• Title/Summary/Keyword: 불확도 평가

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Cost-effective Investigation on Contaminated Land and Assessment of Measurement Uncertainty (오염토양의 효율적 조사기법과 측정불확도의 평가방법)

  • 이종천
    • Economic and Environmental Geology
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    • v.37 no.1
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    • pp.49-59
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    • 2004
  • The concectration and distribution of contaminants obtained from a contaminated land investigation or an environmental geochemistry survey constitutes the basis of a decision-making process on environmental policies or of scientific researches. As the quality of data determines the reliability of the result, the investigation plan should be adjusted according to the purpose of the investigation. In general, the effort to improve the data quality had been focused mainly on the QA/QC procedures in laboratories. The rapid progress of analytical instrument has also contributed toward improving the analytical precision to a sacrificable degree. Nevertheless, in many cases, it is not the analytical precision that needs improvement for the better precision of overall measurement process: it is rather during the sampling process in the field that is responsible for the poor precision. To assess the data quality on a measured value, ISO recommends to provide information on "measurement uncertainty" along with the measured value. The measurement uncertainty in an environmental measurement context can be explained as the statistical number that expresses the degree of the uncertainty stemming from the sampling and analytical procedures. There is a cost involved in order to improve the precision of sampling and analytical methods so as to decrease the degree of measurement uncertainty. The economical point of compromise in an investigation planning can be achieved when the allowable degree of uncertainty has been set before-hand. The investigation can then be planned accordingly not to exceed the uncertainty limit. Furthermore, if the measurement uncertainty estimated from the preliminary investigation can be separated into sampling and analytical uncertainties, it can be used as a criterion where the resources for the investigation should be allotted cost-effectively to reinforce the weakest link of the whole investigation process. This paper aims to present a method of estimating the level of measurement uncertainty of a measured contamination concentration at a site used as an example and to show how the estimated uncertainty can be applied to serve the particular purpose of an investigation.

Estimation of Uncertainty on Greenhouse Gas Emission in the Agriculture Sector (농업분야 온실가스 배출량 산정의 불확도 추정 및 평가)

  • Bae, Yeon-Joung;Bae, Seung-Jong;Seo, Il-Hwan;Seo, Kyo;Lee, Jeong-Jae;Kim, Gun-Yeob
    • Journal of Korean Society of Rural Planning
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    • v.19 no.4
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    • pp.125-135
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    • 2013
  • Analysis and evaluation of uncertainty is adopting the advanced methodology among the methods for greenhouse gas emission assessment that was defined in GPS2000 (Good practice guideline 2000) and GPG-LULUCF (GPG Land Use, Land-Use Change and Forestry). In 2006 IPCC guideline, two approaches are suggested to explain the uncertainty for each section with a national net emission and a prediction value on uncertainty as follows; 1) Spread sheet calculation based on the error propagation algorithm that was simplified with some assumptions, and 2) Monte carlo simulation that can be utilized in general purposes. There are few researches on the agricultural field including greenhouse gas emission that is generated from livestock and cultivation lands due to lack of information for statistic data, emission coefficient, and complicated emission formula. The main objective of this study is to suggest an evaluation method for the uncertainty of greenhouse gas emission in agricultural field by means of intercomparison of the prediction value on uncertainties which were estimated by spread sheet calculation and monte carlo simulation. A statistic analysis for probability density function for uncertainty of emission rate was carried out by targeting livestock intestinal fermentation, excrements treatment, and direct/indirect emission from agricultural lands and rice cultivation. It was suggested to minimize uncertainty by means of extraction of emission coefficient according to each targeting section.

An Experimental Study on Magnus Characteristics of a Spinning Projectile at High Speed Region (회전발사체 마그너스 특성에 관한 고속 유동장 실험연구)

  • Oh, Se-Yoon;Lee, Do-Kwan;Kim, Sung-Cheol;Kim, Sang-Ho;Ahn, Seung-Ki
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.39 no.5
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    • pp.385-390
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    • 2011
  • The purpose of this research is to determine the dynamic Magnus effect data of a spinning projectile in wind-tunnel testing. In the present work, the high-speed wind-tunnel tests for the Magnus effect measurements were conducted on a 155-mm spin-stabilized projectile model in the Agency for Defense Development's Tri-Sonic Wind Tunnel at spin rates about 12,000 rpm. The test Mach numbers ranged from 0.7 to 2.0, and the angles of attack ranged from -4 to +10 deg. The validity of the wind-tunnel measurement techniques was evaluated by comparing them with the previous test results on the same configuration. The experimental results show that fair to good agreement is obtained with resonable accuracy.

