• Proceedings of the KSEG Conference
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• 2003.04a
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• pp.109-116
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• 2003

본 기술사례는 과학기술부가 주도하는 자연재해방재기술개발 국가중점연구사업 중 기상청 주관의 기상지진기술개발사업의 한반도 지각속도 구조연구 과제 중 서산지역과 포항지역을 연결하는 200km 측선에서 2차원 지각구조를 밝히기 위한 지각규모 굴절파탐사의 지진동 source 제공을 위해 발파로 실시하였다. 본 연구를 위하여 국내에서는 거의 실행해 본 경우가 없는 지발당 장약량이 500~1000kg의 발파를 실시하였다. 200개의 계측지점에 지진동이 전달될 수 있도록 충분한 폭속을 가진 폭약과 외부의 충격과 우수한 기폭력, 시차가 정확한 이중비전기뇌관을 특수 제작하여 사용하였다. 시추공내로 유출되는 물에 의한 사압을 방지하기 위하여 폭약은 철관용기를 제작하여 벌크 형태로 장약을 하여 발파를 하였다. 발파전 용기 밀폐 시험 및 용기제작 후 기폭실험, 수압작용으로 인한 폭약 및 뇌관에 미치는 영향 등을 실험을 통하여 사전 파악을 하였다. 또한 실제 발파 중 진동치를 측정한 결과 보안물건에 대한 진동치값은 미광무국식(USBM)을 이용하여 예측한 진동치보다 평균 180% 정도 높게 나타났다.

• Journal of the Korean Ceramic Society
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• v.38 no.1
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• pp.68-73
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• 2001

Active belite cement clinker 합성을 위하여 안정제로 borax (3 wt%)를 사용하였으며, 1300, 1350, 140$0^{\circ}C$에서 소성하고, 각각의 소성온도에서 아세톤 급냉, 공냉, 로냉의 3가지 방법으로 냉각속도를 달리하여 합성하였다. 클링커의 특성분석은 TG-DTA, XRD, FT-IR, SEM-EDS로 조사 분석하였으며, free-CaO 함량은 KSL 5120의 ethylene glycol법으로 정량하였다. Borax(3 wt%)를 첨가한 시료의 시차열분석에서 ${\gamma}$상으로의 전이는 관찰되지 않았으며, 각각의 소성온도와 냉각속도에 따른 free-CaO 분석에서 0.07~0.14%의 범위로 낮게 나타났으며, borax가 첨가되지 않은 시료는 140$0^{\circ}C$에서 소성하고 급냉시켰지만 ${\gamma}$상으로 전이되어 dusting 현상을 나타내었다. Borax(3 wt%) 첨가된 시료의 SEM 미세구조는 140$0^{\circ}C$에서 소성하고 급냉시켰지만 ${\gamma}$상으로 전이되어 dusting 현상을 나타내었다. Borax(3 wt%) 첨가된 시료의 SEM 미세구조는 140$0^{\circ}C$에서 소성된 모든 시료와 135$0^{\circ}C$에서 소성하고 급냉과 공냉시킨 시료는 type I belite, type III belite($\alpha$상) 구조를 나타낸다. 135$0^{\circ}C$에서 소성하고 로냉한 시료와 130$0^{\circ}C$에서 소성된 모든 시료는 type II belite($\beta$상) 구조를 나타내었다.

• Journal of the Korean Chemical Society
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• v.39 no.8
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• pp.627-634
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• 1995

