• Title/Summary/Keyword: 액적분무

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Preparation of Mesoporous and Spherical-shaped Silica Particles by Spray Pyrolysis (분무열분해 공정을 이용한 메조기공을 가지는 실리카 구형입자의 제조)

  • Baek, Chul-Min;Jung, Kyeong Youl;Park, Kyun Young;Park, Seung Bin;Cho, Sung Baek
    • Korean Chemical Engineering Research
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    • v.46 no.5
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    • pp.880-885
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    • 2008
  • Spray pyrolysis was applied to prepare spherical silica particles with mesopores of a regular structure. The physical properties such as surface area, pore size, pore structure, particle size, and morphology were studied by BET, SEM, SAXS, and DLS analysis. At a fixed gas flow rate, the BET surface area changed from 200 to $1,290m^2/g$ as changing the CTAB/TEOS molar ratio from 0.05 to 0.3. At a fixed CTAB/TEOS ratio, the surface area of silica particles was varied from 1,062 to $1,305m^2/g$ with changing the gas flow rate from 10 to 40 l/min. The average pore size measured by BJH desorption was about $21{\sim}23{\AA}$ and not significantly influenced by the CTAB/TEOS ratio and the gas flow rate. Finally, the highest surface area which was $1,305m^2/g$ were obtained when the CTAB/TEOS ratio and the gas flow rate were 0.2 and 20 l/min, respectively. According to SAXS analysis, the prepared silica particles showed a strong peak at $2{\theta}=2.6^{\circ}$ and two minor peaks around $2{\theta}=4.4^{\circ}$ and $5.1^{\circ}$, which are due to regular mesopores of hexagonal structure. The morphology of silica particles prepared were spherical shape and the average particle size was $1.0{\mu}m$.

Spray and Combustion Characteristics of High Density Hydrocarbon Fuel (고밀도 탄화수소계 연료의 분무 및 연소특성)

  • Lim, Byoung-Jik;Moon, Il-Yoon;Seo, Seong-Hyeon;Han, Yeoung-Min;Choi, Hwan-Seok
    • Journal of the Korean Society of Propulsion Engineers
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    • v.10 no.4
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    • pp.26-33
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    • 2006
  • The use of high-density propellants can provide performance advantages in space launch vehicles by allowing an improved structural ratio due to smaller propellants tanks. The Jet A-1 fuel is currently used in Korean space launch vehicle development and it has lower density than other advanced hydrocarbon fuels such as RP-1 or RG-1. In this paper, the results of hydraulic and combustion tests conducted for the two newly developed densified hydrocarbon fuels are presented and they are compared with the results of Jet A-1. Conclusively, the two densified hydrocarbon fuels presented equivalent or even higher combustion performance compared to the Jet A-1 and the performance difference was found to be more obvious in the injector of external mixing.

Spferical fine ZnO Particles prepared from zinc nitrate by Ultrasonic Spray Pyrolysis technique (초음파 분무 열분해법에 의해 질산아연용액으로부터 구형의 ZnO 미분말 제조)

  • 이서영;김영도;신건철
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.1 no.2
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    • pp.46-58
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    • 1991
  • The synthesized ZnO powder was prepared by spray pyrolysis method using ultrasonic vibrator. The starting solutons were the aqueous solution of $Zn(NO_3)_2\cdot6H_2O$. The concentration was prepared 1M, O.5M, O.25M, and O.lM. The Nz carrier gas was 2.3cm$\cdot{sec}^{-1}$. The prepared powder from the $Zn(NO_3)_2{\cdot}6H_2O$ aqueous solution was Zine oxide with hexagonal structure. The shape of prepared powder was fine size, narrow size distribution, agglomerate-free, nearly sphere particle. Also, the particle size was about $ 0.28-0.61\mum$.

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The study on the variable orifice spray of the steam power plant desuperheater (화력발전설비의 과열증기저감용 가변오리피스 분사 특성)

  • Kim, Jeong-Sik;Kim, Kwang-Hee;Lee, Jong-Sun
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.14 no.1
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    • pp.63-68
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    • 2013
  • The steam power plant is becoming more important to supply a stable power lately. Desuperheater of the steam power plant facility plays a role in maintaining the proper superheat to avoid damage turbine power due to the superheated steam produced in the boiler. In this study, when the steam flows $530^{\circ}C$, 36.7 kg/s, 1.36 MPa in the 460mm pipe, variable orifice nozzle developed in Korea was carried out the performance analysis in coolant injection conditions of $150^{\circ}C$, 4.28 MPa. Findings, steam pipe coolant temperature was maintained at $446^{\circ}C$ and sprayed droplet size was verified by $50{\mu}m$ or less.

A Study on the Optimal Generation Conditions of Micro-Droplet in Electrostatic Spray Indirect Charging Method (정전 분무 간접 하전 방식에서 미세액적 최적 발생 조건에 관한 연구)

  • Jihee Lee;Sunghwan Kim;Haiyoung Jung
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.37 no.1
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    • pp.79-87
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    • 2024
  • This paper is a study on the optimal microdroplet generation conditions in indirect charging electrostatic spraying. Unlike the direct charging method, which applies power to the nozzle, the indirect charging method applies power to the discharge electrode between the nozzle and the collection electrode. Therefore, an electrically simplified system can be obtained by minimizing the insulation part a stable spray pattern can be obtained with a wide spray angle, and a stable spray pattern can be obtained with a wide spray angle. To conduct the study, an indirect charging type electrostatic spray visualization system was constructed and the static characteristics of the microdroplets were analyzed through image processing of the spray shape of the microdroplets. The total number of microdroplets and the number of microdroplets per power consumption are confirmed according to the changes in the distance between the discharge electrode and the collection electrode, the flow rate, and the applied voltage, which affect the generation of microdroplets, and using this, the optimal generation conditions are derived and the corresponding microdroplet size distribution was analyzed. As a result of the experiment, it was confirmed that the optimal generation condition was at a flow rate of 15 to 20 mL/min and a voltage of -22.5 to -25 kV in terms of the number of microdroplets, and at a flow rate of 15 to 20 mL/min and a voltage of -20 kV in terms of energy consumption efficiency.