• Title/Summary/Keyword: 시간-온도곡선

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Studies on the Quality Control of Insulin Radioimnunoassay Kit (I) -Pitfalls in Radioimmunoassay of Insulin-

  • Lee, Kyung-Hee;Awh, Ok-Doo;Kim, Jae-Rok
    • Nuclear Engineering and Technology
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    • v.10 no.4
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    • pp.223-229
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    • 1978
  • A typical abnormal standard dose response curve of nearly convex form. often encountered in insulin radioimmunoassay (IRIA) has been analyzed by varying incubation conditions. The cause of such abnormality has been turned out to be the results of an incomplete equilibrium between the two reactants. By careful control of the temperature of serum sample an immediate cause of sharp deviation of B/F value of tile sample tube from the measurable range in the standard curve has also been investigated. The two main troubles have been proven to be stemed from incubation conditions. Incubation at 4$^{\circ}C$ for 48 hrs is emphasized for IRIA.

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Variation of Asymmetric Hysteresis Loops with Chemical Composition of Amorphous Ferromagnetic Alloys (비정질 자성 합금의 조성에 따른 비대칭 자기 이력 곡선의 변화)

  • 신경호;민성혜;이장로
    • Journal of the Korean Magnetics Society
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    • v.5 no.4
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    • pp.261-268
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    • 1995
  • In order to investigate the origin of the asymmetric magnetization reversal effect, we studied the variation of magnetic hysteresis loops with the alloy composition in amorphous ferromagnetic alloy ribbons of ${(Fe_{1-x}Co_{x})}_{75}Si_{10}B_{15}$ system annealed at $380^{\circ}C$ for 16 hours in a zero field condition. The asymmetric magnetization reversal effect developed more strongly in amorphous ribbons having two metallic components than in ribbons having a single metallic component. The effect developed more strongly in ribbons showing a smaller value of the saturation mag¬netostriction. The development of the asymmetric magnetization reversal effect was affected by the ratio of two metallic components as well as the magnitude of the saturation magnetostriction.

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Effect of Temperature on Formation of Polymer in Oxidation of Methyl Linoleate (Methyl Linoleate 산화중 중합체 형성에 미치는 온도의 영향)

  • Kim, In-Hwan;Kim, Chul-Jin;Kim, Dong-Hoon
    • Korean Journal of Food Science and Technology
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    • v.28 no.3
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    • pp.446-450
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    • 1996
  • To investigate the effect of heating conditions on the polymerization of methyl linoleate, the esters were heated at $60^{\circ}C,\;90^{\circ}C,\;120^{\circ}C$ and $150^{\circ}C$, respectively, with sparging oxygen for different periods of time. On the basis of the peroxide curve obtained at each of the four temperatures, four heating times were chosen for the analysis of the polymers and total oxidation products. Significant linear relationships were found between polymer contents and total oxidation product contents. The contents of polymers and their linkage types were analyzed by High Performance Size Exclusion Chromatography. The polymers formed at four temperatures were qualitatively identified as dimers. The dimers with peroxide linkages were detected from methyl linoleate oxidized at $60^{\circ}C\;and\;90^{\circ}C$ but they were not detected from methyl linoleate oxidized at $120^{\circ}C\;and\;150^{\circ}C$. Therefore, all dimers formed at $120^{\circ}C\;and\;150^{\circ}C$ seemed to be the ones with ether linkage or carbon to carbon linkage. The degradation rate of the dimers with peroxide linkages at $90^{\circ}C$ was faster than at $60^{\circ}C$.

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Browning and Sorption Characteristics of Dried Garlic Flakes with Relative Humidity and Storage Temperature (상대습도와 저장온도에 따른 건조마늘 플레이크의 갈변 및 흡습특성)

  • Kim, Hyun-Ku;Jo, Kil-Suk;Kang, Tong-Sam;Shin, Hyo-Sun
    • Korean Journal of Food Science and Technology
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    • v.19 no.2
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    • pp.176-180
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    • 1987
  • The sorption characteristics of dried garlic flakes stored at various relative humidity and storage temperature were studied. At low relative humidity below RH 51%, the sorption equilibrium was easily attained, whereas at higher relative humidity above RH 67%, the flakes were browned by higher equilibrium moisture content. The flakes were browned at relative humidity above 67% at $20^{\circ}C$ and $35^{\circ}C$, above 84% at $5^{\circ}C$, respectively. The moisture contents of monolayer value for the flakes were ranging from 5.80% to 6.20% (DB) with varying temperatures. And the necessity of moisture-proof packaging material suggested for the long term storage of the flakes because the lower moisture content and storage temperature, the higher driving force of wetting. Regression equation for browning rate prediction with relative humidity and storage temperature of the flakes was determined.

