• Title/Summary/Keyword: 분말 철

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Study on Improvement of Tungsten Alloy Granular Powder in Defense Industry (방산 분야 텅스텐 합금 과립분말 개선 연구)

  • Ji, Sangyong
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.21 no.10
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    • pp.206-211
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    • 2020
  • Tungsten alloys are used widely in general industrial fields, but they are difficult to cast, so products are manufactured using powder metallurgy. In this study, a mixed powder of tungsten, nickel, and iron homogenized using a ball mill was added to pure water as a solvent, and PVA as a binder was added to prepare a spray drying mixture. The mixed liquid was prepared using a spraying machine. A study was carried out to produce a granular powder that can reduce the variations between products during the molding and sintering process of the powder metallurgy method. A preliminary experiment was conducted to confirm the influence of the variables in the granulation process. Through the preliminary test results, this experiment was performed with the volume of solvent of the spray drying the mixture as an independent variable, and granular powder having a mean particle size similar to that of the existing mass-production conditions and an increased apparent density was prepared. In addition, a pilot test was conducted for the molding and sintering process. The improved granular powder reduced the characteristic variation (weight variation) of the mass-produced product.

Removal of Nickel from the Etching Waste Solution of Ferric Chloride (엣칭용 염화제2철 폐액중의 니켈제거)

  • Doh, Yong-Il;Jeung, Woo-Won;Lee, Man-Ho
    • Applied Chemistry for Engineering
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    • v.7 no.4
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    • pp.614-622
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    • 1996
  • Efficient removal of nickel from the ferric chloride etching solution has been studied. At first, $Fe^{3+}$ was reduced to $Fe^{2+}$ by the electrolytic iron flake or the waste shadow mask iron plate. And then, $Ni^{2+}$ was removed from the solution by electrolytic iron powder. Under the optimum conditions the reduced rates of nickel were 99 % and 98%, respectively at the initial $Ni^{2+}$ concentrations of 1.0% and 0.1%. Sludge formed during reduction of $Fe^{3+}$ in the solution were analyzed by XRD and SEM.

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Control of Nano-Scaled Surface Microstructure of Al Sample for Improving Heat Release Ability (Al 소재의 방열특성 향상을 위한 미세조직 제어 연구)

  • Yeo, In-Chul;Kang, In-Cheol
    • Journal of Powder Materials
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    • v.22 no.1
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    • pp.21-26
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    • 2015
  • In this study, the control of microstructure for increasing surface roughness of Al with an electro-chemical reaction and a post treatment is systematically investigated. The Al specimen is electro-chemically treated in an electrolyte. In condition of the post treatment at $100^{\circ}C$ for 10 min, a change of the surface microstructure occur at 50V (5 min), and a oxidized layer is at 400V, to which lead a decreasing surface roughness. The minimum temperature of the post treatment for a change of microstructure is $80^{\circ}C$. Moreover, in the condition of 300V (5 min), the electro-chemical reaction is followed by the post treatment at $100^{\circ}C$, the critical enduring time for the change of microstructure is 3 min. The longer post treatment time leads to the rougher surface. The treated Al specimen demonstrate better heat release ability owing to the higher surface roughness than the non-treated Al.