• Title/Summary/Keyword: 비탄성 중성자 산란

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Introduction to Neutron Scattering for Magnetic Materials Research (자성소재 연구를 위한 중성자산란 입문)

  • Jeong, Jae-Hong;Lee, Sang-Hyun;Park, Je-Geun
    • Journal of the Korean Magnetics Society
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    • v.22 no.3
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    • pp.103-108
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    • 2012
  • Having a de Broglie wavelength of a few ${\AA}$ with its corresponding energies in the range of a few to a few hundreds meV, neutrons are ideally suited for the studies of structure and dynamics in condensed matter research. Neutron scattering has been developed over the past 60 years or so and become a very mature and established experimental technique in the very broad range of material sciences. In this short introductory article, we have explained its working principles and provided few selected examples of application.

Study of the Molecular Reorientation in Ammonium Sulfate by Neutron Scattering

  • Kim, Huhn-Jun
    • Nuclear Engineering and Technology
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    • v.4 no.4
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    • pp.306-321
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    • 1972
  • Molecular reorientation in (NH$_4$)$_2$SO$_4$, has been studied by cold neutron scattering. For T=300$^{\circ}$K data, the isolated quasielastic spectra and form-factors at various scattering angles are compared with four reorientational models based on SKOLD theory. Front these, it is concluded that the NH$_4$ions are performing either 3-fold four axes or 2-fold three axes reorientation with $\tau$$_{c}$=2.0$\times$10$^{-11}$ sec. The temperature dependence of f. is studied over 100$^{\circ}$K-413$^{\circ}$K and for the high-temperature phase, the widths of composite spectra are compared with the results from NMR relaxation measurements. All the results have shown that the neutron scattering method is capable of giving detalis of the reorientational modes in solids and therefore some discussions are given on the application of this method. A study of the form-factor is applied for NH$_4$I (Phase I) by comparing the measurement with the calculation based on free rotation approximation and proposed a reorientation model of NH$_4$ ions in the octahedral potential cage with $\tau$$_{c}$$\leq$10$^{-12}$ sec. Also a brief theoretical prediction for the effect of reorientational motions on the inelastic spectrum is discussed.sed.

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Comparison of Light Output from NE213 for Electrons and Protons

  • Shin, Hyun-Kook;Koh, Byung-Joon
    • Nuclear Engineering and Technology
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    • v.11 no.2
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    • pp.111-117
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    • 1979
  • The light output of the NE213 liquid scintillator to electrons and protons was measured by coincidence spectrometer which employs the time of flight technique. The proton energies (3.2Mev, 4Mev, 5Mev, 6Mev) represent the kinetic energies of recoil protons from elastic scattering of a polyenergetic neutron source Am-Be (about 2-9 Mev) at angle of 45$^{\circ}$ and 60$^{\circ}$. The response of the NE213 liquid scintillator to protons was varied nonolinearly as the energy increased. while the response to electrons was varied linearly. The light intensity produced by electrons was relatively larger than that of protons in the rate of about three times when the same energy was introduced. The results of the light output to protons were similar to those of Batchelor et al.

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Borehole Elemental Concentration Logs: Theory, Current Trends and Next Level (암석구성성분검층: 원리, 연구동향 및 향후 과제)

  • Shin, Jehyun;Hwang, Seho
    • Geophysics and Geophysical Exploration
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    • v.22 no.3
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    • pp.149-159
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    • 2019
  • Borehole elemental concentration logging, measuring neutron-induced gamma rays by inelastic scattering and neutron capture interactions between neutron and formation, delivers concentrations of the most common elements found in the minerals and fluids of subsurface formation. X-ray diffraction and X-ray fluorescence analysis from core samples are traditionally used to understand formation composition and mineralogy, but it represents only part of formations. Additionally, it is difficult to obtain elemental analysis over the whole intervals because of poor core recovery zones such as fractures or sand layers mainly responsible for groundwater flow. The development of borehole technique for in situ elemental analysis plays a key role in assessing subsurface environment. Although this technology has advanced consistently starting from conventional and unconventional resources evaluation, it has been considered as exclusive techniques of some major service company. As regards domestic research and development, it has still remained an unexplored field because of some barriers such as the deficiency of detailed information on tools and calibration facility for chemistry and mineralogy database. This article reviews the basic theory of spectroscopy measurements, system configuration, calibration facility, and current status. In addition, this article introduces the domestic researches and self-development status on borehole elemental concentration tools.

New Magnetic Phases of Fe-N and Mn-Al Alloys Produced by Mechanochemical Milling (기계적 밀링 및 화학적 추출법에 의해 제조한 Fe-N 및 Mn-Al계의 새로운 자성재료)

  • Kyu-Jin Kim;Tae-Hwan Noh;Kenji Suzuki
    • Journal of the Korean Magnetics Society
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    • v.4 no.4
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    • pp.347-354
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    • 1994
  • The structural change and magnetic properties of mechanically milled Fe-N and Mn-Al alloy powders have been investigated by XRD, TEM, VSM, $M\"{o}ssbauer$ spectroscopy and inelastic neutron scattering measurements. During milling of ${\gamma}'-Fe_{4}N$ powders, and fcc ${\gamma}'-Fe_{4}N$ phase is transformed to a bct ${\alpha}'-Fe(N)$ phase by stress-induced martensitic transformation, being accompanied by an initial increase in saturation magnetization. During annealing the bct ${\alpha}'-Fe(N)$ nanocrystalline phase which is obtained by mechanical grinding for a long time, an ${\alpha}'-Fe_{16}N_{2}$ phase partially appears as an intermediate phase at 673~773 K, causing an increase in saturation magnetization. During milling of Mn-45, 70 and 85 at.% Al mixed powders, Al atoms are partially solubilized into an ${\alpha}-Mn$ phase. The Al supersaturated ${\alpha}-Mn-type$ phases change from paramagnetic to ferromagnetic : the saturation magnetization is 11 emu/g for the as-milled Mn-70 at.% Al powders. Moreover, by removing almost all Al atoms from the as-milled Mn-85 at.% Al powders using chemical leaching, the saturation magnetization increases up to 36 emu/g. The above bct ${\alpha}'-Fe(N)$ and ferromagnetic ${\alpha}-Mn$ type alloys are the magnetic materials found for the first time, by using the present mechanochemical process.

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