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Heat resistant characterization of PMDA /4,4′-DBE polyimide of fabricated by vapor deposition polymerization (진공증착중합법에 의해 제조된 PMDA /4,4′-DDE 폴리이미드의 내열 특성)

  • 김형권;이은학;우호환;김종석;이덕출
    • Fire Science and Engineering
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    • v.10 no.3
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    • pp.3-9
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    • 1996
  • The Polyimide thin films based on PMDA and 4,$4^{\circ}$'-DDE were fabricated by VDPM, and their heat resistance characteristics were invastigated by TGA(Thermogravimetry Analyzer). It was found that deposition rate decreased with increasing substrate temperature and the thin films were not fabricated over the substrate temperature of $70^{\circ}$. $T_{TG}$ of weight loss temperature is $565^{\circ}$, $397^{\circ}$ and $210^{\circ}$ at the substrate temperature of $20^{\circ}$, $40^{\circ}$ and $70^{\circ}$, respectively. It is realized that the endurace temperature for 20,000 hour of thin films fabricated at $20^{\circ}$ and $40^{\circ}$ is $230^{\circ}$ and $200^{\circ}$, respectively.

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Heat Treatment of Dimension Lumber and Roundwood Used for Hanok Above $170^{\circ}C$

  • Kang, Ho-Yang
    • Journal of the Korea Furniture Society
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    • v.21 no.6
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    • pp.499-504
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    • 2010
  • Korean traditional buildings, Hanok, are mostly constructed with dimension lumbers and roundwoods. They are hardly kiln-dried without severe defects, thus usually air-dried from some months to an year. Dimension lumbers and roundwoods were heat-treated above $170^{\circ}C$ and drying defects were examined. Temperature rising curves of all dimension timbers used for this study show one or two deflection points. The time when the temperature at 37.5mm depth reached at $100^{\circ}C$ for spruce dimension heat-treated at $170^{\circ}C$ was twice longer than that heat-treated at $190^{\circ}C$. There were many internal checks in roundwoods of $148mm{\Phi}$, while surface checks were apparently closed at the end of heat treatment. The drying time of $300{\times}300mm$ dimensions with 65mm hole was shorter than that without hole by half.

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Numerical Study on the Phenomenon of Spontaneous Ignition of Coal Stockpile (저탄장 자연발화 현상의 수치해석적 연구)

  • Kim, Chul-Jin;Park, I-Sun;Sohn, Chae-Hoon
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.34 no.7
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    • pp.721-727
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    • 2010
  • The spontaneous ignition of coal stockpile causes serious safety and economic problems. Such spontaneous ignition occurs in coal stockpile when the rate of heat released by the oxidation of coal is greater than the rate of heat lost to the surroundings. In this study, a two-dimensional unsteady model is adopted for studying spontaneous ignition and the numerical results are compared with experimental results. The numerical results are in a good agreement with the experimental ones. Depending on the porosity, the internal maximum temperature, pressure, and oxygen mass fraction during spontaneous ignition are investigated. On the basis of the numerical results, the transient temperature variations for several shapes of coal stockpiles are analyzed. Further, the physical mechanisms of hot-spot formation and spontaneous ignition are analyzed.

The Effect of Drying Temperature and Time on Ginseng Tea Quality (건조온도(乾燥溫度) 및 시간(時間)이 인삼차(人蔘茶)의 품질(品質)에 미치는 영향(影響))

  • Park, Kil-Dong;Choi, Jin-Ho;Kim, Ok-Chan;Park, Taek-Kyu
    • Korean Journal of Food Science and Technology
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    • v.13 no.3
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    • pp.202-208
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    • 1981
  • Contents of moisture, sugar and saponin, and color intensity of red ginseng tea (RGT) prepared at various drying conditions were investigated for quality evaluation. 1. The sorption isotherm of RGT showed step-wise isotherm. 2. The moisture content of RGT dried at $80,\;90\;and\;105^{\circ}C$ reached at nearly constant values below 1.5% after 3 hours. 3. The HPLC patterns of sugar and saponin at various drying temperatures were quality same but different in quantity. 4. The color intensity of RGT was changed little below $80^{\circ}C$, but significantly above $90^{\circ}C$. 5. A significant relationship was found between decrease of sugar content and increase of color intensity above $80^{\circ}C$.