Layered double hydroxides ($Mg-Al-CO_3$ systems, LDH), which are hydrotalcite-like anionic clay minerals, having different $Mg^{2+}\;to\;Al^{3+}$ ratio were synthesized by coprecipitation method. The subsequent products were characterized by the following methods; elemental analysis, X-ray powder diffraction, thermal analysis (DSC and TGA), FT-IR and $^{27}$Al-MAS NMR. X-ray powder patterns showed that the products formed were layered structure materials. Two heat absorption peaks were observed around 20 ∼280$^{\circ}C$ (surface water and interlayer water) and 280∼500$^{\circ}C$ (water from lattice hydroxide and carbon dioxide from interlayer carbonate) in DSC diagrams, and they were quantitatively analyzed by TGA diagrams (in case LDH4 16.2% and 28.6% respectively). FT-IR spectra indicate that the interlayer carbonate ions occupied symmetrical sites between two adjacent layers in a parallel direction. $^{27}$Al-MAS NMR spectra show only single resonance (8.6 ppm) of the octahedrally coordinated aluminum similar magnesium. When LDH4 was calcined at 560$^{\circ}C$ for 3 hours in air, its layered structure was destroyed giving a mixed metal oxide. However it readily became rehydrated in aqueous chromate solution to its original structure.

• Journal of the Korea institute for structural maintenance and inspection
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• v.17 no.2
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• pp.94-100
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• 2013

In this paper, Machinery analysis was conducted, in order to predict highest exposure temperatures and the analyze fire damage in the case of fire on reinforced concrete structure. After analyzing differential thermal of reference materials in accordance with temperature of concrete reference core specimen, it turned out that powerful endothermic peak came resulting from evaporation of capillary water and get water untill $200^{\circ}C$, another endothermic peak came resulting from decomposition of calcium hydroxide at $520^{\circ}C$, and then mass of reference materials remarkably decreased due to endothermic reaction. Another powerful endothermic reaction came after decomposition of calcite at $720^{\circ}C$. After analyzing X-ray diffraction of reference materials in accordance with temperature of concrete reference core specimen, it turned out that calcium hydroxide existed until the temperature of $400^{\circ}C$, but CH almost disappeared and CaO appeared from $600^{\circ}C$. The production increased in proportion to the temperature. This is because that calcium hydroxide and calcite are decomposed and CaO is produced when the temperature of concrete increases with fire. It is estimated that calcium hydroxide and calcite are utterly decomposed and peak disappears, and peak of CaO is remarkably formed instead, at the temperature of $700-800^{\circ}C$.

• The Korean Journal of Financial Management
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• v.22 no.2
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• pp.1-41
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• 2005

In the literature, much research has been focused on the relationships between financial policies and corporate valuation, including the effects that internal equity and capital structure have on corporate value, as well as how capital structures, investments and dividends relate to one another. However, comprehensive studies considering three facets of financial policies, namely capital structures, investments, and internal equity altogether, are scant. This study follows 361 companies listed on the Korean Stock Exchange, excluding financial institutions, from 1996 to 2002. Using 3SLS methods, an empirical analysis was conducted of the relationships among capital structures, investments, dividends, and internal equity and the results are summarized. Capital structures were found to be negatively related with investments, while investments were mainly related to dividends. Dividends were positively related with internal equity, simultaneously affecting capital structures. We were not able to find any clear evidence of a direct relationship between internal equity and capital structures; however they seemed to be indirectly related. Thus, there seems to be mutual relationships between financial policies and internal equity.

• Journal of the Korean Applied Science and Technology
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• v.25 no.3
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• pp.313-321
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• 2008

오래전부터, 많은 여성들은 자신들의 젊음을 연장하고, 외모를 더 아름답게 가꾸고, 이를 죽을 때까지 유지하는 것을 바래왔다. 이에 의사와 약사들뿐만 아니라, 많은 화장품 연구자들도 노화와 관련된 기술개발에 총력을 기울여 왔다. 따라서, 이들 연구자들은 노화방지를 위한 새로운 원료를 찾고, 이를 안정화하고, 피부로 전달하는 기술개발에 항상 관심을 쏟아왔다. 뛰어난 노화방지 화장품 개발을 위해서, Ubiquinone의 일종인 ldebenone에 대해 연구하였고, 이를 비수계 피부유사막 기술을 가지고 캡슐화하고 약물전달하는 연구를 진행하였다. 먼저, 편광현미경(PM, Polarized Microscope), X-선 회절분석(XRD, X-ray Diffractions) 및 시차주사열량계 (DSC, Differential Scanning Calorimetry)를 이용하여 Idebenone을 담지한 피부유사막 액정을 비수계 조건에서 구조 및 열적특성을 조사하였다. 그 결과 비수계 조건에서도 규칙적으로 패킹(Packing)된 지질이중층(Lipid bilayer)과 용매의 연속층으로 이루어진 고밀집된 라멜라(Lamella) 구조의 형성유무와 이때의 상거동을 확인할 수 있었다. 결론적으로 높은 극성도로인해 물분자와 접촉하면 불안정해지는 경향이 있는 Idebenone을 비수계 조건에서 각질층(SC, Stratum Corneum)과 구조 및 조성이 유사한 피부유사막을 디자인하여 안정하게 캡슐화 하였다. 이를 적용한 화장품은 모든 보관조건에서 유화입자의 안정성을 유지함을 확인하였고, Idebenone의 활성역가 또한 $40^{\circ}C$에서 6개월 동안 약 90%이상을 유지하는 우수한 결과를 나타냈다.

