• Journal of the Korea Academia-Industrial cooperation Society
• /
• v.9 no.2
• /
• pp.257-263
• /
• 2008

We have examined explosion characteristics of bituminous coal dusts in cement manufacturing process. In order to find the thermal properties, we investigated weight loss and ignition temperature of coal materials using TGA and DSC. Also specific surface area of dust was investigated. Dust explosion experiments with Hartman's dust explosion apparatus have been conducted by varying concentration and size of coal dust for explosion probability and lower limit explosion concentration. According to the results for thermal properties, there is a little change by dust size. However, the specific surface area of dust is increased by decreasing dust size. The explosion test results show that small size and increasing concentration of dusts make dust explosion easier. And we find that the lower limit explosion concentration of bituminous coal is $0.3mg/cm^3$ and the probability is 100% on $0.9mg/cm^3$ in 170/200 mesh used in cement manufacturing process.

• Proceedings of the Korean Society of Propulsion Engineers Conference
• /
• 2017.05a
• /
• pp.172-178
• /
• 2017

Thermal property is one of the important characteristic in the field of energetic materials. As the energy material is released during decomposition, DSC(Differential Scanning Calorimetry) is frequently used for the thermal analysis. In case of the dynamic DSC measurements, thermal dynamic change like melting is prevented from the thermal property measurements. And due to the predicting kg scale, the conditions of the heat exchange with the environment significantly is changed. In this study, As the method to resolve the problem, we predict the thermal aging property using the AKTS thermokinetic program from DSC measurements which performed isothermal method. Predicting the thermal aging properties from ARC(Accelerating Rate Calorimetry) measurement, we compare two results.

• Polymer(Korea)
• /
• v.37 no.1
• /
• pp.15-21
• /
• 2013

Encapsulation of a paraffin wax core as a phase change material with polystyrene shell and the its thermal characteristics caused by the encapsulation were studied. For the nanoencapsulation, the miniemulsion polymerization method was selected. The factors affecting the thermal properties of prepared nanocapsule particles of phase change material were analysed in aspect of the structure of crosslinking agents, amounts of surfactant, ratio of paraffin wax to monomer, and hydrophilicity of initiators. It was assumed that Oswald ripening plays the most important role in the changes of particle size, particle morphology, and thermal capacity of nanocapsule core. It was elucidated that the thermal capacity was also dependent on the hydrophilicity and crosslinking density of polystyrene shell components.

• Proceedings of the KIEE Conference
• /
• 2003.04a
• /
• pp.34-36
• /
• 2003

철심형 PMLSM의 열적인 특성, 디텐트력 해석 및 저감, 그리고 자계의 비선형성에 대하여 살펴보며, 이에 따른 설계 특성을 고려하였다.

• Proceedings of the Membrane Society of Korea Conference
• /
• 1996.10a
• /
• pp.69-70
• /
• 1996

Polyethersulfone(PES)은 열적 특성이 우수하고 넓은 pH 범위에서 사용이 가능하며 특히, 막 제조 특성이 우수하여 막 소재로서 지금까지 널리 사용되어 오고 있다. Polysulfone(PSf)에 비하여 구조적으로 친수성이 우수하고 열적 특성이 더 뛰어난 장점이 있지만, 친수화를 시키기가 어려워서 지금까지는 주로 PSf의 친수화 연구로 한정되었었다. PES가 PSf에 비해 친수성이 좋다고는 하지만 PES 자체가 여전히 소수성을 띠므로 막 운전시 막의 내부나 표면에 투과 물질이 흡착되어 일어나는 Fouling으로 인해 막의 수명을 단축시키며 운전 효율도 크게 떨어진다. 이러한 Fouling을 줄이기 위한 방법으로 여러 가지 방법이 있지만 본 연구에서는 막의 재질을 친수성으로 개질시켜서 Fouling억제를 시도하였다.

• Proceedings of the Korean Vacuum Society Conference
• /
• 1999.07a
• /
• pp.111-111
• /
• 1999

