• Proceedings of the Korean Vacuum Society Conference
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• 2013.02a
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• pp.258-258
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• 2013

최근 건조 제품의 양질화, 고급화 및 편의화가 요구되어 이를 충족시키기 위한 새로운 건조방법이 계속 개발 되어 왔다. 이러한 방법들 중에서 저온과 진공하에서 건조가 이루어지는 진공 동결 건조는 가장 완벽한 건조 방법으로 최근 실용화 되고 있다. 진공동결건조란 건조의 한 종류로 수분을 함유한 시료를 동결시킨 후 진공펌프를 이용하여 수증기압을 3중점 이하로 낮추어 얼음을 직접 증기로 만드는 승화의 원리에 의해서 얻어진다. 분무진공동결건조의 특징은 (1) 물리적구조의 보존성, (2) 화학적인 안정성, (3) 생물학적인 활동의 보존성, (4) 제품의 높은 복원성 및 재생성이다. 따라서 분무진공동결건조 기술은 크게 진공, 분무, 동결, 건조, 멸균 등과 같은 요소기술의 복합기술이라 할 수 있다. 분말을 제조하기 위해서 진공동결건조 후 분쇄하는 방법을 사용하나 본 방법에서는 정밀화학품 제조를 위해서 분무진공동결건조 방식을 사용한다. 이를 통하여 적당한 크기인 5~10 um의 입경 제조가 가능하고, 공기동력학적인 입경이 기존 방식에 비해 작아서 허파까지의 운반효율이 1.5~2배 우수하다. 화학, 의학 분야에서의 분무동결 건조는 주로 민감한 제품, 즉 생물학적 고유성의 손상 없이 물을 제거하는데 사용되어 영구적으로 저장 가능한 상태로 보관할 수 있으며 물의 첨가로 원상태로 복구할 수 있어서 매우 각광을 받고 있다. 의약용 냉동건조 제품은 항생물질, 박테리아, 혈청, 백신, 검사 약물, 단백질을 포함하는 생물공학 제품들, 세포, 섬유, 화학제품 등이 있으며 주로 vial 또는 ampule 상태로 건조가 이루어진다.본 연구에서는 원료를 $-194^{\circ}C$의 액체질소에 분무시켜 동결된 미립자를 형성한 후 진공 및 저온상태에서얼음의 승화(sublimation)에 기반한 1차 건조와 수증기 탈착(desorption)에 기초한 2차 건조 과정으로 구성된 분무진공동결건조기를 개발하였다. 분무동결 과정의 해석을 통해 2유체식 노즐을 통해 분무된 미세 입경의 액적이 액체 질소 표면까지 도달하는 회수률, 분무 노즐의 위치, 운전 조건 및 용기의 설계의 최적화를 수행하였다. 초기 액적속도, 분무노즐의 높이, 흡입구 추가에 따른 액적 유동 및 회수의 특성을 제시하였으며 이를 통한 분사시스템 고도화 가능성을 제시하였다. 구형의 미세 입자가 적층된 제품의 동결건조 공정의 해석은 흡착승화 모델(sorption sublimation model)을 기반으로 다음과 같은 열전달, 물질전달, 상변화 모델을 고려하여 유도되었다. 분무노즐 및 냉동/진공 배기계 시작품을 개발하여, 표면의 고다공도를 갖춘 입경 3~20 m 정도의 시료를 얻을 수 있으며, 동역학적 입경 5 m 충족함을 확인하였다.

• Journal of the KSME
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• v.23 no.4
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• pp.288-294
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• 1983

고속기류에 의한 수표면의 유통은 호수나 강에서 흔히 볼 수 있는 물리적인 현상으로서 기류의 속도가 증가함에 따라서 수표면에서 액적이 발생하게 되는 이른바 액체미립화 현상(atomization )이 일어나게 된다. 이러한 액체의 미립화는 내연기관에서의 분무연소에서 부터 가정에서 습도를 유지하는 가습기 및 살충제분무기에 이르기까지 그 운용도가 매우 광범위하며 최근에 이르러 액체미립화가 유체역학의 한 부분을 차지하는 단계에까지 이르러 매년 각국에서 미립화에 대한 심포지움이 개최되고 있으며 연구실적면에서는 미국보다도 오히려 가까운 일본에서 미립화에 대한 연구가 더 활발히 진행되고 있는 반면 아직 우리나라에서는 이렇다할 연구가 없으며 미립 화에 관한 논문도 불과 한두 편에 이르는 실정이다. 이러한 중요한 물리적인 현상에 대해 좀더 자세한 이해를 위해서는 액체와 기체의 상호접촉면에서의 정량적인 특성에 대한 연구가 필요하며 이러한 정량적 인자에는 (1) 액막의 평균두께 (2) 액막내의 속도분포, (3) 액막표면의 파고, 파장의 파면구조, (4)기체중의 속도분포 등이 있다.

• Polymer(Korea)
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• v.32 no.2
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• pp.183-188
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• 2008

Reinforced open cell micro structured foams were prepared by the polymerization of high internal phase emulsions incorporating inorganic thickeners. Organoclays were used as oil phase thickener, and sodium montmorillonite was used as aqueous phase thickener. Rheological properties of emulsions increased as oil phase thickener concentration and agitation speed increased, due to the reduced drop size reflecting both competition between continuous and dispersed phase viscosities and increase of shear force. Drop size variation with thickener concentration could be explained by a dimensional analysis between capillary number and viscosity ratio. Upon the foams polymerized by the emulsions, compression properties, such as crush strength and Young's modulus were measured and compared. Among the microcellular foams, the foam incorporated with an organoclay having reactive group showed outstanding properties. It is speculated that the exfoliated silicate layers inside polystyrene matrix, resulting in nanocomposite foam, are the main reason why this foam has enhanced properties.