Evaluation of Uncertainty Sources in Temperature Measurement Using Platinum Resistance Thermometer Caused by Temperature Gradient in Furnace and Sealed-type Freezing Point Cells (전기로 및 봉입형 응고점 셀 내의 온도구배가 미치는 표준백금저항온도계 온도측정의 불확도 요소 평가)

  • Kang, Kee-Hoon;Gam, Kee-Sool;Kim, Yong-Gyoo;Song, Chang-Ho
    • Journal of Sensor Science and Technology
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    • v.13 no.6
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    • pp.411-416
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    • 2004
  • In the international temperature scale of 1990 (ITS-90), standard platinum resistance thermometer (SPRT) is a defining standard thermometer used in the temperature range from 13.8033 K to $961^{\circ}C$. Uncertainty of SPRT is about several mK and uncertainty of defining fixed points of the ITS-90 which is used for calibrating SPRT is about several tenth of mK. Above $0^{\circ}C$. the defining fixed points are gallium melting point and indium, tin, zinc, aluminium and silver freezing points which are all realized using an electric furnace or a liquid bath. To realize freezing point of tin ($231.928^{\circ}C$) and zinc ($419.527^{\cir}C$), two 3-zone furnaces which have 3 electric heaters were manufactured. Temperature gradient of the constructed furnaces were tested. Uncertainty caused by temperature gradient of furnace and immersion effect of SPRT in the sealed-type freezing point cells were evaluated 0.038 mK for tin freezing point and 0.036 mK for zinc freezing point.

A W-Band Millimeter-Wave Power Standard Transfer System Using the Direct Comparison Method (직접 비교법을 이용한 W-Band 밀리미터파 전력 표준 전달 시스템)

  • Kwon, Jae-Yong;Kang, Tae-Weon;Kang, Jin-Seob;Lee, Dong-Joon
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.24 no.1
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    • pp.47-54
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    • 2013
  • This paper introduces a W-band millimeter-wave power standard transfer system using the direct comparison method. The transfer system was developed to evaluate the effective efficiency and calibration factor of a W-band waveguide power sensor. The evaluation method and the measured results of the directional coupler that characterizes the calibration system are studied. The uncertainties of the standard transfer system are investigated, and the major uncertainty contributors are discussed as well. The performance of the realized W-band power standard transfer system was verified by comparing results with reference values.

Calibration by Comparison and Uncertainty Assessment of Industrial Thermometers at the Boiling Point of Nitrogen (질소의 끓는점에서의 산업용 온도계 비교 교정과 불확도 평가)

  • Yang, Inseok;Gam, Kee Sool;Joung, Wukchul;Kim, Yong-Gyoo
    • Journal of Sensor Science and Technology
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    • v.22 no.6
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    • pp.404-409
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    • 2013
  • We devised calibration procedure for industrial thermometers by a comparison method at the boiling point of nitrogen (${\sim}-196^{\circ}C$). The uncertainty of the calibration was 4 mK (k = 2). As experimentally demonstrated in this work, the effect of the atmospheric pressure on the boiling point of nitrogen can be easily detected by the thermometer. Therefore, when the boiling point of nitrogen is used for calibration of thermometer by comparison, either a reference thermometer must be used to provide the reference temperature or the effect of atmospheric pressure should be carefully considered. The use of a copper block with a large thermal mass soaked into the liquid nitrogen was proven to be more reliable, and the stability of the temperature immersed into the copper block was 1.4 mK. The temperatures at the thermometer wells, evaluated by the crossed-measurement method to compensate for the inaccuracy of the thermometers and the linear drift of the temperature of the copper block, were equivalent within 0.23 mK of standard uncertainty.

Calculation and Projection of Greenhouse Gas Emissions from La Chureca Landfill in Managua, Nicaragua (니카라과 마나과시 La Chureca 매립장 온실가스 발생량 산정 및 예측)

  • Kim, Choong Gon;Lee, Hyun Jun;Kang, Ho Jeung;Kim, Jae Young
    • Journal of the Korea Organic Resources Recycling Association
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    • v.30 no.4
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    • pp.131-139
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    • 2022
  • The aim of this study was to assess the feasibility of a landfill project to reduce greenhouse gas (GHG) from La Chureca Landfill in Managua, Nicaragua ("Project"). The feasibility study involved surveying the status and composition of waste on its way in to the landfill and projecting GHG emissions from the landfill. A projection of the GHG emissions with the IPCC model based on the survey results indicated the period 2006 to 2043 would see mean yearly GHG emissions of 290,147 ton-CO2/year with model certainty not considered, and 217,610 ton-CO2/year with model certainty considered. Thus, the result exceeded the corresponding median and mean values of other CDM projects implemented in Central America, even after model uncertainty was considered together with the conservative estimation of carbon capture efficiency. The similar result was produced even with an analysis of sensitivity to error factors. All the findings of the study are expected to be applicable as basic data for deciding about whether & how to proceed with the Project.

