• Title/Summary/Keyword: 분산입도

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Research on the Dispersion Stability and Scale up of Carbon Slurry Fuel (카본슬러리 연료의 분산안정성 개선 및 scale up 제조연구)

  • Jo, Min-Ho;Yang, Mun-Kyu;Lee, Ik-Mo;Cho, Joon-Hyun;Kwon, Tae-Soo;Jeong, Byung-Hun;Han, Jeong-Sik
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2008.11a
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    • pp.459-462
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    • 2008
  • In manufacture of slurry fuel, the effects of process parameters on the carbon dispersion stability have been investigated. The particle size and contents of the carbon slurry taken from 3 (top, medium, bottom) positions in fuel reservoir were analyzed to estimate the dispersion of the carbon in Jet A-1. Through the application of various additives, it was found that NB463S84 additive showed the best dispersion and stability of carbon at accelerated gravity condition. The mixer performance was compared by the observation of height change of carbon-containing layer and measurement of particle sizes at the same conditions. Application of the mixing conditions obtained from the lab-scale to bench scale manufacture confirmed the practical feasibility of our research.

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Preparation of Ag Fine Particles from Aqueous Silver Solution by Reduction Reaction (Ag 水溶液으로부터 還元反應에 의한 Ag 微粒子의 製造 硏究)

  • Lee, Hwa-Young;Jin, Seon-Ah;Han, Young-Ju
    • Resources Recycling
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    • v.14 no.1
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    • pp.26-32
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    • 2005
  • A study on the preparation of Ag fine particles was performed through a reduction reaction using ascorbic acids as a reductant, which is one of the indispensable processes for the recycling of silver-bearing wastes. Silver nitrate solution in the range of 10~120 mmole/l was used and Tamol NN8906 or PVP was also used as a dispersant in the preparation of Ag fine particles size analyze, SEM, and TEM to determine the particle size and morphology of them. As a result, the reduction reaction of silver ions with ascorbic acid reached equilibrium within 10 min. It was found that about 60% excess of ascorbic acid was required in order to reduce completely silver ions in the solution. The particle size distribution of Ag particles prepared through the reduction reaction showed typically biomodal or trimodal distribution. Especially, initial Ag concentration in the solution, the type and amount of dispersant added during the reduction reaction played an important role in determining the mean particle size of Ag particles.

The Dispersion Capacity of Some Chemical Dispersing Agents in Korean Soils (우리나라 토양(土壤)에 있어서 수종(數種) 분산제(分散劑)의 분산능(分散能)에 관(關)하여)

  • Im, Jeong-Nan;Cho, In-Sang;Cho, Seong-Jin
    • Korean Journal of Soil Science and Fertilizer
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    • v.13 no.2
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    • pp.65-70
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    • 1980
  • This experiment was aimed at selecting the most suitable dispersing agent to the Korean soils. The particle size distribution of 18 soil samples representing the great soil groups in Korea was analysed with 5 different dispersing agents by pipette-method. Passing percent of 0.05, 0.02 and 0.002mm in diameter was used for the comparision of the dispersion capacity of chemical agents. The results obtained are as follows; 1. The influence of chemical agents on dispersion seemed to be greater to finer soil particles. The passing percents of 0.002mm showed a great differences according to the chemical agents used, while little differences was observed in those of 0.05mm. 2. It was showed that sodium pyrophosphate had the highest dispersion capacity for the most of Korean soils, the dispersion capacity of sodium hexametaphosphate was also high enough except for volcanic ash soils. 3. It was recommendable that sodium hexametaphosphate could widely be used as a dispersing agent in the routine analysis of soil particle size distribution except for the Volcanic ash soils. 4. The dispersion of Volcanic ash soils was rather poor when chemical agents used. Therefore, special care should be taken for the dispersion of allophane soils.