• Journal of the Korean Society of Propulsion Engineers
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• v.8 no.2
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• pp.39-45
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• 2004

Experiments were performed in a two-phase swirling spray facility that has been described elsewhere. Measurements of spray transport and drop size distribution are analyzed over wide ranges of air to liquid mass flow ratios, utilizing four different internal mixing pneumatic nozzles. The spatial distributions of mean velocities. fluctuating velocities, and velocity-diameter correlation were quantitatively analyzed. Also, the exponential correlation curves were obtained with ALR along the spray centerline, which indicated an approximately identical formulation regardless of ALR. It indicated that the atomization characteristics were remarkably superior in the case of 30o of swirl angle with higher ALR. Among other things. nozzle configuration is one of the significant parameters affecting spray phenomena from an internal mixing nozzle. Turbulence intensities are increasingly degenerated with an increase of nozzle configuration, allowing a rapid increment of drop size distribution.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.35 no.9
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• pp.799-804
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• 2007

The behavior of spray emanating from an injector to be employed in a liquid-propellant thrust chamber is investigated by optical measurement techniques. The injector has eight holes, each of which has 30 cant angle from the center-axis with the diameter of 0.406 mm. In order to examine an atomization process according to the spray-generation conditions and the evolution along spray downstream, variational features in the velocity and size of droplets obtained through Dual-mode Phase Doppler An 799emometry (DPDA) are delineated and discussed together with instantaneous plane images captured by using Nd:Yag laser sheet beam. A categorization of spray-flow regime representing the atomization and turbulent nature is made through evaluating the non-dimensional parameters, i.e., Reynolds number and Weber number based upon the theoretical injection velocity. These qualitative and quantitative data of spray breakup will be a firm basis for the design of brand-new thruster

• Journal of the Korean Society of Propulsion Engineers
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• v.22 no.4
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• pp.44-54
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• 2018

In a spray experiment using a venturi mounted on a lean premixed LPP injector, droplets appear to have non-uniform distributions. To solve this problem, the exit angle of the venturi was changed to form a dump surface on the nozzle neck. The dump surface improved the atomization performance and minimized droplet loss while forming recirculation zone in the venturi exit. In order to solve the non-uniform spray of the injector, the flow characteristics inside the venturi and SMD of the spray are compared. Finally, an optimum venturi shape is selected to minimize the spray loss and improve the spray performance.

• The Journal of the Convergence on Culture Technology
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• v.10 no.2
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• pp.531-536
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• 2024

Control drones, which are recently classified as smart agricultural machines in the agricultural field, are striving to build smart control and automatic control systems by combining hardware and software in order to shorten working hours and increase the effectiveness of control in the aging era of rural areas. In this paper, the characteristics of the nozzle dedicated to the control drone were analyzed as a basic study for the establishment of management control and automatic control systems. In order to consider various variables such as the type of various drone models, controller, wind, flight speed, flight altitude, weather conditions, and UAV pesticide types, related studies are needed to be able to present the drug spraying criteria in consideration of the characteristics and versatility of the nozzle. Therefore, to enable the consideration of various variables, flow analysis (CFD) simulation was conducted based on the self-designed nozzle, and the theoretical and experimental values of the droplet distribution were compared and analyzed through water reduction experiments. In the future, we intend to calculate accurate scattering in consideration of various variables according to drone operation and use it in management control and automatic control systems.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.25 no.7
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• pp.923-932
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• 2001

A series of experiments were conducted to generate fine liquid(water) drops through the electrohydrodynamic atomization process. The atomization mode depended on flow rate and DC voltage input. For water, having electric conductivity larger than 10(sup)-7S/m, the spindle mode turned out to be the only mode to generate uniform-size drops within the range of 30-450 microns that have wide applications. Within this mode, both the uniformity and the fineness of drops were improved at an optimum voltage input for a given flow rate. This optimum voltage increased with increasing of the liquid flow rate. Another important parameter considered was the nozzle material with different electric conductivity and liquid wettability. A stainless-steel nozzle (the material with high electric conductivity and high liquid wettability) and a silica nozzle (the electrically non-conducting material with low liquid wettability) were tested and compared; and more uniform drops could be obtained with the silica nozzle.

• Journal of the Korean Society of Propulsion Engineers
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• v.12 no.1
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• pp.16-22
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• 2008

The effect of two-phase spray injected into subsonic cross-flow was studied experimentally. External-mixing of two-phase spray from orifice nozzle with L/d of 3 was tested with various air-liquid ratio that ranges from 0 to 59.4%. Trajectory of spray and breakup phenomena were investigated by shadowgraph photography. Detailed spray structure was characterized in terms of SMD, droplet velocity, and volume flux using PDPA. Experimental results indicate that penetration length was increased and collision point of liquid jets approached to nozzle exit and distributions of mist-like spray were obtained by increasing air-liquid ratio.

• Journal of the Korean Society of Visualization
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• v.5 no.2
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• pp.39-47
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• 2007

This paper describes an experimental study on the droplet formation and the subsequent motion in a microchannel having a cross junction. While one kind of liquid (pure water or water-surfactant mixture) is drawn into a horizontal inlet channel, the other kind (oil) is introduced through two vertical inlet channels. Due to the effect of surface tension on the interface between the two fluids, the droplets of the first fluid are formed near the cross junction. In this study, we have found that the droplet formation is affected even by slight difference in the surface tension. When the surface tension between two fluids is decreased, the droplet size is decreased in order to keep the equilibration between the pressure and the surface tension. In addition, the time interval between each of the droplet formations is decreased and the distance between droplets is also decreased when the surface tension is decreased.