• Journal of Food Hygiene and Safety
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• v.29 no.4
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• pp.312-315
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• 2014

The present study demonstrated the development and validation of the method for the quantification of phenol in food using gas chromatography coupled with mass spectrometry (GC-MS). After spiking of internal standard (Phenol-$d_5$) to food, those samples were extracted with organic solvent mixture (acetone : dichloromethane = 1 : 1, v/v) using ultra sonic extractor and cleaned by gel permeation chromatography (GPC) technique. The amount of phenol was determined by GC/MS. To validate the developed method, we evaluated parameters were the selectivity, linearity, accuracy, precision, and recovery. To demonstrate the selectivity of the method, blank samples of rice, corn, and fish(mackerel) were prepared and subjected to GC-MS analysis. To verify the linearity of the method, six different standard concentrations of phenol at 0.01, 0.05, 0.1, 0.5, 1 and 2.5 mg/kg were evaluated. The correlation coefficient ($r^2$) of calibration curve was 0.9999. The recovery rate for phenol standard calculated by internal standard method were 82.2~101.5% for samples fortified with 0.25, 0.50, and 1.0 mg/kg, respectively. Also the repeatability and reproducibility for validation of precision were 0.2~5.5%. According to the result of the validation, this established method was suitable for AOAC guideline. The limit of detection (LOD) for phenol analysis were 0.03~0.1 mg/kg, and the limit of quantification (LOQ) were 0.1~0.3 mg/kg. Therefore, we established the optimal analysis method for determination of phenol in food using GPC and GC/MS.

• Journal of the Korea Institute of Information Security & Cryptology
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• v.14 no.3
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• pp.13-25
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• 2004

The key exchange protocols are very crucial tools to provide the secure communication in the broadband satellite access network. They should be required to satisfy various requirements such as security, key confirmation, and key freshness. In this paper, we present the guideline of security functions in BSAN(Broadband Satellite Access Network), and analyze the specification of the security primitives and the hey exchange Protocols for the authenticated key agreement between RCST(Return Channel Satellite Terminal) and NCC(fretwork Control Centre). In addition, we propose the security specification for a domestic broad satellite network based on the analysis on the analysis profile of ETSI(European Telecommunications Standards Institute) standards. The key exchange protocols proposed in ETSI standard are vulnerable to man-in-the-middle attack and they don't provide key confirmation. To overcome this shortcoming, we propose the 4 types of the key exchange protocols which have the resistant to man-in-the-middle-attack, key freshness, and key confirmation, These proposed protocols can be used as a key exchange protocol between RCST and NCC in domestic BSAN. These proposed protocols are based on DH key exchange protocol, MTI(Matsumoto, Takashima, Imai) key exchange protocol, and ECDH(Elliptic Curve Diffie-Hellman).

• Journal of Food Hygiene and Safety
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• v.37 no.5
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• pp.297-305
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• 2022

Antioxidants are food additives that extend the shelf life of food products by preventing lipid rancidity caused by active oxygen. They can either be naturally-derived or manufactured synthetically via chemical synthesis. In this study, method validation of five synthetic antioxidants, namely butylated hydroxyanisole, butylated hydroxytoluene, tertiary butylhydroquinone, propyl gallate, and disodium ethylenediaminetetraacetic acid, was performed using a high performance liquid chromatography-ultraviolet visible detector, and the method applicability was evaluated by analyzing foods containing antioxidants. The coefficient of determination (R²) average was 0.9997, while the limit of detection and limit of quantification were 0.02-0.53 and 0.07-1.61 mg/kg, respectively. The intra and inter-day accuracies and precisions were 83.2±0.7%-98.7±2.1% and 0.1%-5.7% RSD, respectively. Inter-laboratory validation for accuracy and precision was conducted using the Food Analysis Performance Assessment Scheme quality control material. The results satisfied the guidelines presented by the AOAC International. In addition, the expanded uncertainty was less than 16%, as recommended by CODEX. Consequently, to enhance public health safety, the results of this study can be used as basis data for evaluating the intake of synthetic antioxidants and assessing their risks in Korea.

