• Journal of Sensor Science and Technology
• /
• v.9 no.3
• /
• pp.153-162
• /
• 2000

Triple points of high purity materials have been used to calibrate primarily the capsule-type platinum resistance thermometer (PRT) in the temperature range of the triple point of equilibrium hydrogen (13.8033 K) and water (273.16 K). In this work, triple points of Ne, $O_2$, Ar, Hg and $H_2O$ except for the triple point of equilibrium hydrogen were realized to establish the International Temperature Scale of 1990 (ITS-90). At each fixed point, two capsule-type PRTs, which were selected for the international comparison, were tested two times. The combined uncertainties of the realization of each triple point were calculated considering the type A and type B evaluation. In Korea Research Institute of Standards and Science, the combined standard uncertainties of the defining triple Points by the ITS-90 were estimated to about 0.18 mK for Ne, 0.14 mK for $O_2$, 0.14 mK for Ar, 0.24 mK for Hg and 0.11 mK for $H_2O$, respectively.

• Journal of the Korean Solar Energy Society
• /
• v.36 no.4
• /
• pp.11-20
• /
• 2016

For accurate wind resource assessment and wind turbine performance test, it is essential to secure wind data covering a rotor plane of wind turbine including a hub height. In general, we can depict wind speed profile by extrapolating or interpolating the wind speed data measured from a meteorological tower where multiple anemometers are mounted at different heights using a power-law of wind speed profile. The most important parameter of a power-law equation is a vertical wind profile exponent which represents local characteristics of terrain and land cover. In this study, we calculated diurnal vertical wind profile exponents of 8 locations in Jeju Island who possesses excellent wind resource according to the GUM (Guide to the Expression of Uncertainty in Measurement) to evaluate its uncertainty. Expanded uncertainty is calculated by combined standard uncertainty, which is the result of composing type A standard uncertainty with type B standard uncertainty. Although pooled standard deviation should be considered to derive type A uncertainty, we used the standard deviation of vertical wind profile exponent of each day avoiding the difficult of uncertainty evaluation of diurnal wind profile variation. It is anticipated that the evaluated uncertainties of diurnal vertical wind profile exponents at 8 locations in Jeju Island are to be registered as a national standard reference data and widely used in the relevant areas.

• Analytical Science and Technology
• /
• v.22 no.4
• /
• pp.302-306
• /
• 2009

A trace amount of boron in steel significantly influences its mechanical and physical properties. A prompt gamma ray activation analysis (PGAA) method is used to measure boron in low alloy steel samples of KRISS 101-01-C21~C26. NIST SRMs of 362, 364, 1761 and 1767 serve as the control standards to validate the measurement method. The measured values of the NIST SRMs are consistent with their certified values within the expected uncertainties, except for that of NIST SRM 362. Experimental uncertainties are evaluated according to the guidelines given by the International Organization for Standardization (ISO). The expanded uncertainties are calculated with a coverage factor of 2, at approximately 95% confidence level. The calculated relative expanded uncertainties of boron mass fractions are between 3% and 7% at the mg/kg level. The results are compared with the results measured by the solvent extraction-inductively coupled optical emission spectrometry (ICP/OES) method.

• Progress in Medical Physics
• /
• v.23 no.2
• /
• pp.71-80
• /
• 2012

In order to verify exact dose distributions in the state-of-the-art radiation techniques, a newly designed three-dimensional dosimeter and technique has been took strongly into consideration. The main purpose of our study is to verify the optimized parameters of polymer gel as a real volumetric dosimeter in terms of the various study of MRI. We prepared a gel dosimeter by combing 8% of gelatin, 8% of MAA, and 10 mM of THPC. We used a Co-60 gamma-ray teletherapy unit and delivered doses of 0, 2, 4, 6, 8, 10, 12, and 14 Gy to each polymer gel with a solid phantom. We used a fast spin-echo pulse to acquire the characterized T2 time of MRI. The signal noise ratio (SNR) of the head & neck coil was a relatively lower sensitivity than the body coil; therefore the dose uncertainty of head & neck coil would be lower than body coil's. But the dose uncertainty and resolution of the head & neck coil were superior to the body coil in this study. The TR time between 1,500 ms and 2,000 ms showed no significant difference in the dose resolution, but TR of 1,500 ms showed less dose uncertainty. For the slice thickness of 2.5 mm, less dose uncertainty of TE times was at 4 Gy, as well, it was the lowest result over 4 Gy at TE of 12 ms. The dose uncertainty was not critical up to 6 Gy, but the best dose resolution was obtained at 20 ms up to 8 Gy. The dose resolution shows the lowest value was over 20 ms and was an excellent result in the number of excitation (NEX) of three. The NEX of two was the highest dose resolution. We concluded that the better result of slice thickness versus NEX was related to the NEX increment and thin slice thickness.

