• Resources Recycling
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• v.7 no.5
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• pp.26-32
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• 1998

Recycline of used plastics is rather restricted due to their variety and difficulties in their separation. In this study, a reliable and economical method for the separation of PVC which utilizes an appropriate control of surface chemistry of pariticles was suggested. this method consists of modification of PET surface from hydrophobic to hydrophilic by NaOH solution and subsequent separation by a froth flotation technique. Flotation results were in terms of NaOH concentration, digestion temperature and time, temperature and pH of solution, PVC concentration. They could be separated up to 95~100% by this method.

• Journal of Energy Engineering
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• v.11 no.3
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• pp.276-282
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• 2002

The process of energy separation in a low Pressure vortex tube with compressed air as a work-ing medium is studied in detail. Experimental data of the temperature of the cold and hot air leaving the vortex tube are presented. The variation of the maximum wall temperature along the inner surface of the vortex tube and the temperature distribution in a vortex tube provide useful information about the location of the stagnation point of the flow field at the axis of the vortex tube. Analysis of the results enabled to find the optimum length of the vortex tube, the optimum shape of the Throttle and the usefulness of the Sleeve. In this study Outer tube is used for the exhaust application. The hot gas flow is turned 180$^{\circ}$and passes the out-side of the vortex tube a second time heating it. From this geometric setup of a vortex tube He effects of energy separation and the prediction of the ignition of Diesel Soot is presented by experimental data.

• Membrane Journal
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• v.26 no.6
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• pp.449-457
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• 2016

In this study, polyvinylidene fluoride (PVDF) membrane with excellent mechanical properties and chemical resistance was prepared and characterized for the application of water treatment. Dibutyl-phthalate (DBP) was used as a diluent for making a membranes through temperature induced phase separation (TIPS) method, and the crystallization temperature, melting point, cloud point and SEM image were observed with different ratio of diluent in polymer/diluent mixture. The crystallization temperature and melting point increased proportionally with the content of polymer, while the cloud point temperature decreased. Finally, it was confirmed that stable membrane could be manufactured at a polymer content of 62 wt% and a temperature $125^{\circ}C$ using the phase diagram of PVDF/DBP mixtures with temperatures.

• Korean Chemical Engineering Research
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• v.47 no.1
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• pp.54-58
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• 2009

Ketoprofen and ibuprofen are non-steroid anti-inflammatory drug(NSAID) that have analgesic and antipyretic properties. (S)-ketoprofen and (S)-ibuprofen have pharmacological activity, while (R)-ketoprofen and (R)-ibuprofen are either inactive or have side effect. The chiral separation of racemic ketoprofen and ibuprofen enantiomers was carried out by using a Kromasil HPLC column. Some chromatographic parameters (selectivity, resolution, number of theoretical plates and ${\Delta}H$) are calculated under different mobile phase compositions of hexane/t-BME/acetic acid and temperatures. The selectivity, resolution and number of theoretical plates were observed high at $25^{\circ}C$ and the composition of hexane/t-BME/acetic acid (80/20/0.1).

• Korean Chemical Engineering Research
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• v.52 no.1
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• pp.98-105
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• 2014

Lysozyme amounts to 0.3% in egg white and functions as an agent of cell lysis and activator of tissue reconstruction. Ion exchange chromatography is the most useful method of separation among affinity chromatography, ion exchange chromatography, and ultra-filtration. The aim of present study is to find the optimum pH and temperature for the separation of lysozyme in egg white within cation exchange gel filled glass column. And we compared results of experiments with those of simulations. Phosphate buffer was used, and pH and temperature were varied as 5~7 and $25{\sim}40^{\circ}C$ respectively. RP-HPLC was the tool for the retention time identification and quantitative analysis of lysozyme. OriginPro 8 measured the peak area of lysozyme chromatogram and quantified the eluted lysozyme. Largest amount of lysozyme was separated under the conditions of pH 5 and T $25^{\circ}C$.

