• Proceedings of the KIEE Conference
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• 2003.07c
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• pp.1987-1989
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• 2003

3차원 형상을 측정하는 측정법으로는 접촉식과 비접촉식이 있는데 최근에는 물체의 표면을 손상 시키지 않으면서 물체의 변형 상태 등을 정밀하게 측정할 수 있는 비접촉식 측정법이 주로 사용되어 지면서 변형, 진동, 결함 등의 다양한 측정 분야에 찰용되고 있다. 이는 광학 간섭의 하나인 Twyman-Green 간섭계를 이용하여 간섭 무의 패턴을 PZT Controller로 위상 이동하여 CCD 카메라로 물체의 영상을 얻어 위상 지도를 추출, 이미지를 분석하여 3차원 물체를 해석하고자 한다. 하지만 이미지 측정시 미세 진동 및 조명 등에 의한 노이즈가 발생하게 되어 물체의 정확한 정보를 얻기가 어려워 노이즈 제거를 위한 이미지 처리 알고리즘 개발과 Unwrapping 처리, 위상이동 알고리즘 개발 등을 통하여 좀더 정확한 정보를 얻고자 한다.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2004.07b
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• pp.1058-1061
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• 2004

미세 소자를 관측, 가공 및 분석하기 위해 사용되는 기존 광학현미경은 빛으로 물체를 관측하므로 대물렌즈 (Object lens)에서의 회절한계 때문에 분해능의 있으므로 매우 뽀족한 탐침(Probe)을 시료의 표면에 근접시킨 후 표면을 주사하여 이미지를 얻는 방법이 개발되어 최근에는 Optical Fiber를 이용하여 fiber 끝단을 nano-scale 정도로 첨예화시키는 기술이 개발되었다. 이러한 광섬유 탐침은 구경의 직경이 작을수록 높은 분해능을 얻을 수 있으므로 광섬유 탐침의 제작 공정 확립은 매우 중요하다. 그 중에서 대표적인 방법이 $CO_2$ 레이저를 이용하여 가열한 후 인장 하는 방법 (Heating and Pulling)이 있다. 그래서 본 연구에서는 $CO_2$ 레이저를 이용하여 100nm 정도의 팁 반경을 갖는 뽀족한 탐침을 제작하고자 한다.

• Korean Chemical Engineering Research
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• v.52 no.2
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• pp.266-271
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• 2014

The effects of antioxidants on the properties of Polycarbonate/Acrylonitrile-Butadiene-Styrene(PC/ABS) blends were studied for the functions of the screw speed and loaded duration of high shear rate processing in order to investigate the degradation for PC/ABS blends. Tris-(2,4-di-tert-butyl-phenyl phosphate) (A1) and Bis(2,4-dicumylphenyl) pentaerythritol diphosphite (A3) as phosphite antioxidants and Octadecyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate (A2) as a phenolic antioxidant are used. The thermal properties were detected by TGA and severely decreased, after the processing. The stress-induced and thermal degradation for PC/ABS blends with the antioxidant A3 was retarded better than the others. By using UTM, the mechanical properties also showed individually decreased according to the antioxidants, after the processing, especially, the elongations showed considerable decline behaviors, while the tensile strengths of PC/ABS blends changed very little. For example, in the operating conditions of 1000rpm of screw speed and 20 seconds of loaded period, the elongations decreased from 148% before the processing, to 91.6% with the A1, to 63% with the A2 and to 131% with the A3 after the processing, respectively. In order to get the morphological properties, the size distributions of the dispersed phases for PC/ABS were investigated by SEM analysis and tended to decrease, as the screw speed and loaded period of the processing increased. Therefore, we confirmed that the antioxidant A3 was the best of all of three to inhibit the stress-induced degradation of PC/ABS blends during the high shear rate processing.