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A Study of Dispersion Characteristics of Sunsik Using Fluidized-Bed Granulator (유동층 과립기를 이용한 선식의 분산 특성)

  • Kim, Gorae;Hwang, Yunhee;Lee, Seokhoon
    • Food Engineering Progress
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    • v.21 no.3
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    • pp.267-272
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    • 2017
  • To improve dispersibility of cereal powder without additives, granulation of cereal powder was conducted using fluidized-bed granulator. Operation condition was sample 300 g, internal temperature $40^{\circ}C$, ventilation speed $30-90m^3/h$, inlet temperature $90^{\circ}C$ and spray pressure 2.5 bar. The amount of distilled water (20-45%) as binder, granulation time (10-15 min) and drying time (3-10 min) were controlled. Mean diameter over volume (Brouckere mean, $D_{4,3}$) was increased from $123{\mu}m$ to $263{\mu}m$ and dispersibility was improved from 73% to 92.25% at experiment conditions. Wettability (wetting time) was drastically decreased from 5,000 second to 7 second. Granulation of cereal powder did not affect sinkability and mean diameter over volume as wet analysis was about the same between raw and granulated cereals. Such phenomenon means that granulation with only water as binder enables cereal powder to disperse in water or milk without rapid sedimentation.

The Measurement of Oil Globule Size Distribution in the Soymilk Suspended with the Soybean Particle (대두입자가 분산된 두유에서 기름입자의 입도분포 측정)

  • Chung, J.B.;Yoon, S.K.;Sohn, H.S.
    • Korean Journal of Food Science and Technology
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    • v.22 no.4
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    • pp.369-372
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    • 1990
  • Although the measurement of oil globule size distribution is necessary to detect the process of demulsification, the reasonable methodology for its measurement has not been suggested because the solution of soymilk contains insoluble soybean particle and the protein to interfere with the detection of oil globule or oil content. The oil globule size distribution was measured by the homogeneous suspension and cumulative method under gravitational force or centrifugal force, which were modified with Stokes' low. The geometric mean diameter of oil globules in this soymilk was $033{\mu}m\;and\;031{\mu}m$ under gravitational method and centrifugal method, respectively. The differences of oil globule size distribution in the solutions emulsified by different pressures were detected by this method. The mean diameter of the solutions treated at higher pressure was shifted to smaller size and the distribution pattern of the solutions at higher pressure became more compact around the mean diameter.

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Research on the Dispersion Stability and Scale up of Carbon Slurry Fuel (카본슬러리 연료의 분산안정성 개선 및 scale up 제조 연구)

  • Cho, Min-Ho;Yang, Mun-Kyu;Lee, Ik-Mo;Cho, Joon-Hyun;Kwon, Tae-Soo;Jeong, Byung-Hun;Han, Jeong-Sik
    • Journal of the Korean Society of Propulsion Engineers
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    • v.13 no.3
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    • pp.34-40
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    • 2009
  • For the preparation of carbon-slurry fuel, the effects of process parameters on the carbon dispersion stability in the liquid fuel have been investigated. The dispersion stability of carbon-slurry fuels could be monitored by measurements of particle size and carbon contents in the different positions, and observation of dispersion states after centrifuging. Through the application of various additives, it was found that NB463S84 based on polyolefin succinimde showed the best dispersion and longest stability life of carbon-slurry fuel. Also, PIBSI (polyisobutenyl succimide) with the similar functional groups to NB463S84 was effectively synthesized and same dispersion stability was verified by application to carbon-slurry fuel. Finally, the possibility of practical use of carbon-slurry fuels was confirmed by application of the mixing conditions obtained from g scale to kg scale preparation.