• KSCE Journal of Civil and Environmental Engineering Research
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• v.30 no.5D
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• pp.453-459
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• 2010

In the study of traffic safety, it is utmost important to obtain more reliable estimates of the expected crashes for a site (or a segment). The observed crashes have been mainly used as the estimate of the expected crashes in Korea, while the empirical Bayes (EB) estimates based on the Poisson-gamma mixture model have been used in the USA and several European countries. Although numerous studies have used the EB method for estimating the expected crashes and/or the effectiveness of the safety countermeasures, no past studies examine the difference in the estimation errors between the two estimates. Thus, this study compares the estimation errors of the two estimates using a Monte Carlo simulation study. By analyzing the crash dataset at 3,000,000 simulated sites, this study reveals that the estimation errors of the EB estimates are always less than those of the observed crashes. Hence, it is imperative to incorporate the EB method into the traffic safety research guideline in Korea. However, the results show that the differences in the estimation errors between the two estimates decrease as the uncertainty of the prior distribution increases. Consequently, it is recommended that the EB method be used with reliable hyper-parameter estimates after conducting a comprehensive examination on the estimated negative binomial model.

• Korean Journal of Environmental Biology
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• v.39 no.3
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• pp.362-373
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• 2021

This study was conducted to establish mosquito distribution density and habitat in Sejong city for the prevention of mosquito-borne infectious diseases. The overall distribution of mosquitoes in the Sejong City was investigated, and the population density of mosquitoes in the old and new city was analyzed. Mosquito populations were determined using MOSHOLE and Blacklight traps once a week overnight. We also compared the mosquito population density of the old city and the new city, and the daily mosquito population was calculated using the data from the smart mosquito trap(DMS). Of all the study sites, Geumnam-myeon had the highest number of mosquitoes captured, and the dominant species were Armigeres subalbatus and Culex pipienspallens. Mosquito species with the potential for transmitting diseases were mainly found in Yeonseo-myeon (106 individual), and Geumnam-myeon (101). Mosquito collection rates by MOSHOLE trap and Blacklight trap were 58.49% and 41.51%, respectively. We concluded that using CO₂ would be the most suitable approach for collecting mosquitoes. The mosquito population density in the old city (92.05±7.04) was approximately twice that of the new city(51.50±4.05). Since Sejong City is divided into old city and new city, it is difficult to spot remarkable effects in a standardized way. For effective quarantine, differentiation of quarantine must be established. This study results provide a basis for Sejong City's integrated mosquito control guidelines, and therefore effective control of which we believe will help control the spread of mosquito-borne diseases and reduce damage from mosquitoes.

• Journal of Korean Society of Transportation
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• v.19 no.3
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• pp.45-58
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• 2001

Subjective mental workload assessment technique becomes a standard human factors and human-machine interface evaluation tool for the evaluation of ITS(Intelligent Transport Systems)-oriented information systems as well as the drivers visual activity analysis, physiological indices(GSR, EEG, ECG, etc.), secondary task performance, reaction time. vehicle control parameters(speed, steering behavior, accelerator control) that are widely applied for transportation and vehicle systems to evaluate the safety, to decide the system or design alternatives, and to establish the design guidelines. This paper reviewed and compared the most globally employed four mental workload assessment techniques that have been designed for the use of various human-machine systems and ITS-oriented in-vehicle information systems. NASA-TLX(National Aeronautics and Space Administration-Task Load Index). SWAT(Subjective Workload Assessment Technique), MCH(Modified Cooper-Harper) scale, and recently developed RNASA-TLX(Revision of NASA-TH) were compared in terms of sensitivity and subjective evaluations to derive the human-machine interface evaluation guidelines for the application of ITS-oriented in-vehicle information systems. Then, experiment results supported that RNASA-TLX is the prospective tool for the mental workload assessment of ITS-oriented in-vehicle information systems.