• Composites Research
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• v.30 no.2
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• pp.138-144
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• 2017

Damage sensing of polymer composite films consisting of poly(dicyclopentadiene) p-DCPD and carbon nanotube (CNT) was studied experimentally. Only up to 1st ring-opening polymerization occurred with the addition of CNT, which made the modified film electrically conductive, while interfering with polymerization. The interfacial adhesion of composite films with varying CNT concentration was evaluated by measuring the wettability using the static contact angle method. 0.5 wt% CNT/p-DCPD was determined to be the optimal condition via electrical dispersion method and tensile test. Dynamic fatigue test was conducted to evaluate the durability of the films by measuring the change in electrical resistance. For the initial three cycles, the change in electrical resistance pattern was similar to the tensile stress-strain curve. The CNT/p-DCPD film was attached to an epoxy matrix to demonstrate its utilization as a sensor for fracture behavior. At the onset of epoxy fracture, electrical resistance showed a drastic increase, which indicated adhesive fracture between sensor and matrix. It leads to prediction of crack and fracture of matrix.

• Elastomers and Composites
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• v.34 no.3
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• pp.199-211
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• 1999

In this work, the effects of the addition of epoxy on the properties of PVC-sol sealants were investigated. PVC-sol was plasticized with dioctyl phthalates(DOP). Two kinds of epoxy resins having different epoxy equivalent weight (E.E.W.) were used. It was found that the properties of the PVC-sol sealants were significantly affected by the contents and types of the added epoxy resins. The viscosity behaviors of the epoxy-modified sealants, in the case of epoxy A addition, the viscosity was decreased with increasing the epoxy contents, but In the case of $CaCO_3$ addition, the viscosity was increased with increasing the $CaCO_3$ contents. The viscosity of epoxy modified sealants aged at $45^{\circ}C$ waterbath was decreased with increasing epoxy contents, since the epoxy acted on the sealants as a stabilizer. The thermal stability of the PVC-sol sealants was slightly improved by adding epoxy. The tensile strength and elongation of sealants modified with epoxy A(two functionalities of epoxy) were increased with increasing the epoxy contents up to a certain epoxy contents but was decreased with further increasing the epoxy contents. In the case of $CaCO_3$ addition, the tensile strength of sealants were decreased with increasing the $CaCO_3$ contents. In view of the electrical properties, such as tan ${\delta}$($0.1{\pm}0.04$) and ${\epsilon}_r$($0.5{\pm}0.04$), it was found that the epoxy modified sealants were as good as insulators.

• Polymer(Korea)
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• v.38 no.4
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• pp.471-476
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• 2014

Polycarbonate (PC) and acrylonitrile-butadiene-styrene (ABS) blends were prepared using a high shear extruder to investigate their thermal decomposition and mechanical properties with shear rate and shear time. In this experiment, high shear rate, from 1000 to 3000 rpm, in blending process was applied for 10 to 40 sec, respectively. At high shear rate over than 2000 rpm, the initial decomposition temperature was dropped significantly compared to a compounded sample because of thermal decomposition of the blend by high shear. Consequently, high shear processing gave an important effect on the mechanical and thermal properties of the PC/ABS blend. In particular, elongation of the blend decreased significantly with shear rate.

• The Journal of the Institute of Internet, Broadcasting and Communication
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• v.12 no.5
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• pp.11-16
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• 2012

Opportunistic transmit cooperative relaying (OTR) system has been interested for its ability to mitigate the fading in wireless channel without multiple antennas in a small terminal. In OTR system, only the relays that the received Signal-to-noise ratio (SNR) from a source is greater than the threshold transmit to the destination. However, the receiving branches of a destination in a realistic system is fixed, the excess number of signals from the transmit relays does not improve the system performance and consequently increases power consumption. In this paper, we adopt Double Opportunistic Transmit (DOT) cooperative diversity system which controls the average number of transmit relays. Although the average number of the transmit relays can be controlled by adjusting the two thresholds in DOT system, the instantaneous number of transmit relays is varying in fading channel. Thus we propose Maximal Ratio Combining (MRC) or Generalized Selection Combining (GSC) according to the number of the signals from relays at the destination. The outage probability of the proposed system is derived in closed form. The analytical results show that the system performance is improved with the number of the branches. Also it is noticed that when the number of the branches is fixed, the outage probability decreases with the increase of the average SNR of S-R path and R-D path.