반도체 소자의 고집적화 및 고속화에 따라 다층 금속배선에서의 RC 지연이 전체 지연의 주된 요소로 되고 있다. 이런 RC 진연을 줄이기 위해서 현재 다층 금속배선의 층간 절연막으로 사용하고 있는 SiO2 박막(k~3.9)을 보다 낮은 유전상수(low-k)를 가지는 물질로 대체할 것이 요구된다. 층간 절연막으로서 가져야 할 가장 중요한 것은 낮은 유전상수와 높은 열적안정성($\geq$45$0^{\circ}C$)이다. 본 연구에서는 Toluene을 precursor로 사용한 PECVD방법으로 low-k 유사중합체 유기박막을 성장시켰으며 부동한 온도에서 성장된 박막의 특성을 비교하여 증착온도가 박막의 특성에 미치는 영향에 대하여 조사하였다. 유사중합체 유기박막은 platinum(Pt)기판과 silicon 기판위에 같이 증착되었다. Precursor는 4$0^{\circ}C$로 유지된 bubbler에 담겨지고 증발된 precursor molecules는 Argon(Ar:99.999%) carrier 가스에 의해 process reactor 내부로 유입된다. Plasma는 RF(13.56MHz generator로 연결된 susceptor 주위에 발생시켰다. Silicon 기판위에 증착한 시편으로 Fourier transform infrared (FTIR) spectra 및 열적 안정성을 측정하였고, Pt 기판위에 증착한 시편으로 Al/유기박막/Pt 구조의 capacitor를 만들어 열적안정성을 측정하였고, Pt 기판위에 증착한 시편으로는 Al/유기박막/Pt 구조의 capacitor를 만들어 K값 및 절연성을 측정하였다. Capacitance는 1MHz 주파수에서 측정하였다. 열적안정성은 30분동안 Ar 분위기에서 annealing하기 전후의 증착막의 두께의 변화를 측정함으로써 조사하였으며 유기박막의 두께는 surface profilometer로 측정하였다. 증착온도가 45$^{\circ}C$에서 15$0^{\circ}C$, 25$0^{\circ}C$로 높아짐에 따라 k값은 높아졌지만 대신 열적안정성은 좋아졌다. plasma power 30W인 경우 45$^{\circ}C$에서 증착했을 때 유전상수는 2.80으로 낮았지만 40$0^{\circ}C$에서 30분 동안 열처리한 후 두께가 49% 감소하였다. 그러나 25$0^{\circ}C$에서 증착했을 때 유전상수는 3.10으로 좀 높아졌지만 열적으로는 40$0^{\circ}C$까지 안정하였으며 45$0^{\circ}C$에서도 두께의 감소는 8%에 불과했다.

• Fire Science and Engineering
• /
• v.22 no.1
• /
• pp.84-92
• /
• 2008

Disclosed is a study related to the thermal characteristics of Pinus densiflora and Quercus dentate identifying the presence of any significant difference in the above trees, which are native to Young Dong Province of Korea, according to different regions of the trees such as branches, barks, living leaves and dead leaves. For this purpose, we have carried out a cone calorimeter test focusing on the variables such as mass loss, heat release, ignition time, flame holding time and concentrations of CO and $CO_2$. The results showed that the total mass loss was greatest in tree branches, whereas the ignition time of dead leaves was fastest both in Pinus densiflora and Quercus dantata. The flame holding times of dead leaves and barks were about $640{\sim}1,016s$ and the total heat release of dead leaves was around 60.1 $MJ/m^2$, twice the total heat release of living leaves. In addition, the maximum exhaust concentrations of CO and $CO_2$ in tree branches of Quercus dentata was 2.82 times higher than those of Pinus densiflora, respectively. From the foregoing, it was confirmed that there exist region-specific differential thermal characteristics in Pinus densiflora and Quercus dentata.

• Fire Science and Engineering
• /
• v.26 no.4
• /
• pp.82-88
• /
• 2012

To analyze the thermal characteristics of wire connection part that is connected to a screw-clamping terminal block depending on screw torque, the normal screw torque defined in KS C 2625 and the abnormal screw torque that can occur due to loosened screws resulting from defective work or aged deterioration were used as experimental variables. After the same load was applied to normal and abnormal screw torques, the thermal characteristics of the wire connector were measured and compared with a thermal imaging camera. The findings from this study will be used to detect heating due to defective screw torque at terminal block connections during electric safety inspection in the future and minimize the hazard of electric fire.

• Fire Science and Engineering
• /
• v.31 no.4
• /
• pp.111-118
• /
• 2017

The present paper is a study on the risk analysis of complex electrical fire by the partial disconnection and tracking. First, in order to analysis the single cause of electrical fire risk by the partial disconnection, the thermal characteristic has been measured by the change in the number of strands and the rated current of a wire. And then, in order to analysis the electrical fire risk by complex cause, an experiment on the accelerated tracking has been carried out in a condition of partial disconnection and confirmed the fire relation between partial disconnection and tracking. From the experiment, if the partial wire disconnection acts as a single cause, the existing thermal characteristics generated by the flowing current has appeared more clearly by the increase in the flowing current due to the complex action of tracking. Accordingly, the disconnection of strands has appeared by the complex cause due to the drastic temperature increase which was not generated in the single cause. Namely, it has been confirmed that if the partial disconnection and tracking act complexly rather than the risk of electrical fire by the existing partial disconnection, relatively its risk has been increased in large.

• Fire Science and Engineering
• /
• v.24 no.6
• /
• pp.7-12
• /
• 2010

This paper is aimed the measurement and estimation the thermal interrelation based on leakage current. The leakage models are analyzed by parameters in open and closed (Panel) states and with wood dust and rainwater, charcoal powder in leakage current occurred point. The thermal characteristic of open state that leakage current is inputted in 90 mA is higher in charcoal powder ($105^{\circ}C$) than in wood dust and rainwater ($88.8^{\circ}C$). Charcoal powder that is inputted in 110 mA shows high thermal characteristic ($238.6^{\circ}C$) and the thermal ($238.6^{\circ}C$) is caused by material strain of electrical wire insulation and Panel. The closed state in 90 mA is higher in charcoal powder ($250.6^{\circ}C$) than in wood dust and rainwater ($90.8^{\circ}C$). The open and closed state appear thermal characteristics of two times in charcoal powder than in wood dust and rainwater. The thermal data that are open and close states are used electrical fire investigation and thermal characteristic for Leakage current.