• Proceedings of the Korean Radioactive Waste Society Conference
• /
• 2008.05a
• /
• pp.337-338
• /
• 2008

• Proceedings of the Korean Radioactive Waste Society Conference
• /
• 2005.11a
• /
• pp.334-335
• /
• 2005

• Proceedings of the Korean Radioactive Waste Society Conference
• /
• 2006.11a
• /
• pp.143-143
• /
• 2006

• Analytical Science and Technology
• /
• v.26 no.2
• /
• pp.125-134
• /
• 2013

This study was demonstrated to estimate the measurement uncertainty of 23 multiple-component amino acids from beef bone extract by high performance liquid chromatography (HPLC). The sources of measurement uncertainty (i.e. sample weight, final volume, standard weight, purity, standard solution, calibration curve, recovery and repeatability) in associated with the analysis of amino acids were evaluated. The estimation of uncertainty obtained on the GUM (Guide to the expression of uncertainty in measurement) and EURACHEM document with mathematical calculation and statistical analysis. The content of total amino acids from beef bone extract was 36.18 g/100 g and the expanded uncertainty by multiplying coverage factor (k, 2.05~2.36) was 3.81 g/100 g at a 95% confidence level. The major contributors to the measurement uncertainty were identified in the order of recovery and repeatability (25.2%), sample pretreatment (24.5%), calibration-curve (24.0%) and weight of the reference material (10.4%). Therefore, more careful experiments are required in these steps to reduce uncertainties of amino acids analysis with a better personal proficiency improvement.

• Transactions of the Korean Society of Mechanical Engineers B
• /
• v.28 no.10
• /
• pp.1219-1230
• /
• 2004

Comparing to the gravimetric and volumetric method, the flowmeter calibration based on the master meter method is relatively economical and convenient, especially for high flowrate. The uncertainty of flow quantity and flowrate using the master meter method was evaluated according to the GUM (Guide to the Expression of Uncertainty in Measurement). In order to apply for the wider flow range, two master meters (electromagnetic flow meter) were employed as reference flowmeters. The uncertainty of the master meter was obtained by combining the statistical variation of the repeated measurements and the variation of fluid density and pipe material due to temperature and pressure changes were scrutinized. for a practical application, the uncertainty of calibrator, whose measuring capacity of 1000 ㎥/h obtained by employing two 500 ㎥/h electromagnetic How meters, was evaluated. The uncertainty budget shows the quantitative contribution of each uncertainty component to the overall uncertainty of the calibrator. As a result, it was found that the dominant uncertainties were from the master meter, which was evaluated statistically, and from the process of least squares fitting. On the contrary, the uncertainties arising from the variation of the fluid density and the pipe volume due to the temperature and pressure were negligible.

• Journal of the Korean Society for Precision Engineering
• /
• v.24 no.10
• /
• pp.91-98
• /
• 2007

This paper describes the development of the calibration system for a multi-axis force/moment sensor and its uncertainty evaluation. This calibration system can generate the continuous forces (${\pm}Fx,\;{\pm}Fy$ and ${\pm}Fz$) and moments (${\pm}Mx,\;{\pm}My$ and ${\pm}Mz$). Many kinds of multi-axis force/moment sensors in industries should be carried out the characteristic test or the calibration with the calibration system that can generate the forces and the moments. The calibration systems have been already developed are the disadvantages of the low capacity, the generation of step forces(10N, 20N ...) and step moments(1Nm, 2Nm ...) with weights, the high coasts in manufacture and so on. In this paper, the calibration system for a multi-axis force/moment sensor that can generate the continuous three forces and three moments was developed. Their ranges are $0{\sim}2000N$ in all force-directions and $0{\sim}400Nm$ in all moment-directions. And the system was evaluated in the expanded relative uncertainty. They were ${\pm}0.0004$ in all forces ${\pm}Fx,\;{\pm}Fy$ and ${\pm}Fz$, and ${\pm}0.0004$ in all moments ${\pm}Mx,\;{\pm}My$ and ${\pm}Mz$.