• Title/Summary/Keyword: 열 중량 분석

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Infrared Spectroscopy and Differential Scanning Calorimetry of Silk Fibroin/Hyaluronic Acid Blend Film (견피브로인/히아론산 브렌드 필름의 적외선 분광 분석 및 시차열분석)

  • Kweon HaeYong;Lee Kwang-Gill;Yeo Joo-Hong;Woo SoonOk;Han SangMi;Lee Yong Woo;Lee Jang Hern;Park Young Hwan
    • Journal of Sericultural and Entomological Science
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    • v.46 no.1
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    • pp.28-31
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    • 2004
  • Bombyx mori silk fibroin/hyaluronic acid blend films were prepared by mixing aqueous solution of B. mori silk fibroin and hyaluronic acid. According to the FTIR spectra, no interaction between silk fibroin and hyaluronic acid was found. The conformation of silk fibroin in blend films was changed from random coil to $\beta$-sheet structure by treatment of EDC ethanol solution. Thermal degradation peak of silk fibroin and hyaluronic acid was also not altered by blending each other. The average swelling ratio of silk fibroin/hyaluronic acid blend films was 70. Therefore, silk fibroin/hyaluronic acid blend films might be one of possible wound dressing materials.

Virgin Hair and Bleach Hair Thermal analysis study according to temperature change (버진 헤어와 블리치 헤어의 온도 변화에 따른 열분석 연구)

  • Park, Jang-Soon;Lim, Sun-Nye
    • Journal of Industrial Convergence
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    • v.19 no.3
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    • pp.91-96
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    • 2021
  • In order to express the ideal appearance, everyone, regardless of age or gender, invests boldly in appearance management. In particular, hair coloring and hair styling using irons are widely used and used. have. Therefore, for the purpose of presenting the efficient use of flat irons, the study of thermal analysis of virgin hair and bleach hair in 120℃ heat treatment is conducted. As a result of the study, it was found that the overall weight of bleached hair decreased more than that of virgin hair at all treatment temperatures of flat irons. Through this thermal analysis study that measures the weight change according to the temperature rise of virgin and bleached hair, beauty consumers provide information on the optimal temperature flat ironing procedure that can minimize hair damage and discoloration while maintaining color in hair subjected to physical friction. It is believed that it will provide them efficiently.

An Experimental Study on the Mechanical Properties of High Density Concrete Using Magnetite Aggregate (자철광 골재를 이용하는 철근콘크리트의 역학적 특성에 관한 관험적 연구)

  • 반호용;한천구;김을용
    • Magazine of the Korea Concrete Institute
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    • v.2 no.3
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    • pp.81-88
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    • 1990
  • For the protectioon of radioactive leakage, the quality control of main concrete structure in nuclear power plants is very important. So, this studey is designed to analyze the influence of kind of cement and aggregate on the mechanical properties of high density concrete. Test results of this study are as follows; 1)The slump of magnetite aggregate concrete(MAC) is found half value of nat.ural aggregate concrete (NAC). 2)As the effect of cement, the compressive strength of concrete using moderate heat cement is found higher 5-19 % than that of ordinary portland cement. 3)As the effect of fine aggregate, t.he compressive strength of MAC is found higher than that. of NAC below 340kg/$cm^2$ and lower t.han NAC above 340kg/$cm^2$. 4)As the effect of coarse aggregate, the compressive strength of MAC is found higher 17-22% than that of NAC.

Quality Characteristics of Cirsium setidens Nakai by Different Drying Method (건조 방법에 따른 곤드레 나물의 품질 특성)

  • Park, Sung Jin;Lee, Dae Won;Park, Sung Hye;Rha, Young-Ah
    • Culinary science and hospitality research
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    • v.22 no.2
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    • pp.104-114
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    • 2016
  • In this study, the quality characteristics of different drying methods of Cirsium setidens Nakai, which contains large amounts of biological substances, were investigated for the improvement of their practical use. During the drying period, the weight reduction was the highest with hot-air drying(82.7%). As for the general component and mineral contents analysis results of Cirsium setidens Nakai, there were no significant difference. Cyclic low pressure drying resulted highest amount of total phenolic components and 1,1-diphenyl-2-picrylhydrazyl (DPPH). Hence, cyclic low pressure drying method is the best method for enhancing antioxidant activity of Cirsium setidens Nakai.