• Korean Journal of Construction Engineering and Management
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• v.14 no.4
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• pp.3-14
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• 2013

Recently, as the size of construction projects is getting bigger and higher, construction disasters have been being serious such as death, also it is hard to manage efficiently since there are plenty of informations about safety management. Thus on the spot & real time safety management is required and one of the ways to support these needs, conjunction with Information Technology(IT) has been being noticed. Accordingly, Personal Digital Assistant(PDA), Palmtop Computer and Tablet Personal Computer and so on have been adopted. However another inefficient sides are showed up such as limitation of equipment(weight, inconvenience of control and others). Meanwhile, exchanging and processing data are improved at wide area due to advance of mobile communication and introduction of smart mobile, which is a simple and convenient, is a proven at many aspects. In this research, to support effective safety management, the framework is realized in connection with smart mobile with finding the problems of safety management and deriving demands. Two smart mobile applications, which are Safety Management application and Safety Guideline application, enable that safety management in real time, less re-work and using safety information.

• Journal of Korean Tunnelling and Underground Space Association
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• v.23 no.6
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• pp.577-587
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• 2021

Room and Pillar method is an underground facility construction method that maximizes the strength of the in-situ ground. In order to secure the safety of the underground space, it is necessary to secure the safety of the room actually used in addition to the safety of pillar of the room and Pillar method. In this study, the evaluation method for the safety of the room and rock pillar in the room and pillar method was studied through numerical analysis. Numerical analysis was performed for a total of 125 cases using ground conditions, pillar width, and room width as parameters, and the results were derived. As for the safety factor of the pillar, it was confirmed that the safety factor increased when the strength of the ground increased, and it was confirmed that the increment in the safety factor decreased when the width of the pillar was widened. The room strain was evaluated by applying the Critical strain. As the width of the pillar became narrower, the Critical strain was higher, and as the width of the room became smaller, the Critical strain was smaller. As a result of the correlation analysis between the safety factor of the pillar and the room strain, it was possible to derive the upper limit of the room strain that can secure the standard safety factor of the pillar according to the width of the pillar. It is judged that the results derived from this study can be used as a guideline to secure the safety of the room when the actual design is performed in consideration of the ground conditions and room width.

• Analytical Science and Technology
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• v.28 no.3
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• pp.160-167
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• 2015

This study aims to develop a new analytical method to detect zinc pyrithione, the ingredient of cosmetics appointed as restricted ingredients and used as preservatives.. The analytical method was based on data gathered from the relevant literature. Information about the amounts of these ingredients was researched in order to select the base-matrix materials used to validate the analytical method. After selecting and preparing the base-matrix materials, the analytical method was validated by method validation procedures. The analytical method was verified first by inter-laboratory validation and then through analyzing the cosmetics sold in the market. Based on the results of this study, guidelines are proposed for the analysis of restricted ingredients in cosmetics, which will provide a method to test the cosmetics circulating in the Korean market. The use of the proposed guidelines will increase the quality of the cosmetics as well as the safety of human health, which will enhance the competitiveness of the Korean cosmetics industry and lead to an increase in the exportation of cosmetics.

• Journal of Acupuncture Research
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• v.26 no.6
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• pp.101-110
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• 2009

Objectives : We developed and proposed a guideline for safety and performance assessment of electric cupping apparatus(Class 2 medical device). Methods : We drafted the guideline for safety and performance assessment of electric cupping apparatus by referring the existing standards and guideline, based on online questionnaire for Korean medical doctors and measurement data from commercially available products. Physical dimension of cups and inner vacuum pressure were acquired for the measurement in order to achieve the purposes. Results : This guideline only can be applied to electric cupping apparatus for enhancing blood circulation by employing negative pressure generated by electricity. Seven items of appearance and label, operation test of pump, variation test of input electricity, vacuum level test, vacuum sustain test, cup-size dependent test, noise level test are suggested for evaluation subjects and methods required for electric cupping devices. Requirements for the design and development of electric cupping devices are suggested: vacuum level indicator, vacuum generation rate, pressure control, valve detachment stability, cup comparability, safety measure, surge protection, user friendliness, instruction for use (IFU). Conclusions : We proposed a guideline for safety and performance assessment of electric cupping apparatus to improve the quality of relating products and aid the commercialization of them, by aiming higher industrial competitiveness of the medical device sectors in Korea. Discussion with related institutes such as industry, academy and government is further required. Public hearings also need to be held prior to the establishment of a final guideline and standard.