• Journal of the Korean Chemical Society
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• v.38 no.9
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• pp.660-666
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• 1994

The effects of temperature and flow rate of eluent on the separation of adjacent lighter lanthanide pairs (La : Ce, Ce : Pr, Pr: Nd) have been studied with displacement chromatography. Two serial columns packed with Amberlite 120 cation exchange resin are used for loading and separation. The retaining ion is $H^+$ ion and the eluent is 0.012M and 0.015M of EDTA solution. The columns and the eluent are maintained at the temperature of 90$^{\circ}C$ and pressurized to reduce vaporizing in the ion-exchange resin column. The eluated solution is analyzed directly with ICP-AES. The separation factors of the lanthanide pairs, La: Ce, Ce :Pr, and Pr: Nd, are 4.6, 2.8, and 1.9, respectively and are higher than that from theoretical calculation at 25$^{\circ}C$. When the flow rate is reduced from 2.5 ml/min to 1.5 ml/min, the HETP is reduced from 1.60 cm to 0.88 cm. The separation efficency can be improved at lower flow rate of eluent and higher operating temperature. The recoveries of pure lanthanides than 99.9% are 49∼77% from this separation.

• Resources Recycling
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• v.32 no.6
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• pp.3-9
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• 2023

Separation of LED packages from PCBs and analysis of the adhesive components was conducted to enhance the recycling potential of LED modules. LED package was separated from PCBs using heat treatment under optimal conditions: temperature of above 250 ℃ and time of 20 minutes. The separation equipment can be established using a hot air injector with controlling the rotational speed of the internal screw. The separation efficiency of each type of substrate (aluminum and glass fiber) was investigated with the thickness range of the adhesive materials (0.25-0.30 and 0.30-0.35 mm). Under the optimal conditions, the efficiency can reach to 97.5% for both types of substrates with adhesive materials of thickness 0.25~0.30mm. Characterization of the residual adhesive substances from the separated LED package and PCB using microwave digestion and ICP analysis showed that the residue contained of 95% of Sn, less than 5% of Cu and Ag.

• Journal of Aerospace System Engineering
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• v.16 no.6
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• pp.123-128
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• 2022

This paper proposes a non-explosive separation device for the deployable SAR antenna. This device utilises a Ni-Cr wire to restrain the antenna's belt mechanism, and joule-heating is used to minimise the impact of deployment. After the Ni-Cr wire has been cut, the device is deployed through the preload of the belt mechanism. Considering the design load(99g) and preload conditions, FEM analysis for AL7050 and Ti was performed. This analysis revealed that the amount of deformation for AL7050 was 0.256 mm with a margin of +0.09. In addition, by performing orbital thermal analysis, the temperature distribution for AL7050 in the worst cold case is confirmed as -50 to +2℃ and -10 to +90℃ in the worst hot case. This analysis confirmed that the separation device would remain stable even in the worst environment.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.10 no.4
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• pp.695-701
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• 2009

Vortex tube is the device that can separate small particles from the compressed gas, as well as compressed gas into hot and cold flow. In this study, computational approach has been performed to analyze the characteristics of the vortex tube. Energy separation characteristics of the vortex tube has been tested for various geometric design parameters. For the given conditions, it is found that as the tube is lengthened, hot end temperature is reduced but cold end temperature does not influenced much. As the orifice diameter decreases, cold end temperature decreases. Also, as hot gas fraction increases, hot end temperature decreases. The results from this study can be used for the basic design parameter of the $CO_2$ reduction device.

• Journal of Energy Engineering
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• v.7 no.1
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• pp.44-56
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• 1998

Separate heat pipe exchanger is considered as the high thermal transportation equipment, because evaporator and condenser are separately positioned in the long distance. Its characteristics are that the working fluid is circulated naturally by the position height of two exchangers. But the operating characteristics are restricted by the temperature of hot and cold fluid, flow pattern and diameter of vapor line, etc. in this study, the vapor pressure and the minimum height of two exchangers are studied about the factors restricting the operating characteristics.