Characteristics of Pearlescent Pigment using in Make-up Cosmetics (색조화장에 사용되는 진주광택 안료의 특성)

  • Kwak, Han-Ah;Choi, Eun-Young;Chang, Byung-Soo
    • Applied Microscopy
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    • v.39 no.1
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    • pp.41-48
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    • 2009
  • We investigated the morphological characteristics of the pearlescent pigment by using scanning electron microscope, energy dispersive X-ray spectrometry and thermal analyzer. The result is that the shape of pigment is platy polygonal form through observing the pearlescent pigment by the scanning electron microscope. The size of pigment is various and not formed in standardized size or shape. The pigment flakes were measured about from $30{\mu}m$ to $300{\mu}m$. The tip of the piece of pigment is pointed shape or angled. The result of observing them by the scanning electron microscope in magnifying high power is that the edge and the lateral face of them is an round form and the measurement of thickness is about $9{\mu}m$. As well using the high magnification scanning electron microscope, the surface of the pigment flake observed like rugged as coating with the $TiO_2$ element, the diameter of the coating particle is around 60 nm, then the coating particle consists of granular substance. Analysis of the configuration elements of pearlescent pigment using by the energy dispersive X-ray spectrometry is that O, Si, C, Na, Ca, Ti, Zn detected in the surface of pigment and its lateral face identifies similar components. In thermal analysis, there are no contained quantity differences between them in beginning from $100^{\circ}C$ to $800^{\circ}C$ showing thermal analysis, 1.1% out of contained quantity reduced at $115^{\circ}C$, 1.7% dropped at $416^{\circ}C$, and 1.9% decreased at $797^{\circ}C$.

Synthesis of Low-Priced Catalyst from Coal Fly Ash for Pyrolysis of Waste Low Density Polyethylene (석탄비산재(石炭飛散災)로부터 저밀도(低密度) 폴리에틸렌 폐기물(廢棄物) 열분해용(熱分解用) 저가(低價) 촉매(觸媒) 합성(合成))

  • Jeong, Byung-Hwan;Na, Jeong-Geol;Kim, Sang-Guk;Mo, Se-Young;Chung, Soo-Hyun
    • Resources Recycling
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    • v.16 no.2 s.76
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    • pp.48-55
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    • 2007
  • A low-priced catalyst for pyrolysis of LDPE has been synthesized. Fly ash, which is waste material generated from coal-fired power plants was used as silica and alumna sources for solid acid catalyst. Amorphous silica-alumina catalysts (FSAs) were pre-pared by dissolution of silica and alumina from fly ash, followed by co-precipitation of the dissoluted ions. A series of LDPE pyrolysis were carried out in a thermogravimetric analyzer to investigate the effects of synthesis conditions such as NaOH/fly ash weight ratio and activation time one catalytic performance of FSAs. The physical properties of FSAs were examined and related to their catalytic performances. FSA(1.2-8) synthesized with NaOH/fly ash weight ratio of 1.2 and the activation time of 8 hours showed the best catalytic performance. The catalytic performance of FSA(1.2-8) was comparable with that of commercial catalysts and it was concluded that the FSA could be a good candidate for catalytic use in the recycling of waste polyolefins.