정적형 유량계를 이용한 소닉노즐의 유출계수 교정 방법에 관한 연구

  • Sin, Jin-Hyeon;Gang, Sang-Baek;Go, Mun-Gyu;Im, Jong-Yeon;Jeong, Wan-Seop
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.08a
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    • pp.45-45
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    • 2010
  • 반도체 및 디스플레이 산업에 사용되는 진공펌프의 효율이 증대됨에 따른 성능 평가 기술의 향상 과 미세 유량을 조절 및 측정할 수 있는 시스템의 개발이 요구되고 있다. 유량 시스템 중 소닉노즐은 기체 유량 측정 표준기로 사용되고 있다. 또한 유량 측정에 있어서 사용상의 편리성, 이동성, 재현성 등 여러 가지의 장점을 가지고 있어 산업 현장에서 많이 사용되고 있다. 본 연구는 소닉노즐을 넓은 유량 범위에서 사용할 수 있도록 소닉노즐의 유출계수 교정을 목적으로 한다. ISO 9300에서 제시한 사양에 맞추어 목 직경 0.03 mm와 0.2 mm 그리고 1.6 mm의 소닉노즐을 제작하였다. 한국표준과학연구원에서 진공용 유량측정 장치로 개발된 정적형 유량계를 이용하여 제작된 3 종의 소닉노즐 유출계수를 확장불확도 3% 이내로 교정하였다. 교정된 소닉노즐의 유량 측정범위는 약 0.6~90, 000 cc/min 범위를 갖는 것으로 나타났으며, 사용유동 조건에 해당되는 레이놀드 수(Reynolds number) 범위는 26~75, 700 으로 확인되었다. 이러한 결과는 교정된 소닉노즐을 이용하여 진공공정에서 필요한 극 미세 유량의 정밀측정을 가능하게한 새로운 연구결과로 판단된다. 교정된 소닉노즐을 이용하여 진공펌프의 배기속도 측정결과는 기 구축된 정적법을 이용한 배기속도 측정결과와 3% 이내의 오차범위내로 매우 잘 일치함을 보였다. 교정된 소닉노즐은 향후 반도체 및 디스플레이 공정에 사용되는 다양한 진공펌프들의 배기속도를 현장에서 간단하게 평가할 수 있는 '현장 성능평가 장치'에 활용할 예정이며, 현재 공정현장에서 배기속도 측정에 널리 사용 중인 MFC를 대체할 수 있을 것으로 예상된다.

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Evaluation of the proficiency testing results using river water-based reference materials for heavy metal analysis (중금속분석용 하천수 매질표준물질을 이용한 숙련도 결과 평가)

  • Song, Ko-Bong;Kim, Young-Hee;Shin, Sun-Kyoung;Lee, Su-Yeong;Kim, Hyun-Jung;Kang, Hak-Gu;Kim, Il-Gyu;An, Hee-Ju
    • Analytical Science and Technology
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    • v.23 no.3
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    • pp.284-294
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    • 2010
  • In this study, river water-based reference materials (RMs), NIER-I08RW and NIER-I09, for trace metal analysis were prepared and certified for Pb, Cd, Cr and Cu with evaluation of uncertainties. The RMs were confirmed to be homogeneous enough to be used as proficiency testing materials since within-bottle homogenieties of the RMs were lower than 0.3 times of targeted standard deviation of proficiency testing. The RMs were distributed to environmental testing laboratories for the proficiency testing and the variation of Z scores of the proficiency testing results were compared for different assigned values. The relative bias, $B_{relative}$, deviations between reference values and consensus values, were lower than ${\pm}$1 except for cadmium of NIERI08RW. The results showed both values were in a good agreement and only 2.9% of Z scores changed by using a different assigned values such as consensus and reference values.

The Evaluation of Recovery Rate of Radioimmunoassay Using Certified Reference Material (CRM) (인증표준물질(CRM)을 이용한 방사면역측정법의 회수율 평가)

  • Choi, Sung Hee;Shin, Sun Young;Lim, So Hee;Hong, Mee Kyung;Noh, Gyeong Woon;Kim, Jin Eui
    • The Korean Journal of Nuclear Medicine Technology
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    • v.18 no.1
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    • pp.158-162
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    • 2014
  • Purpose: Reference material (RM) is defined as material that is safe and homogeneous enough about specified characteristic that is made with a purpose of using test of measurement or nominal characteristic. Certified reference material (CRM), which is issued by authorized organization, is defined as reference material that provides characteristic value, link uncertainty and retroactivity. The purpose of this paper was to evaluate recovery of radioimmunoassay by Certified Reference Material enclosed with a certificate and therefore to enhance reliability of test. Materials and Methods: WHO certified reference material is purchased from NIBSC (National Institute for Biological Standard and Control, United Kingdom) and made of 3 levels that are C-1 (low concentration), C-2 (medium concentration) and C-3 (high concentration) and measured for kit at the Seoul National University Hospital. Recovery rate is evaluated after measurement at four different days. Results: Recovery rate results using WHO certified reference material are T4 90%, Ferritin 88%, PSA 94%, Prolactin 99%, AFP 94% and TSH 93%. Conclusion: A procedure that appropriate accuracy, precision, specificity, sensitivity, reproducibility, and validate on the subject of kit for radioimmunoassay is essential. Recovery rate assay as extraction efficiency of analysis process is percent about already measuring results of analysis result after all measuring process. This is very important assessment standards of performance evaluation of immunoassay kit. Recovery rate results of 6 type used WHO CRM are satisfactory to 88~99%. This demonstrates that the radioimmunoassay is a very accurate measurement, which is very effectively utilized in clinical practice.

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