• Title/Summary/Keyword: 복합분쇄

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Preparation Of Composite particles with planarized $SiO_2$ Particles (평탄면을 갖는 $SiO_2$미립자의 제조와 이를 이용한 $SiO_2/TiO_2$복합입자의 제조)

  • 신달식;김광수;이옥섭;이성호
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.25 no.1
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    • pp.37-54
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    • 1999
  • Planarized SiO$_2$ particles were prepared by two-step reduction method of making much smaller particles, micron-sized ones, to improve spreadability, adherence, and smoothness. Various pigments known as flaky extender usually have terrace layers on their surfaces, but SiO$_2$ Particles in this study exhibit a smooth surface structure. These single SiO$_2$ particles were used for core particles to prepare the composite particles coated with ultra fine TiO$_2$ particles by a homogeneous precipitation method. The thickness and the morphology of the deposited TiO$_2$ layer could be altered by adjusting the reactant concentrations, reaction time and temperature. The characteristics of SiO$_2$/TiO$_2$composite in the field of color cosmetics is to give a UV-cut effect and to enhance the chroma of human skin color, one of optical properties.

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Attrition Milling and Reaction-sintering of the Oxide-Metal Mixed Powders: II. Reaction-sintering Behavior as the Milling Characteristics of Powders (산화물과 금속 복합 분말의 Attrition Milling 및 반응소결: II. 분말의 분쇄특성에 따른 반응소결 거동)

  • 황규홍;김의훈
    • Journal of the Korean Ceramic Society
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    • v.31 no.4
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    • pp.448-456
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    • 1994
  • The reaction-sintered alumina and zirconia-alumina ceramics were fabricated from the Al/Al2O3 or Zl/ZrO2(Ca-PSZ) powder mixtures via the attrition milling. And the effects of the milling characteristics of used raw powders on reaction sintering were investigated. After attrition milling and isopressing at 400 MPa the Al/Al2O3 specimen was oxidated at 1200℃ for 8 hours followed by sintering at 1550℃ for 3 hours. Because mixed powders of flake-type Al with coarse alumina was much more effectively comminuted than the globular-type Al with coarse alumina powders, it's sintered body of more than 97% theoretical density was achived, but low contents of Al leads to relatively higher shrinkage of about 8%. And because coarse alumina particles was much more beneficial in cutting and reducing the ductile Al particles, using the coarse alumina powder was much more effective in reaction sintering. Fused Ca-PSZ powder was reaction sintered with Al at 1550℃ for 3 hours and low shrinkage ZrO2-Al2O3 composites were fabricated. But because Al/Ca-PSZ powder mixtures were not effectively milled the reaction sintering and densification was difficult. And the Ca ion in Ca-PSZ grains diffused into alumina grains during sintering so that the unstabilization of Ca-PSZ body was occured which gave the microcracks in the specimens.

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Fabrication and Comparative Evaluation of Soybean Hull Nanofibrillated Cellulose (대두피 나노 섬유화 셀룰로오스 제작 및 비교 평가)

  • Jin-Hoon Kim;Hui-Yun Hwang
    • Composites Research
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    • v.37 no.3
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    • pp.150-154
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    • 2024
  • In this study, nanofibrillated cellulose was extracted from soybean hulls - a by-product of soybeans - and compared with soybean hull nanofibrillated cellulose obtained by using other nanofibrillated methods. Dry soybean hulls were ground into prepare micrometer-sized powders, from which microcellulose was isolated using NaOH and HCl. The nanometer-sized cellulose was successfully extracted through ultrasonic dispersion and ball milling. The soybean hull nanofibrillated cellulose exhibited a diameter of 60-100 nm and a length of 0.3-1.0 ㎛, which matches the diameter of soybean nanofibrillated cellulose made by other nanofibrillated methods but is significantly shorter in length.