Preparation of Ag Nano-Powder from Aqueous Silver Solution through Reductive Precipitation Method (환원침전법을 이용한 수용액으로부터 은 나노분말의 제조 연구)

  • Lee Hwa-Yaung;Oh Jong-Kee
    • Resources Recycling
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    • v.14 no.6 s.68
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    • pp.21-27
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    • 2005
  • As one of the hydrometallurgical processes available in the recycling of silver-bearing wastes, the preparation of Ag nano-powder was investigated by a reductive precipitation reaction in silver solution using sodium formaldehydesulfoxylate and ascorbic acid as a reducing agent. Silver solution was prepared by dissolving silver nitrate with distilled water, and Tamol NN8906, PVP, SDS and caprylic acid were also used respectively as the dispersant to avoid the agglomeration of particles during the reductive reaction. Ag particles obtained from the reduction reaction from silver solution were characterized using the particle size analyzer and TEM to determine the particle size distribution and morphology. It was found that about $40\%$ excess of sodium formaldehydesulfoxylate was required to reduce completely silver ions in the solution. It alto appeared that the particle size generated with sodium formaldehydesulfoxylate was much greater than that with ascorbic acid. As far as the effect of dispersant on the Ag particles was concerned, the particle size distribution showed typically bimodal distribution in case of Tamol/FVP while very broad distribution ranged from 0.01 to $100{\mu}m$ appeared in case of SDS/caprylic acid.

Performance Improvement of Parallel Processing System through Runtime Adaptation (실행시간 적응에 의한 병렬처리시스템의 성능개선)

  • Park, Dae-Yeon;Han, Jae-Seon
    • Journal of KIISE:Computer Systems and Theory
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    • v.26 no.7
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    • pp.752-765
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    • 1999
  • 대부분 병렬처리 시스템에서 성능 파라미터는 복잡하고 프로그램의 수행 시 예견할 수 없게 변하기 때문에 컴파일러가 프로그램 수행에 대한 최적의 성능 파라미터들을 컴파일 시에 결정하기가 힘들다. 본 논문은 병렬 처리 시스템의 프로그램 수행 시, 변화하는 시스템 성능 상태에 따라 전체 성능이 최적화로 적응하는 적응 수행 방식을 제안한다. 본 논문에서는 이 적응 수행 방식 중에 적응 프로그램 수행을 위한 이론적인 방법론 및 구현 방법에 대해 제안하고 적응 제어 수행을 위해 프로그램의 데이타 공유 단위에 대한 적응방식(적응 입도 방식)을 사용한다. 적응 프로그램 수행 방식은 프로그램 수행 시 하드웨어와 컴파일러의 도움으로 프로그램 자신이 최적의 성능을 얻을 수 있도록 적응하는 방식이다. 적응 제어 수행을 위해 수행 시에 병렬 분산 공유 메모리 시스템에서 프로세서 간 공유될 수 있은 데이타의 공유 상태에 따라 공유 데이타의 크기를 변화시키는 적응 입도 방식을 적용했다. 적응 입도 방식은 기존의 공유 메모리 시스템의 공유 데이타 단위의 통신 방식에 대단위 데이타의 전송 방식을 사용자의 입장에 투명하게 통합한 방식이다. 시뮬레이션 결과에 의하면 적응 입도 방식에 의해서 하드웨어 분산 공유 메모리 시스템보다 43%까지 성능이 개선되었다. Abstract On parallel machines, in which performance parameters change dynamically in complex and unpredictable ways, it is difficult for compilers to predict the optimal values of the parameters at compile time. Furthermore, these optimal values may change as the program executes. This paper addresses this problem by proposing adaptive execution that makes the program or control execution adapt in response to changes in machine conditions. Adaptive program execution makes it possible for programs to adapt themselves through the collaboration of the hardware and the compiler. For adaptive control execution, we applied the adaptive scheme to the granularity of sharing adaptive granularity. Adaptive granularity is a communication scheme that effectively and transparently integrates bulk transfer into the shared memory paradigm, with a varying granularity depending on the sharing behavior. Simulation results show that adaptive granularity improves performance up to 43% over the hardware implementation of distributed shared memory systems.