Loading Effects on Thermal Conductivity of Soils: Particle-Scale Study (하중 조건이 지반의 열전도도에 미치는 영향: 입자 스케일에서의 연구)

  • Lee, Jung-Hwoon;Choo, Jin-Hyun;Yun, Tae-Sup;Lee, Jang-Guen;Kim, Young-Seok
    • Journal of the Korean Geotechnical Society
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    • v.27 no.9
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    • pp.77-86
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    • 2011
  • The stress condition mainly dominates the thermal conductivity of soils whereas governing factors such as unit weight and porosity suggested by empirical correlations are still valid. The 3D thermal network model enables evaluation of the stress-dependent thermal conductivity of particulate materials generated by discrete element method (DEM). The relationship among dominant factors is analyzed based on the coordination number and porosity determined by stress condition and thermal conductivity of pore fluid. Results show that the variation of thermal conductivity is strongly attributed to the enlargement of inter-particle contact area by loading history and pore fluid conductivity. This study highlights that the anisotropic evolution of thermal conductivity depends on the directional load and that the particle-scale mechanism mainly dictates the heat transfer in soils.

Analysis on Thermogravimetric Characteristics about Copyrolysis of Waste Wood Chip and Linear Low Density Polyethylene (선형 저밀도 폴리에틸렌과 폐목재 우드칩 혼합열분해의 열중량 특성 분석)

  • Lee, Young-Man;Bae, Wookeun;Park, Young-Kwon
    • Applied Chemistry for Engineering
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    • v.22 no.1
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    • pp.87-90
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    • 2011
  • Copyrolysis of biomass/plastic mixture was carried out from room temperature to $600^{\circ}C$ with varing the heating rates of 10, 20, and $30^{\circ}C/min$ using a thermogravimetric analyzer. Waste wood chip (WWC) and linear low density polyethylene (LLDPE) were selected as a biomass and plastic, respectively. Individual pyrolysis temperature ranges were $430{\sim}550^{\circ}C$ and $230{\sim}600^{\circ}C$ for LLDPE and WWC, respectively. For the copyrolysis of WWC and LLDPE, the decomposition temperature range of WWC was not varied, while the decomposition temperature range of LLDEP was increased to a higher temperature. The results imply that the interaction might occur between LLDEP and WWC during copyolyis of LLDPE and WWC.

Investigation of the Effects of CNT Dosages on the Hydration and Heating Properties of Cement Composites with Low Water-to-binder Ratio (낮은 물-바인더 비를 갖는 시멘트 복합체의 CNT 첨가량에 따른 수화특성 및 발열특성)

  • Oh, Sungwoo;Jung, Sang-hwa;Chung, Wonseok;Choi, Young Cheol
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.22 no.6
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    • pp.182-188
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    • 2018
  • Recently, various researches on the utilization of carbon nanotube(CNT) with superior electrical conductivity and large surface areas into concrete have been actively conducted. Thus, mechanical and thermal properties of cement-flyash composites were evaluated concerning the CNT replacements. Based on the low binder-to-water ratio, the cement composites were produced with 0.2 % and 0.5 % of CNT solids. The compressive strengths with various ages, isothermal calorimetry measurement, SEM analysis, thermal conductivity of cement composites and thermal gravimetry analysis were implemented. As the amount of CNT addition was increased, the thermal conductivity of cement composites were also increased. Also, there was no significant mechanical property differences between mixtures with and without CNTs.

