• Journal of Biomedical Engineering Research
• /
• v.27 no.4
• /
• pp.189-196
• /
• 2006

Micro computed tomography (micro-CT) has been used for in vivo animal study owing to its noninvasive and high spatial resolution capability. However, the sizes of existing detectors for micro-CT systems are too small to obtain whole-body images of a small animal object with $\sim$10 micron resolution and a part of its bones or other organs should be extracted. So, we have introduced the zoom-in micro-tomography technique which can obtain high-resolution images of a local region of an live animal object without extracting samples. In order to verify our zoom-in technique, we performed in vivo animal bone study. We prepared some SD (Sprague-Dawley) rats for making osteoporosis models. They were divided into control and ovariectomized groups. Again, the ovariectomized group is divided into two groups fed with normal food and with calcium-free food. And we took 3D tomographic images of their femurs with 20 micron resolution using our zoom-in tomography technique and observed the bone changes for 12 weeks. We selected ROI (region of interest) of a femur image and applied 2D FDT (fuzzy distance transform) to measure the trabecular bone thickness. The measured results showed obvious bone changes and big differences between control and ovariectomized groups. However, we found that the reliability of the measurement depended on the selection of ROI in a bone image for thickness calculation. So, we extended the method to 3D FDT technique. We selected 3D VOI (volume of interest) in the obtained 3D tomographic images and applied 3D FDT algorithm. The results showed that the 3D technique could give more accurate and reliable measurement.

• Proceedings of the Korea Water Resources Association Conference
• /
• 2018.05a
• /
• pp.498-498
• /
• 2018

가뭄으로 인해 발생할 수 있는 가장 심각한 피해는 용수 부족으로 인한 수자원 시스템의 용수공급 실패이며, 따라서 가뭄 위험도는 사용 가능한 용수의 부족과 관련하여 정량화되어야 한다. 이러한 맥락에서 수자원 시스템의 가뭄 위험도를 평가하기 위해 주로 신뢰도(reliability), 회복도(resiliency) 및 취약도(vulnerability)와 같은 세 가지 이수안전도 평가지표가 사용된다. 이러한 평가지표는 각각 용수공급 실패가 평균적으로 얼마나 자주 발생하는지, 얼마나 오래 지속되는지, 또한 어느 정도의 규모로 발생하는지를 위험도를 정량화하는 것으로, 용수공급 실패사상의 빈도, 지속기간 및 심도를 나타낸다. 본 연구에서 DRI(Drought Risk Index)는 신뢰도, 평가도 및 회복도의 가중평균값으로 정의되며, 이는 지속기간과 심도를 변수로 하는 이변량 가뭄빈도해석과 같은 변수를 공유한다. 본 연구에서는 두 가지 형태의 DRI 를 이용하여 지역 가뭄 위험도 평가 기준 산정 방안을 제시하였다. DRI_O(observed DRI)는 용수부족 시계열을 통해 산정된 공급실패 사상으로부터 산정되며, DRI_D(designed DRI)는 이변량 빈도해석을 통해 산정된 특정 지속기간을 갖는 확률가뭄심도로부터 계산된다. 기후변화 시나리오를 이용해 DRI_O 를 산정함으로써 미래의 이수안전도를 예측할 수 있으며, 이를 DRI_D 와 비교하여 지역의 용수부족으로 인한 가뭄 위험도를 산정하는 방법을 제안하였다. 또한 기존에는 주로 과거 최대 가뭄사상을 목표안전도로 설정하였으나 DRI_D 를 이용하여 보다 현실적인 목표안전도를 설정할 수 있다. 낙동강 권역의 10 개 중권역의 10 개 기후변화 시나리오를 대상으로 분석을 수행한 결과 병성천 유역과 형산강 유역이 각각 최저 및 최고 위험도를 갖는 것으로 분석되었으며, 지역 안전도 기준은 평균적으로 재현기간 5-20 년 사이의 범위를 갖는 것으로 나타났다.