• Applied Chemistry for Engineering
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• v.5 no.2
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• pp.361-372
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• 1994

Vanadium containing MFI type zeolites have been prepared hydrothermally or by the impregnation method with $NH_4VO_3$ solution after dealumination of HZSM-5. Incorporation of vanadium into the framework of zeolite has been demonstrated by XRD, DTA, FT-IR and ESR analyses. Upon $NH_4VO_3$ impregnation and calcination of dealuminated zeolite, vanadium substitution into the framework could be performed like a hydrothermally synthesized zeolite. Vanadium in zeolite is able to pass redox cycles at high temperatures, and it is shown that vanadium is probably fixed and atomically dispersed in the structure of zeolite. The catalytic benzene hydroxylation, hexanes and alcohols oxidation were used for evaluating the properties of vanadium incorporated MFI zeolite.

• Explosives and Blasting
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• v.31 no.1
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• pp.41-48
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• 2013

Progressive collapse is generally defined as a local failure of structural members occurring due to abnormal load which results in the partial collapse or total collapse of a structure. Unlike progressive collapse, explosive demolition is a method of inducing the total collapse of structure by removing all or portion of structural members. In explosive demolition the partial collapse of the structural members can be controlled at appropriate time intervals by blasting, to induce the progressive collapse of the structure and control the collapse behavior. In this study, a nonlinear dynamic analysis was carried out in order to apply the progressive collapse process to explosive demolition design of the RC structure. The occurrence of progressive collapse of analytical models was examined according to the number of floors, the removed column height and span length. For models that resisted progressive collapse, progressive collapse resisting capacity was evaluated.

• Journal of Broadcast Engineering
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• v.19 no.2
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• pp.205-214
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• 2014

Minimization of visual fatigue is important for production of high quality stereoscopic 3D contents. Vertical disparity of stereo images occurred during contents production is considered as the main factor of visual fatigue. To ensure correct stereoscopy vertical disparity needs to be eliminated. In this paper, a method for automated image alignment was proposed for Stereoscopic 3D contents generation and post-processing steps. The proposed method consists of two parts: rectification for image alignment and camera motion detection. The proposed method showed that its rectification performance was the most superior among the existing methods tested and that camera motion detection had a success rate of 98.35%. Through these evaluations, we confirmed that the proposed method can be effectively applied to 3D contents production.

• Composites Research
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• v.24 no.4
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• pp.5-10
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• 2011

As environmental pollution getting worse, biodegradable materials have been drawn more attention than ever. In this study, polylactic acid (PLA)/carbon nanotubc (CNT) nanocomposites were manufactured via extrusion molding and injection molding, In order to change the crystallinity, annealing treatment was done for different time span, Crystallization kinetics of PLA was analyzed by differential scanning calorimeter (DSC), and it was confirmed that a proper amount of CNT can increase the crystallization rate of PLA. In addition, the presence of CNT significantly accelerates the hydrolytic degradation rate of PLA, however, it decreases with the increase of crystallinity. The reason is that degradation may occur in the PLA/CNT interface easily, and the molecular structure of the composite becomes dense with the increase of crystallinity.