포스트텐션 PC 골조 구조 시스템의 실용화를 위해 골조 전체의 구조 성능 시험을 수행하며, 여기서 보-기둥 접합부 및 내민 보-단순 보 접합부의 구조 성능과 골조의 안전성을 확인한다. 시험은 400 mm$\times$800 mm 단면의 경간 3 m 보와 500 mm$\times$600 mm 단면을 갖는 높이 3 m 기둥의 실물 크기 시험체를 제작하여, 기둥에 80 톤의 축 하중을 준 상태에서 단순 보 중앙에 하중을 가력하여 기둥-보 접합부와 단순 보-내민 보 단면 축소 연결부의 구조성능을 파악한다. 시험 결과, 보 - 기둥 접합부는 예상 설계 하중 40톤 이상에서도 강 접합에 가깝게 거동하였고, 단순 보- 내민 보의 단면 축소 연결부는 경사철근의 사용으로 초기 균열 및 균열 확산에 대한 억제 효과가 있었으며, 예상 설계 전단력 40톤에서 안전하다는 것이 확인되었다.

  • PDF

Experimental Study on the Machenical Properties of Composite Beam Composed End Reinforced Concrete and Center Steel (RC-S 복합보의 역학적 특성에 관한 실험적 연구)

  • Kim, Cheol Hwan;Chae, Won Tak
    • Journal of Korean Society of Steel Construction
    • /
    • v.14 no.5 s.60
    • /
    • pp.675-682
    • /
    • 2002
  • The beam of composite structure composed of the RC structure in the end part and steel structure in the central palt were investigated during cyclic loading, in order to evaluate strength, stiffness, and deformational capacity. The parameters used in this study include the amount of reinforced steel bar between the steel beam and RC structure and the existence of the sticking plate. Test results showed that all specimens had stabilized hysteresis loops. Likewise, the specimens with sticking plate had higher load-carrying capacity compared with the one without it. In addition, the stiffness of the composite structure was higher than the steel structure. All specimens also showed good rotational capacity.

Evaluation of Fracture Toughness on Interface Cracks in Bonded Components of Dissimilar Materials (이종 접합부재의 계면균열 파괴인성의 평가)

  • Chung, Nam-Yong;Lee, Myung-Dae;Park, Chul-Hee
    • Proceedings of the KSME Conference
    • /
    • 2003.04a
    • /
    • pp.346-351
    • /
    • 2003
  • In this paper, an evaluation method of fracture toughness on interface cracks has been investigated under various mixed-mode conditions of the bonded scarf joints. Two types of the bonded scarf joints with an interface crack were prepared to analyze the stress intensity factors using boundary element method(BEM) and to perform the fracture toughness test. From the results of fracture toughness experiments and BEM analysis, an evaluation method of fracture toughness on interface cracks in the bonded components of dissimilar materials has been proposed and discussed.

  • PDF