• Corrosion Science and Technology
• /
• v.17 no.6
• /
• pp.287-291
• /
• 2018

In this study, corrosion behavior of a SA178-A alloy used in the boiler tube of a district heating system was investigated in different environments where it was exposed to pure water, district heating (DH) water, and filtered district heating (FDH) water. After the corrosion test, the surface morphology was examined for observation of the number of pitting sites and pitting area fraction, using a scanning electron microscope. The DH water and FDH water conditions resulted in a lower corrosion potential and pitting potential, and revealed a significantly higher corrosion rate than the pure water condition. The pitting sites in the DH water (pH 9.6) were approximately eighteen times larger than those in the pure water (pH 9.6). Compared to the DH water, the corrosion potential became more noble in the FDH water condition, where iron ions were reduced through filtration. However, the corrosion rate increased in the FDH water due to an increased concentration of chloride ions, which deteriorated the stability of passive film.

• Korean Journal of Materials Research
• /
• v.29 no.1
• /
• pp.11-15
• /
• 2019

Severe wall thinning is found on the tube of a low-pressure evaporator(LPEVA) module that is used for a heat recovery steam generator(HRSG) of a district heating system. Since wall thinning can lead to sudden failure or accidents that lead to shutdown of the operation, it is very important to investigate the main mechanism of the wall thinning. In this study, corrosion analysis associated with a typical flow-accelerated corrosion(FAC) is performed using the corroded tube connected to an upper header of the LPEVA. To investigate factors triggering the FAC, the morphology, composition, and phase of the corroded product of the tube are examined using optical microscopy, scanning electron microscopy combined with energy dispersive spectroscopy, and x-ray diffraction. The results show that the thinnest part of the tube is in the region where gas directly contacts, revealing the typical orange peel type of morphology frequently found in the FAC. The discovery of oxide scales containing phosphate indicates that phosphate corrosion is the main mechanism that weakens the stability of the protective magnetite film and the FAC accelerates the corrosion by generating the orange peel type of morphology.

• Corrosion Science and Technology
• /
• v.18 no.2
• /
• pp.55-60
• /
• 2019

Corrosion failure in the convection part of peak load boiler (PLB) of the district heating system led to water leakage. Herein, Internal Rotary Inspection System (IRIS) inspection was employed to examine wall thinning and the cause of leakage in the flue tube. The corrosive products of the turbulator and tube were investigated using scanning electron microscope combined with energy dispersive spectroscopy, X-ray diffraction, and inductively coupled plasma (ICP). Majority of the serious corrosion damage was observed near the turbulator located in the upper flue tube. ICP analysis of the boiler water revealed oxide formation of sodium chloride in the lower end part of the flue tube. A cross-sectional view of the turbulator revealed the presence of double-layers of the oxide film, indicating environmental change during operation associated with water leakage. The outer surface of the turbulator consisted of the acid oxides such as $NO_x$ and $SO_x$ along with sodium and chloride ions. Dew-point corrosion is hypothesized as the main cause for the formation of acid oxides in the region of contact of the flue tube and the turbulator.

• Journal of The Korean Society For Urban Railway
• /
• v.6 no.4
• /
• pp.393-399
• /
• 2018

It is well recognized that residual stresses of the rails, generated from the manufacturing process including roller straightening and heat treatment, play an important role in determining fatigue and fracture properties of the rails. Thus, it has been a challenge to measure the residual stresses accurately. In this work, contour method was employed to evaluate the residual stresses existing in interior of the rails. The cross section perpendicular to the longitudinal direction of the rail was cut at a very slow rate using electric discharge machining (EDM), after which a laser-based flexural measuring instrument enabled us to precisely measure the flection of the cross section. The measured data were converted into the residual stresses using the commercial finite element package, ABAQUS, through a user-defined element (UEL) subroutine, and the residual stresses of the new rails (50N, KR60, UIC60) with three different specifications were compared.