고출력 LED 패키지용 고밀도 W-20wt%Cu 나노복합체 제조에 관한 연구

  • Ryu, Seong-Su;Park, Hae-Ryong;Kim, Hyeong-Tae;Lee, Byeong-Ho;Lee, Hyeok;Kim, Jin-U;Kim, Yeong-Do
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2010.05a
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    • pp.26.2-26.2
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    • 2010
  • 최근에는 차세대 조명용 후보광원인 고출력 백색 LED를 개발하기 위한 경쟁이 치열하며, 이를 위해 업체가 고심하고 있는 가장 큰 문제 중의 하나가 칩에서 발생하는 열을 어떻게 관리하는가 하는 방열의 문제이다. 따라서, LED의 가장 큰 특징인 장수명을 손해보지 않기 위해서는 칩에서 발생되고 있는 열을 외부에 확산시키기 위한 기술 개발이 필수적이다. 다양한 방열소재 중 W-Cu 복합재는 W의 낮은 열팽창계수와 Cu의 높은 열전도도로 인해 방열소재로써 유망한 소재로 주목받고 있으나, 우수한 열적 특성을 발현하기 위해서는 고치밀화를 갖는 W-Cu 복합재 제조가 우선적으로 필요하다. W-Cu 복합체는 일반적으로 액상소결법을 통해 균일한 미세조직을 얻을 수 있으나, 열팽창계수를 낮추기 위해 Cu 함량이 적어지게 되면 치밀화가 어려우며 이를 해결하기 위해 나노입자를 갖는 분말을 이용하고자 하는 연구가 많이 진행되고 있다. 본 연구에서는 W과 Cu 산화물을 이용하는 것이 구성성분끼리의 편석이 발생하지 않으며, 소결성도 우수하여 양산화에 가장 접근한 방법으로 알려져 있다. 그러나, 지금까지의 얻어진 W-Cu 복합체의 경우, 분말상태에서의 얻어진 나노입자가 승온시에 마이크로 크기로 과도한 입자성장이 일어나기 때문에 소결 후에도 나노크기를 유지하기 어려울 뿐만 아니라, 구성상끼리의 응집체가 형성된다. 본 연구에서는 액상소결후에 W 입자가 Cu 기지내에 균일하게 분산되는 동시에 나노크기의 입자를 가지는 고분산 W-Cu 소결체를 얻고자 하였다. 이를 위해 금속산화물 분말의 분쇄를 위해 효과적인 방법으로 알려진 습식상태에서의 고에너지 볼밀링을 통하여 혼합된 텅스텐과 구리 산화물 분말의 수소환원공정을 통해 얻어진 100nm 이하의 입자를 가지는 W-20wt%Cu 나노복합분말을 출발분말로 사용하였다. W-20wt%Cu 나노복합분말의 성형체를 $1050^{\circ}C-1250^{\circ}C$의 온도범위에서 소결거동을 조사하였다. 그 결과, $1100^{\circ}C$ 온도에서 이론밀도에 가까운 소결밀도를 나타내었으며, 이는 기존에 비해 $100^{\circ}C$ 정도 치밀화 온도를 낮추는 결과이다. 소결체의 미세구조 관찰결과, 소결 후 약 200nm의 텅스텐 입자가 Cu내에 균일하게 분산되어 있었다. 제조된 W-Cu 시편에 대해서는 LED 응용성을 조사하기 위해 열전도도와 열팽창계수 등을 평가하였다.

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Characteristics of Recycled Aggregate Powder Containing Mortar Depending on Grinding Efficiency (분쇄 효율에 따른 순환골재 분말 혼입 모르타르의 특성)

  • Bang, Jinwook;Jang, Youngil;Lee, Jongwon;Mun, Seokho;Chu, Hyunseung
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.23 no.2
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    • pp.116-121
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    • 2019
  • In order to evaluating applicability of RAP (recycled aggregate powder) in mortar, in this study, physical and mechanical tests was carried out. Material characteristics of recycled aggregate and RAP were evaluated and the mechanical properties of mortar replaced with RAP were analyzed. Test result of sieve analysis showed that as the milling time increased the fineness modulus was decreased and the distribution of 0.6 mm particle size was found to increase. The fluidity of mortar mixture substituted with RAP tended to increase than Plain mixture. It was result that the increasing fluidity was affected by unreacted surplus water in the mortar as the binder was replaced with RAP. From the compressive strength result of the mortar subjected to RAP, it was found that the RAP was able to replace up to about 10% of unit binder weight although the compressive strength of mortar was decreased as the RAP replacement increased. From the above study, it can be concluded that the physical properties of RAP satisfied the quality standard of aggregate for replacement with fine aggregate. Moreover, in case of the RAP was replaced up to 10% of unit cement weight, it was able to be possible to improve fluidity and compressive strength of mortar.