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Fire Retardant Treatment to the Plywood with Di-ammonium Phosphate [(NH4)2 HPO4](I) -Hot and Cold Soaking Treatment and Redrying of Treated Plywood by Hot Platen- (제2인산(第二燐酸) 암모늄에 의한 합판(合板)의 내화처리(耐火處理)(I) -온냉침지처리(温冷浸漬處理)와 열판(熱板)에 의한 처리합판(處理合板)의 재건조(再乾燥) -)

  • Lee, Phil Woo;Chung, Woo Yang
    • Journal of Korean Society of Forest Science
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    • v.60 no.1
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    • pp.30-36
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    • 1983
  • Plywood, the representative interior decorative or structural material, is so inflammable that it may cause big fires. Therefore, it is required inevitably to manufacture the "Fire retardant treated plywood", and it will be a study on the redrying of treated plywood that we ought to solve. This study was carried out to investigate the absorption of 20% $(NH_4)_2HPO_4$ solution into the soaked plywoods by hot/cold soaking for 3/3, 6/3, 9/3 and 12/3 hours and to study drying process with drying curves and drying rates by press-drying at the platen temperature of 130, 145, 160 and $175^{\circ}C$. Solution absorption of plywoods in hot/cold soaking method increased steadily with the prolonged soaking time, and water absorption is higher than DAP absorption, and then chemical retention (DAP) exceeded the minimum retention [$1.125kg/(30cm)^3$] even in the shortest soaking treatment. Drying curves of water-soaked plywoods inclined more steeply than those of DAP soaked plywoods. And the drying proceeded rapidly with the increase in platen temperature and terminated in 2.5-4 minutes at the temperature of 160 and $170^{\circ}C$. Drying rate also increased generally with the increase of platen temperature. So it was at $175^{\circ}C$ in DAP-soaking and at $160^{\circ}C$ in water-soaking when the drying rate became above 10%/min.

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Studies on Thermal Resistance of Selected Yeast Strain for Pasteurization of Solid Packed Peach (복숭아 Solid Pack 적정(適定) 살균조건(殺菌條件) 구명(究明)을 위(爲)한 선발(選拔) 효모(酵母)의 열저항성(熱抵抗性)에 관(關)한 연구(硏究))

  • Koo, Young-Jo;Lee, Dong-Sun;Shin, Dong-Hwa;Yu, Tae-Jong
    • Korean Journal of Food Science and Technology
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    • v.13 no.1
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    • pp.43-52
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    • 1981
  • A series of thermal destruction studies of the most heat resistant yeast strain No. 15 among 61 isolates were conducted in order to establish the optimum pasteurization condition of peach solid pack. The results obtained are summarized as follows: 1. A survival curve of the selected yeast strain No. 15 at $58^{\circ}C$ consisted of heat labile and heat stable fraction, showing broken curve. 2. The actively growing cell showed less recovery rate than 10 day rested cell after agitation-growing for 90 hr. For heating menstrua, peptone solution gave higher recovery rate than peach juice. For recovery medium, YM agar gave higher recovery rate than peach juice agar. The selected yeast was more resistant to heat at pH 4.0 than at pH 3.5 in both heating menstrua and recovery medium. 3. Z value of TDT curve of the selected yeast (heating : at pH 3.5 in peach juice. recovery: at pH 3.5 in peach juice agar) was $4.8^{\circ}C$. 4. The selected yeast No. 15 was identified as Torulopsis candida. 5. In the inoculated pack test of 4 oz can, it was concluded that the optimum P.U. 70/5 was 168 (center temp; $78.5^{\circ}C$, initial temp; $18^{\circ}C$, processing time; 18 min, initial yeast count; $1.0{\times}10^7$ per can).

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