• Journal of the Korean Chemical Society
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• 제41권3호
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• pp.150-156
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• 1997

A precursor of bulgecinine, (4S,5R)-1-acetyl-2-formyl-5-benzyloxymethyl-4-pyrrolidinol (15) has been synthesized from diacetone-D-glucose. Barton deoxygenation, conversion to an L-sugar and displacement with $N_3^-$ at C-5, and one-pot reductive cyclization at C-2 produced (6R)-6-Ο-benzyloxymethyl-(3R)-3-methoxy-2-oxa-5-azabicyclo-[2,2,1]heptane(13), a key intermediate for bulgecinine. N-Acetylation and acid hydrolysis of 13 furnished a precursor of bulgecinine, (2S,4S,5R)-pyrrolidinol derivative 15 and its (2R,4S,5R)-diastereomer.

• Analytical Science and Technology
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• 제5권4호
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• pp.409-415
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• 1992

Factor analysis was applied to X-ray diffraction patterns of the precursor of $BaTiO_3$. For that purpose, the precursor was synthesized in water solvent system using $Ba(NO_3)_2$ and $TiO(NO_3)_2$ as the starting materials and calcined at various temperatures. The samples obtained from the various calcined temperatures were analyzed by the X-ray diffractometer. Factor analysis was applied to the intensity data of the X-ray diffraction patterns. As the results, three factors were found and they were found to be $BaCO_3$, $BaTiO_3$ and $Ba_2TiO_4$. The relative concentrations of the three components were estimated during calcination.

• Journal of the Korean Chemical Society
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• 제39권2호
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• pp.103-110
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• 1995

Phenylthio substituted 14-membered lactone(23) which can serve as a precursor of a potential antitumor antibiotics (6), was successfully prepared. The synthesis of the lactone was accomplished via lactonization of the corresponding enediyne hydroxy acid (22). This hydroxy acid was derived from Pd(0)-catalyzed coupling reaction of methyl pentynoate and cis-1,2-dichloroethylene followed by another Pd(0)-catalyzed coupling reaction of the resulting methyl chloroenyne ester (20) and enyneol (17). The required enyne alcohol was successfully synthesized from vinyltin compound (12) in good overall yield.

• Journal of the Korean Chemical Society
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• 제50권1호
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• pp.60-64
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• 2006

has been synthesized using the layered organic-inorganic hybrids, Cu2(OH)3(CH3COO)·H2O as a precursor. Cubic Cu2O is synthesized by reducing Cu2(OH)3(CH3COO)·H2O with glucose in water at 75oC. The effects of precursor and glucose are investigated. The structure of Cu2(OH)3(CH3COO)·H2O plays an important role in preparing the uniform size of Cu2O.

• Proceedings of the Materials Research Society of Korea Conference
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• 한국재료학회 2005년도 춘계학술발표대회 및 제8회 신소재 심포지엄 논문개요집
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• pp.244-244
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• 2005

• Journal of the Korean Vacuum Society
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• 제5권2호
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• pp.133-138
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• 1996

Epitaxial cubic silicon carbide films have been deposited on carbonized Si(001) substrates using the single precursor 1, 3-disilabutane in the temperature range 900-$1000^{\circ}C$ under high vacuum conditions. The films grown were characterized by in situ RHEED, XPS, XRD, x-ray pole figure, SEM, and TEM. The results show that epitaxial cubic SiC films with smooth morphology and good crystallinity were formed in this temperature range. The single precursor 1, 3-disilabutane has been found suitable for the epitaxial growth of cubic SiC on Si(001) substrates.

• Proceedings of the Materials Research Society of Korea Conference
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• 한국재료학회 2005년도 춘계학술발표대회 및 제8회 신소재 심포지엄 논문개요집
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• pp.295-295
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• 2005

• Polymer Science and Technology
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• 제8권3호
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• pp.293-297
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• 1997

• Proceedings of the Korea Air Pollution Research Association Conference
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• 한국대기환경학회 2002년도 춘계학술대회 논문집
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• pp.183-184
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• 2002

도시와 산업의 발달 및 인구의 도시 집중화로 다양한 종류의 오염물질이 다량으로 대기 중으로 배출되는 통 환경오염이 날로 심각해지고 상황에서, 특히 악취(odor)와 VOCs(Volatile Organic Compounds) 물질이 사회의 중요한 환경오염 문제고 부각되고 있다 광화학스모그의 선구물질인 VOC의 주요 배출원은 도로차량, 비도로차량, 용제사용과 유류저장으로 파악되고 있으며 그중 용제사용 부문에는 세정, 인쇄, 세탁, 도장, 농약살포, 소비용품, 도로포장 통에서 대부분 배출되는 것으로 알려져 있다 또한 환경기초시설인 하폐수처리장, 폐기물 소각장 및 매립장 등에서도 다량의 VOC/악취 물질들이 배출되고 있다. (중략)

• Proceedings of the Korean Vacuum Society Conference
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• 한국진공학회 1996년도 제10회 학술발표회 논문개요집
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• pp.49-50
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• 1996