Exchange Decoupling Of $Fe_3$Fe_3B+Nd_2Fe_{14}B Spring Magnet Powder Compact (Fe_3B+Nd_2Fe_{14}B Spring magnet분말 압분체의 Exchange Decoupling)

  • 한종수;양충진;박언병
    • Journal of the Korean Magnetics Society
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    • v.11 no.5
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    • pp.232-238
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    • 2001
  • Experimentally it is well known that the magnetic properties significantly deteriorate when nanocomposite bonded magnet are made from nanocomposite ribbon. A decrease in maximum energy product of F $e_3$B+N $d_2$F $e_{14}$B nanocomposite from 14 MGOe in nanocomposite ribbon to 6.5 MGOe in powder compact was fecund to be general. Thus, the present study is focused on finding out the root of exchange decoupling of N $d_4$F $e_{73.5}$ $Co_3$H $f_{0.5}$G $a_{0.5}$ $B_{18.5}$ nanocomposite powder compacts. The exchange decoupling behavior of the powder compact of F $e_3$B+N $d_2$F $e_{14}$B composition was studied by measuring DC demagnetization and isothermal remanent demagnetization curves, which are essential for plotting produced $\delta$M curve. From the $\delta$M plot the deterioration in the magnetic properties resulted from the fact that the magnetostatic interaction became dominant rather thanthe exchange interaction in powder compact. It is concluded that the demagnetization behavior governed by the dominant magnetostatic interaction reduced the remanence magnetization, which caused the reduction of maximum energy Product of the powder compact. We also found that the elimination of residual stress which is unavoidably accumulated during grinding process enhanced the magnetic properties considerably.bly.bly.

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Fabrication of Electrospun Composite Membranes with Silk Powder (실크 입자가 도입된 전기방사 복합막 제조)

  • Seo, Young Jin;Kang, Hoseong;Im, Kwang Seop;Choi, Kang-min;Park, Chi Hoon;Nam, Sang Yong;Jang, Hae Nam
    • Membrane Journal
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    • v.32 no.2
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    • pp.133-139
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    • 2022
  • As the issue of reducing greenhouse gases is emerging due to global warming and extreme weather, research on materials capable of radiative cooling without energy consumption is being actively conducted. Among them, silk is known as a natural self-cooling material, but in the conventional mixing process using chemically powdered silk, there is a problem that the radiative cooling effect disappears by the collapses of the intrinsic crystal structure of silk fibroin, so it is difficult to manufacture it in the form of a film or coating agent for radiative cooling. In this study, various types of membranes were manufactured using silk powder that went through a physical pulverization process that does not damage the intrinsic structure of silk fibroin, and the study was conducted to examine its applicability as a coating agent. Electrospun membranes and flat sheet membranes were prepared by using silk fibroin powder for this purpose, and it was observed that the viscosity of the solution had a significant effect on the membrane fabrication and its properties.

Functional Magnetizing Treatment of Natural Quartz and Volcanic Lava Scoria (내추럴 퀄쯔와 화산암재 스코리아의 기능성 마그네타이징 처리)

  • 소대화;소현준;배두안;김정희
    • Journal of the Speleological Society of Korea
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    • no.63
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    • pp.1-8
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    • 2004
  • The non-magnetic materials with non-conductive showing high structure dispersity were developed on the base of natural quartz and lava-scoria which was collected from Je-ju island in Korea, and treated by methane-chemical technology those were obtained novel properties of magnetization through the analyzing. Depending on the processing conditions and subsequent applications the materials produced by strong methane-chemical reaction (MCR) in alcohol solution showed concurrently magnetic, dielectric and electrical properties. The obtained magnetic-electrical powders classified by aggregate complex of their features as segnetomagnetics, containing a dielectric material as a carrying nucleus, particularly the quartz on that surface one or more layers of different compounds were synthesized having thickness up to 10~50 nm and showing magnetic, electrical and other properties. It was confirmed in magnetizing process that powders of quartz and lava-scoria produced by MCR were better oil adsorbent as of oleophilic and floating matter on water surface although their specific gravities are comparably more than 1 in quartz or less than unity, as that of water, in lava-scoira. Therefore, it will be Possible and very useful to remove low density and light gravity oil spillage in difficult recovery from sea and inland water contamination spread on water surface, by marine accident and ship sinking accident occurring frequently in recent years, by way of magnetic adsorbent conveyer system in continuous, if it could be built up the mass Production system of water-floating magnetizable oleophilic adsorbent materials with use of iow cost and good Qualify lava-scoria spread on volcano district in Je-ju island. And, there will also be urgent advent of necessity with strong possibility to develop useful applications of various magnetic functional materials include oleophilic adsorbent for removal of sea oil-contaminants and maritime pollutants, and other kinds of various utilities in industrial applications and practical uses of novel functional materials in the fields of environments and health care applications with in deep expectation.