• Polymer(Korea)
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• v.26 no.2
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• pp.218-226
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• 2002

For the preparation of high resilience polyurethane (PU) foams with polyether type cell openers which have different ethylene oxide (EO) content, molecular weight and chain structure, the influences of tell opener structure on the kinetics, rheology, structural stability, open cell content and mechanical properties of the obtained foam were investigated. It was observed that urea formation reaction was delayed with the increase of EO content and incorporation of ester linkage in cell opener molecule and was relatively independent on the molecular weight. With the rheological studies, the decreases of viscosity and storage modulus were confirmed for the increase of EO content and molecular weight, so that the resulted foam had low structural stability and high open cell content. The cell opener having ester linkage in molecule exhibited the lowest values of viscosity and storage modulus and the obtained foam has high open cell content. However, the structural stability increased due to the larger intermolecular interaction of ester linkage. The hardness, tensile strength, tear strength and elongation of foam were deteriorated with increase of EO content and molecular weight of tell opener. On the other hand, the cell opener having ester linkage in molecule improved the values of tensile strength, tear strength and elongation.

• Korean Journal of Food Science and Technology
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• v.46 no.2
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• pp.135-142
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• 2014

Physicochemical, pasting, and digestion properties of sweet potato starches from 11 Korean cultivars were investigated. Starch granules were variably oval, round, polygonal, spherical, and bell-shaped, and of 10.2-15.3 ${\mu}m$ in mean particle diameter. Amylose contents varied from 12.3 to 17.4%. A similar chain length distribution of amylopectin was found in each of the cultivars. The portion of $B_3$ correlated with the degree of amylose leaching. Thermal properties determined by differential scanning calorimetry showed high values of gelatinization temperatures in Shinyulmi and Jeungmi starches, but a relatively low value in Daeyumi starch. All starches exhibited a Ca-type diffraction pattern. Differing patterns were observed in swelling factors, depending on temperature. The contents of rapidly digestible starch, slowly digestible starch, and resistant starch ranged from 9.6-17.4, 31.4-45.6, and 35.7-62.8%, respectively. In Rapid Visco Analyser profiles, differences were observed in pasting parameters such as pasting temperature, peak viscosity, final viscosity, and breakdown.

• Journal of the Korean Applied Science and Technology
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• v.33 no.4
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• pp.802-812
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• 2016

Silicone foam is very useful as flame resistant material for many industrial areas such as high performance gasketing, thermal shielding, vibration mounts, and press pads. A silicone foam was prepared through simultaneous crosslinking and foaming by hydrogen condensation reaction of a vinyl-containing polysiloxane (V-silicone) and a hydroxyl-containing polysiloxane (OH-silicone) with hydride containing polysiloxane (H-silicone) in the presence of platinum catalyst and imorganic filler at room temperature. This is more convenient process for silicone foam manufacturing than the conventional separated crosslinking and foaming systems. Funtionalized silicones we used in this experiment were consisted with a V-silicone containing 1,0 meq/g of vinyl groups and a viscosity of 20 Pa-s, an OH-silicone with 0.4 meq/g of hydroxyl groups and a viscosity from 50 Pa-s, and an H-silicone containing 7.5 meq/g of hydride groups and a viscosity of 0.06 Pa.s. The effects of compositions of functionalized silicones and additives, such as catalyst and filler on the structure and mechanical properties of silicone foam were studied. 0.5 wt% of Pt catalyst was enough to accelerate the foaming rate of silicone resins. The addition of OH-silicone with lower viscosity accelerates the initial foaming rate and decreases the foam density, but the addition of V-silicone with lower viscosity reduces the tensile strength as well as the elongation. The final foam density, tensile strength, and elogation of silicone foam prepared under the SF-3 condition increase maximum to $0.58g/cm^3$, $3,51kg_f/cm^2$, and 176 %, repectively. We found out the filler alumina also played an important role to improve the mechanical properties of silicone foams in our foaming system.