Applied-Mineralogical Characterization and Assessment of Some Domestic Bentonites (II): Mineralogical Characteristics, Surface Area, Rheological Properties, and Their Relationships (국내산 벤토나이트에 대한 응용광물학적 특성 평가 (II): 광물학적 특징, 체표면적 및 유변학적 특성과 그 연계성)

  • 노진환;유재영;최우진
    • Journal of the Mineralogical Society of Korea
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    • v.16 no.1
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    • pp.33-47
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    • 2003
  • Various applied-mineralogical characterization including measurements of surface area, size distribution, swelling index, and viscosity were done for some domestic bentonites in order to decipher the rheological properties and their controlling factors. The bentonites, which are Ca-type and relatively low-grade (rnontmorillonite contents: 30 ∼ 75 wt%), occur mostly as subhedral lamellas with the size range of 2 ∼ 4 $\mu\textrm{m}$. The size distribution of mineral fractions in bentonite suspension is dominant in the range of 10 ∼ 100 $\mu\textrm{m}$, and though rather complicated, exhibits roughly bimodal patterns. The feature is more conspicuous in the case of zeolitic bentonite. The bentonites have surface areas ranging 269 ∼ 735 $\m^2$/g, which are measured by EGME adsorption method. The EGME surface areas are nearly proportional to the rnontmorillonite contents, moisture contents, or total CEC. In the surface area measurements, zeolitic bentonites have slightly higher values than those zeolite- free types. The measured swelling index and viscosity of domestic bentonites are comparatively low in values. The swelling values of bentonites were measured to be 250∼500% at maximum by progressively mixing amounts of 2 ∼ 5 wt% Na$_2$CO$_3$, which varies depending on the contents of rnontmorillonite and other impurities, especially zeolite. Much amount of sodium carbonate is required for optimum swelling property of zeolitic bentonited which has usually strong Na- exchanged capacity. The bentonites, which are comparatively feldspar-rich and low in size and crystallinity, tend to be higher in viscosity values. Tn addition, the viscosity is largely higher in case of the bentonites with higher pH in suspension. However, the rheological properties of bentonites such as swelling index and viscosity do not show any obvious relationships with rnontmorillonite contents and mean particle size in suspension. In contrast, roughly speaking, the swelling index of bentonites is reversely proportional to the values of surface area which can be regarded as a collective physico-chemical parameter encompassing all the effects caused by mineral composition, surface charge, particle size, morphological farm, and etc. in bentonites. Thus, the rheological properties in bentonite suspension appear to be rather complicated characteristics which mainly depend on the flocculation of clay particles and the mode of particle association, i.e. quasicrystals, controlled by surface charge, morphology, size, and texture of rnon-tmorillonite, and which partly affected by the finer impurities such as zeolite.

Molten salt method에 의한 $BaTiO_3$ 나노 입자 합성

  • Park, Guk-Hyo;Sin, Hyo-Sun;Yeo, Dong-Hun;Hong, Yeon-U;Kim, Hyeong-Sun
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.273-273
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    • 2010
  • 최근 들어 에너지 개발과 환경문제의 해결방안으로 열전발전 및 열전냉각에 많은 관심과 연구가 진행되고 있다. 열전소재의 특성 향상을 위해 열전성능지수를 높이기 위하여 나노 입자상을 열전소재 내에 분산하고자 하는 연구가 진행되었다. Grain 내에 나노 입자를 분산하기 위해서는 원료 입자에서부터 나노 입자가 열전소재 내에 분산되어야 하며 이것은 산화물 나노입자의 코어-쉘 형성으로부터 가능하다. 이 과정에서 나노 입자를 열전소재 내에 코어로 분산하기위한 나노입자의 합성 및 제어가 필수적이다. 본 연구에서는 용융염법을 이용한 BaTiO3 나노 일자를 합성하고 이들을 용매에 분산하는 것을 목표로 하였다. 염으로는 KCl, LiCl, NaCl 및 이들의 혼합 염을 사용하였으며 염의 청가량, 염의 종류, 반응온도 및 반응시간의 변화에 따라 BaTiO3 나노 입자를 합성하였다. 또한, 합성된 나노 입자의 입자크기와 응집 제어를 통해 나노입자들의 분산 상태를 확인해 보았다. 이 결과는 SEM, TEM, 입도측정기, XRD등의 측정 결과를 통하여 확인하고자 하였다.

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