Processing of anchovy based powder for instant soup packed in tea bag and the taste compound of its extractives (Tea bag 포장한 멸치 복합 분말의 가공 및 그 추출물의 정미성분)

  • Lee, Ho-Yeon;Chung, Bu-Gil;Lee, Jung-Suck;Kim, Poong-Ho;Kim, Jin-Soo;Lee, Eung-Ho
    • Applied Biological Chemistry
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    • v.36 no.4
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    • pp.271-276
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    • 1993
  • This study was carried out to prepare anchovy based powder for instant soup packed in tea bag which can be used handily as a extractives, and to determine the taste compounds of extractives of anchovy based powder for instant soup. The anchovy based powder for instant soup was made by adding of 72% in the redried anchovy, 14% in the sea tangle, 7% in the mushroom and 7% in the katsuobushi to the total mixtures. And the anchovy based powder for instant soup was packed in tea bag. The desirable extraction time are 5 min in package in tea bag with air permeability $100\;m^3/m^2/min$ and over 20 min in package in tea bag with air permeability $65\;m^3/m^2/min$, respectively. Judging from the result of extraction rate of total nitrogen, color and sensory evaluation in extractives of anchovy based powder for instant soup extracted by optimal extraction time, the quality in extractives of instant soup packed in tea bag with air permeability $100\;m^3/m^2/min$ was superior to those of instant soup unpacked in tea bag and of instant soup packed in tea bag of air permeability $65\;m^3/m^2/min$. The principal taste compounds of extractives of anchovy based powder for instant soup packed in tea bag with air permeability $100\;m^3/m^2/min$ were IMP (9.26 mg/100ml in 5% solution) and free amino acids (24.30 mg/100 ml in 5% solution) such as histidine, proline, lysine and taurine. Total creatinine, betaine and TMAO were seemed to act an auxiliary role in taste of extracives of anchovy based powder for instant soup packed in tea bag with air permeability $100\;m^3/m^2/min$.

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TREATMENT OF COMPOUND COMMINUTED MANDIBULAR FRACTURES (하악골 복합 분쇄 골절의 치험례)

  • Jeong, Jong-Cheol;Kim, Keon-Jung;Choi, Jae-Sun;Sung, Dae-Kyung;Kim, Ho-Sung;Lee, Gye-Hyeok
    • Maxillofacial Plastic and Reconstructive Surgery
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    • v.20 no.2
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    • pp.101-105
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    • 1998
  • Compound comminuted mandibular fracture is defined as the presence of multiple fracture lines with open wound resulting in many small pieces within the same area. The incidence of mandibular comminution is difficult to determine but reported as 2.7~18.6 % incidence among mandibular fractures. There are controversies in the treatment of mandibular comminuted fractures. Treatment of comminuted mandibular fracture has traditionally involved closed reduction in an effort to avoid stripping periostcum from the bony segments, but rigid internal rigid fixation is used more popular at present. The extent of comminution, displacement of bony fragments and patient general conditions are important factors in decision of the treatment methods. When significant bone displacement is present, it is necessary to reduce these comminuted fragments to an anatomic, pretraumatic relationship to restore facial form and function. In these cases, ORIF allows anantomic reduction of comminuted segments as well as pretraumatic occlusion. Gentle handling of the soft tissue, rigid fixation of bony fragments and adequate immobilization are essential for reducing the complications. This is the report the incidence, causes, complications and treatment of the patients who visited our department for compound comminuted mandibular fractures.

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