경주시 양남 제4기 역질 해안단구 퇴적층 풍화단면내 앨로패인(allophane) 교결층의 기원

  • 정기영;배진한;정창식
    • Proceedings of the Mineralogical Society of Korea Conference
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    • 2001.06a
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    • pp.115-115
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    • 2001
  • 경주시 양남면의 4기 단층으로 추정되는 수렴단층에 의해 절단되는 해안단구 퇴적층 풍화단면에서 저결정질 광물인 앨로패인 교결층을 기재하였다. 이들은 자갈퇴적층 내에 협재하는 수조의 모래층에 한정되어 형성되어 있으며, 3-17 cm 두께로 연장성이 매우 좋다. 편광현미경 관찰에 의하면 모래층에는 사장석편들이 다량 함유되어 있으며 앨로패인은 광학적 등방성의 치밀한 점토집합체들로서 사장석 입자를 선택적으로 교대하거나 자갈과 모래입자들을 피복하고 있다. 앨로패인은 광학적 이방성인 상하위층의 고령토질 점토피복물과 명확히 구분된다. 앨로패인의 전자현미분석에 의하면, Al/Si 원자비가 1.3-1.7 범위이고 평균값은 1.5이다. X선회절분석 결과 3.49$\AA$과 2.26$\AA$에서 두 개의 넓은 회절대가 관찰된다. 주사 및 투과전자현미경관찰에 의하면 앨로패인을 특정한 입자형태 없이 치밀한 겔상태를 이루고 있다. 열분석에 의하면 96$^{\circ}C$에서 큰 흡열피크와 992$^{\circ}C$에서 발열피크가 관찰되며, 총 45% 정도의 중량감소를 보인다. 사장석의 평균조성은 An$_{87}$이며, 사장석내 유리포유물의 전자현미분석결과는 화산암 화학분류도에서 현무암 영역에 도시된다. 이 지역의 기반암은 현무암질 라필리응회암이나 사장석편을 제외하고 벤토나이트화되어 있다. 따라서 해빈환경에서 사장석이 벤토나이트에서 분리되어 퇴적한 것으로 보인다. 앨로패인 교결층은 해수면 강하로 단구퇴적층이 지표로 노출된 후, Al의 함량이 높고 비교적 풍화에 약한 사장석이 선택적으로 풍화되어 생성되었다. 앨로패인으로 피복된 모래층 내의 자갈은 풍화반응이 지체되어 상하위층의 자갈과 비교하여 풍화도에 있어서 현저한 차이를 보인다.. 파이프 중심에서 외곽부로 갈수록 전기석의 함량은 줄어들고 있고 장석들이 알바이트ㆍ칼스베드 쌍정을 보이며, 흑운모가 각섬석보다는 우세하게 나타나고 있다. 전기석은 주상 결정, 자형 내지 반자형의 입자로 다색성을 보이며, 결정 중심에서 가장자리로 갈수록 파란색과 황갈색의 광학적 누대구조를 관찰할 수 있다. 일광광산에서 산출되는 전기석에 대한 현미경 관찰은 열수기원임을 지시하고 있다. 야외조사와 현미경 관찰의 예비조사에 의하면 일광광산의 전기석이 형성된 환경은 다른2가지 화학적인 저장소의 혼합 효과의 결과로 생성되어진 것으로 예상된다. 일광의 화강암류를 만든 마그마는 전기석을 형성할 만큼의 Fe-Mg성분이 충분하지 않았을 것이다. 화강암 내에 흑운모와 각섬석의 결정작용에 의해 마그마의 Fe-Mg성분이 고갈되어지고 이로 인해 그 함량이 감소하며 상대적으로 마그마 내에 남은 붕소(B$_2$O$_3$)는 열수로 용리되고 흑운모, 각섬석과 평형을 유지하며 열수에 남아있게 된다. 잔류용융체에 남은 붕소의 함량은 전기석을 만들기에 충분함에도 불구하고, Fe-Mg 함량이 부족하여 마그마 기원의 전기석 결정을 만들 수가 없다가 광맥이 형성된 시기에 또 다른 열수가 공급되면서 이전의 평형이 깨지고 기존의 흑운모와 같은 염기성 광물이 붕소(B)를 함유한 새로운 열수와 반응하여 전기석을 형성한 것으로 예상한다. 앞으로 전암과 광물에 대해 지화학적 연구를 통해 화강암류와 전기석과의 지화학적 연관성, 주성분 원소와 열수의 특성과의 상관관계, 전기석의 기원(마그마 기원인지 열수기원인지)이 보다 정확하게 파악될 것이다. 마그마 진화에 따른 전기석의 성분변화와 기원을 이용하여 일광광산의 동광화대를 형성한 마그마 계에서 열수계로 이어지는 지질학적 과정을 이해할 수 있을 것이며, 암석 성인론적 지시자로서

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