• Title/Summary/Keyword: 실리카 나노분말

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Effect of Water Volume and Relaxation Time in the Design of Nano Shock Absorbing Damper Using Silica Particle (실리카 분말을 이용한 나노 충격완화 장치의 설계에서 작동 유체 영향과 복원 시간에 대한 연구)

  • 문병영;김병수
    • Journal of the Korean Ceramic Society
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    • v.40 no.3
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    • pp.286-292
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    • 2003
  • In this study, new shock absorbing system was proposed using silica gel particles according to the nano-technology. For the design and real application of the proposed damper, an experimental investigations are carried out using colloidal damper, which is statically loaded. The porous matrix is composed from silica gel(labyrinth architecture), coated by organo-silicones substances, in order to achieve a hydrophobic surface. Water is considered as associated lyophobic liquid. Reversible colloidal damper static test rig and the measuring technique of the static hysteresis were described. Iufluence of the water volume and particle diameters upon the reversible colloidal damper hysteresis was investigated. Also, influence of the relaxation time on the hysteresis of the damper was investigated. As a result, the proposed new shock absorbing damper is proved as an effective one, which can be replaced for the conventional hydraulic damper.

Silica Coating of Nanosized CoFe2O4 Particles by Micro-emulsion Method (마이크로에멀젼법을 이용한 나노 CoFe2O4 분말의 실리카 코팅)

  • Kim, Yoo-Jin;Yu, Ri;Park, Eun-Young;Pee, Jae-Hwan;Choi, Eui-Seok
    • Journal of the Korean Ceramic Society
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    • v.46 no.1
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    • pp.69-73
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    • 2009
  • We report the preparation of nanocrystalline cobalt ferrite, $CoFe_2O_4$ particles and their surface coating with silica layers using micro emulsion method. The cobalt ferrite nanoparticles with the size 7nm are firstly prepared by thermal decomposition method. Hydrophobic nanoparticles were coated with silica using micro-emulsion method with surfactant, $NH_4OH$, and tetraethylorthosilicate (TEOS). Monodispersed and spherical silica coated cobalt ferrite nanoparticles have average particle diameter of 38 nm and narrow sized distribution.

Fabrication and Characterization of Silica Coated Fe3O4 Nanoparticles in Reverse Micro Emulsion (마이크로에멀젼법을 이용하여 실리카 코팅된 나노 Fe3O4 분말의 합성과 분석연구)

  • Yu, Ri;Kim, Yoo-Jin;Pee, Jae-Hwan;Hwang, Kwang-Taek;Yang, Hee-Seung;Kim, Kyung-Ja
    • Journal of the Korean Ceramic Society
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    • v.47 no.2
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    • pp.113-116
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    • 2010
  • The silica coated $Fe_3O_4$ nanoparticles have been synthesized using a micro-emulsion method. The $Fe_3O_4$ nanoparticles with the sizes 6 nm in diameter were synthesized by thermal decomposition method. Hydrophobic $Fe_3O_4$ nanoparticles were coated silica using surfactant and tetraethyl orthosilicated (TEOS) as a $SiO_2$ precursor. Shell thickness of silica coated $Fe_3O_4$ can be controlled (11~20 nm) through our synthetic conditions. The $Fe_3O_4$ and silica coated $Fe_3O_4$ nano powders were characterized by transmission electron microscopy (TEM), x-ray diffraction (XRD) and vortex magnetic separation (VMS).

Effect of Heat-Treatment on the Optical Properties of Self-Assembled SiO2 Photonic Crystals (자기조립을 통해 형성된 실리카 광자결정의 광특성에 미치는 열처리 효과)

  • O, Yong-Taeg;Kim, Myung-Soon;Shin, Dong-Chan
    • Journal of the Korean Ceramic Society
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    • v.42 no.2 s.273
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    • pp.127-131
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    • 2005
  • We examined the effect of low temperature heat-treatment on the optical properties of the photonic crystals self-assembled using a monodispersed spherical $SiO_2$ nanoparticle. When the heat treatment temperature increased, the reflectance peak, which is induced by the photonic band gap, moved to a shorter wavelength direction, and the peak intensity of Fabry-Perot fringes also increased. The highest reflectance peak intensity was obtained in the sample heat-treated at $250\~300^{\circ}C$. The heat-treatment reduced the average particle size and the quantity of defects, and increased the packing density of the photonic crystal.

Surface Modification Silica Nanoparticles by Aerosol Self Assembly (에어로졸 자기조립에 의한 실리카 나노분말의 표면개질)

  • Kil, Dae-Sup;Jang, Hee-Dong;Chang, Han-Kwon;Cho, Kuk;Kim, Sun-Kyung;Oh, Kyoung-Joon;Choi, Jin-Hoon
    • Korean Journal of Materials Research
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    • v.20 no.2
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    • pp.78-81
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    • 2010
  • Surface modification of silica nanoparticles was investigated using an aerosol self assembly. Stearic acid was used as surface treating agent. A two-fluid jet nozzle was employed to generate an aerosol of the colloidal suspension, which contained 20 nm of silica nanoparticles, surface modifier, and ethyl alcohol. Powder properties such as morphology, specific surface area and pore size distribution were analyzed by SEM, BET and BJH methods, respectively. Surface properties of the silica power were analyzed by FT-IR. The OH bond of the $SiO_2$ surface was converted to a C-H bond. It was revealed that the hydrophilic surface changed to a hydrophobic one due to the aerosol self assembly. Morphology of the surface treated powder was nanostructured with lots of pores having an average diameter of around $2\;{\mu}m$. Depending on the stearic acid concentration (0.25 to 1.0 wt%), the pore size distribution of the particles and the degree of hydrophobicity ranged from 1.5 nm to 180 nm and 29.6% to 50.2%, respectively.

A Fundamental Study on Nano-cement by Chemical Synthesis (화학적 방법에 의한 나노시멘트 개발에 관한 기초 연구)

  • Jo, Byung-Wan;Kang, Seok-Won;Yoon, Kwang-Won;Choi, Ji-Sun
    • Journal of the Korea Concrete Institute
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    • v.21 no.6
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    • pp.713-718
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    • 2009
  • Advanced industries-IT, BT, NT and ET are rapidly developing in 21 century. And the cement industry is becoming the principal factor in air pollution because of the creation of $CO_2$ during manufacturing. Also, the cement industry will be faced with a crisis due to the exhaustion of natural resources. In this study, nano cement by Bottom-up method of a chemical synthesis was developed. The generation of $CO_2$ during the plasticization process of cement manufacturing was avoided. The purpose was to produce building materials that have both high strength and durability as the high value-added growth engine industry of the 21 century. The nano cement was developed using hydrothermal synthesis. This is a method of mixing after ripening, by manufacturing the high density gel and low gel, which does not require special test equipment or pressure conditions to produce. Particle size, SEM, EDX, and porosity tests were conducted. This study investigated the compressive strength of concrete with various compositions. Specimens were tested for compressive strength at 3, 7, 14 and 28 days. The medium-sized (50% by weight) cement particles created by chemical synthesis were less than 168 nm. The compressive strength of the mortar prepared using this cement was 53.9 MPa. But it was judged that succeeding study will be necessary for development of nano building materials with high ability and economical analysis.