• Corrosion Science and Technology
• /
• v.20 no.4
• /
• pp.204-209
• /
• 2021

Corrosion failure analysis of the flow plate, which is one of the accessories of the plate heat exchanger in a district heating system, was performed. The flow plate is made of 316 stainless steel, and water at different temperatures in the flow plate exchanges heat in a non-contact manner. The flow plate samples in which water mixing issues occurred were collected. Corrosion-induced pits, oxides, and contaminants were observed at locations where two plates are regularly in contact. The EDS analysis of the surface oxides and contaminants revealed that they were composed of carbon, silicon, and magnesium, which came from chemical adhesives. The IC/ICP analyses showed that the concentration of chloride ions was 30 ~ 40 ppm, which was not sufficient to cause corrosion of stainless steel. In the crevice, a local decrease in dissolved oxygen occurs along with an increase in chloride ions, thus forming an acidic environment. These environments destroyed the passive film of stainless steel, resulting in pits. Moreover, contaminants formed a narrower gap between the two metal plates and inhibited the diffusion of ions, thereby accelerating crevice corrosion.

• Corrosion Science and Technology
• /
• v.19 no.6
• /
• pp.296-301
• /
• 2020

Failure analysis on the welded type 304 pipe used for cooling water piping in the district heating primary side was conducted. Inorganic elements and bacteria in the cooling water and in corrosion products were analyzed, and the weldment was inspected by microscopy and a sensitization test. Corrosion damages were observed in the heat-affected zone, on weld defects such as incomplete fusion or excessive penetration caused by improper welding, or/and at the 6 o'clock position along the pipe axial direction. However, the level of concentration of chloride in the cooling water as low as 80 ppm has been reported to be not enough for even a sensitized type 304 steel, meaning that the additional corrosive factor was required for these corrosion damages. The factor leading to these corrosion damages was drawn to be the metabolisms of the types of bacteria, which is proved by the detection of proton, sulfur containing species, biofilms, and both bacteria and corrosion product analyses.

• Corrosion Science and Technology
• /
• v.21 no.2
• /
• pp.130-137
• /
• 2022

In this work, the degradation of high-pressure superheater tubes exposed to the flame of a duct burner in a heat recovery steam generator of a district heating system was evaluated. To assess the deterioration of the used superheater tube, the microstructure, microhardness, and tensile properties were investigated by comparison to an unused tube. The study found that a fin bound at the outer surface of the used tube became fragile only in the location facing the flame. This indicates that the tube was directly exposed to the flame from the duct burner or underwent abnormal overheating. While the unused tube showed a uniform value in hardness and equiaxial grain structure, the used tube revealed a decrease in hardness up to 105 HV and an increase in grain size with a plate-like morphology in the location facing the flame. The coarsening of the grain structure by the flame weakened the mechanical properties of yield strength, tensile strength, and elongation.

• Journal of the Korean Society for Heat Treatment
• /
• v.36 no.3
• /
• pp.153-160
• /
• 2023

The use of biogas is an industrially necessary means to achieve resource circulation. However, since biogas obtained from waste frequently causes corrosion in pipes, it is important to elucidate corrosion mechanisms of the pipes used for biogas transportation. Recently, corrosion failure occurred in a pipe which supplied for the biogas at the speed of 12.5 m/s. Pinholes and pits were found in a straight line along the seamline of the pipe. By using corrosion-damaged samples, residual thickness, microstructure, and composition of oxide film and inclusion were examined to analyze the cause of the failure. It was revealed that the thickness reduction of biogas pipe was ~0.11 mm per year. A thin sulfuric acid film was formed on the surface of the interior of a pipe due to moisture and hydrogen sulfide contained in a biogas. Near the seamline, microstructure was heterogeneous and manganese sulfide (MnS) was found. Pits were generated by micro-galvanic corrosion between the manganese sulfide and the matrix in the interior of the pipe along the seamline. In addition, microcracks formed along the grain boundaries beneath the pits revealed that hydrogen-induced cracking (HIC) also contributed to accelerating the pitting corrosion.