• 전기의세계
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• v.53 no.8
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• pp.20-23
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• 2004

현재 사용되고 있는 전자디바이스 소자의 기능은 급속도로 변화하고 있는 정보화 사회로의 진입이라는 시대적 요구와 함께 필요한 기능과 수요를 확보하기 위하여 지속적으로 발전하고 있다. 현재까지 연구개발 결과로 몰리브덴과 실리콘으로부터 전계에 의한 전자 방출을 응용한 Flat pannel display (FPD)의 실현 가능성은 확보하였으나, 전극의 첨예화를 기하는 기술이 아직 까지 개발 도상 단계에 있으며, 소자의 경량화와 저전압 구동의 실현을 위하여 해결하여야 할 많은 과제를 안고 있다. (중략)

• Journal of the Korean Society for Nondestructive Testing
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• v.18 no.1
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• pp.33-41
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• 1998

The response characteristics of the PZT transducers during glass capillary breakage were studied at the epicenter of the glass plate. The PZT transducers had been made by using EC-65 PZT ceramics(supplied by Edo co.) with a constant area and a various thickness. The theoretical displacement and velocity at the epicenter of glass plate with an air boundary condition were calculated by assuming the point load of 1N force strength and a rise time of 280 ns with a ramped functional dependence, and the 1st pulses of the PZT transducer may be considered as the vertical velocity incident on the electrode of the PZT ceramic. The responses of the PZT transducer may be depended on the thickness mode of the PZT ceramic below 0.33 in the ratio of the thickness to the diameter of PZT ceramic, but the reponse of the PZT transducer may be depended on the other modes of PZT transducer in the addition of the thickness mode of the PZT ceramic above 0.33. The full time of half maximum at the 1st pulse was nearly 280 ns without a variation of applied breakage load and the resonant frequency of the PZT transducer, and then may be considered as the rise time of a AE source. The maximum amplitude of the 1st pulse depended on the incident vertical velocity and capacitance of the PZT transducer. Therefore, the full time of half maximum and maximum amplitude of the 1st pulse may be considered as the rise time and strength of acoustic emission source respectively.

• Polymer(Korea)
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• v.27 no.5
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• pp.464-469
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• 2003

In this work, the fragrant oil release behavior of poly($\varepsilon$-caprolactone) (PCL) microcapsules containing SiO$_2$ was investigated. The SiO$_2$ was chemically treated in 10, 20, and 30 wt% hydrochloric acid and sodium hydroxide. The acid and base values were determined by Boehm's titration technique and $N_2$/77 K adsorption isotherm characteristics, the specific surface area and total pore volume were studied by BET. The PCL microcapsules containing SiO$_2$ and fragrant oil were prepared by oil-in-water (o/w) emulsion solvent evaporation method. The shape and surface of PCL microcapsules were observed using image analyzer and scanning electron microscope (SEM). The fragrant oil release behavior of PCL microcapsules was characterized using UV/vis. spectra. The average diameters of PCL microcapsules were decreased from 35 to 21 $\mu$m with increasing stirring rate. It was found that in the case of acidic treatment the fragrant oil adsorption capacity and release rate were increased due to the increase of specific surface area and acid value. In the case of basic treatment, the fragrant oil adsorption capacity and release rate were decreased due to the decrease of sp ecific surface area and the increase of acid-base interactions between SiO$_2$-NaOH and fragrant oil with increasing base value of SiO$_2$.

• Journal of the Korean Chemical Society
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• v.26 no.2
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• pp.88-94
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• 1982

The concentrations of gaseous ammonia and particulate ammonium emitted from a urea plan were measured, and the conversion rate of ammonia to ammonium was estimated. The conversion of ammonia to ammonium has two stages with transport time in the atmosphere. In the initial 15min the conversion rate was 3.2% min$^{-1}$, and thereafter 0.26% min$^{-1}$. The high conversion rate of ammonia to ammonium at the initial period of it's transport might be due to the dissolution of ammonia into water droplets formed by the decrease in temperature of the stack effluent. The concentration of ammonium is further increased by the decomposition of urea in alkaline droplet formed. Half-lives of ammonia gas at initial and latter slag were 16 min and 192 min respectively. No correlation of particulate ammonium concentration to temperature, relative humidity, and concentrations of sulfur dioxide, nitrogen oxides and airborne particulate matter were found in this field measurement.

• Journal of the Korean Society for Nondestructive Testing
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• v.23 no.3
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• pp.237-245
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• 2003

Since the velocity is dependent on the fiber orientation in anisotropic composites, the application of traditional acoustic emission (AE) source location techniques based on the constant velocity to composite structures has been practically impossible. The anisotropy makes the source location procedure complicated and deteriorates the accuracy of the location. In this study, we have divided the region of interest(ROI) into a set of finite elements, taken each element as a virtual source, and calculated the arrival time differences between sensors by using the velocities at every degree from 0 to 90. The calculated and the experimentally measured values of the arrival time difference aye then compared to minimize the location error. The results from two different materials, namely AA6061-T6 and CFRP(uni-directional; UD, $[0]_{32}4$) laminate confirmed the practical usefulness of the proposed method.

• Journal of Adhesion and Interface
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• v.9 no.2
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• pp.1-7
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• 2008

Using biodegradable polycaprolactone, the microcapsules were prepared by solvent evaporation method. Retinol was selected as a core material, which was used as an important ingredient material in cosmetic fields. Poly(vinyl alcohol) was used as a stabilizer. The shape and property of the microcapsules were characterized by scanning electron microscope and differential scanning calorimeter, and the release rate of the microcapsule was measured by UV spectrophotometer. The microcapsules were prepared, changing the concentration of wall material, the stirring rate, and the concentration of stabilizer. Under the optimum condition, the microcapsules were formed, which showd 5~6 um in diameter and got the homogeneous sphere shape.

• Proceedings of the Membrane Society of Korea Conference
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• 1991.04a
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• pp.1-4
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• 1991

고분자와 희석제 간의 interaction은 phase diagram의 형태로 결정하고 상분리 mechanism은 phase diagram에 의해 설명된다. Thermodynamic interaction이 TIPS 분리막의 구조에 미치는 영향을 조사하기 위하여 PP/C20alkane, PP/C20acid, PP/TA 3가지 system을 선택하였다. 200$^{\circ}$C에서 25 $^{\circ}$C로의 급냉과 분당 10 $^{\circ}$C의 냉각조건을 적용하였다. 각 phase diagram의 형태와 냉각조건에 따라 상분리 mechanism이 달라져서 서론에서 언급한 바와 같이 각기 특유의 구조를 갖게됨을 확인하였다. 같은 종류의 희석제의 chain length가 분리막의 구조에 미치는 영향을 조사하였다. 희석제의 chain length에 따라 결정화 온도가 달라지며 PP와의 결정화 속도 차이에 의하여 구조가 다양하게 변화되었다. 또한 가 희석제의 확산계수의 차이에 의하여 PP 결정화 시 희석제의 외부 방출 정도가 달라 이에 의한 구조의 차이도 관찰되었다. TIPS 공정에서 용액의 조성이 분리막의 구조에 미치는 영향을 조사하였는데, 조성에 의한 nucleation density의 차이에 따라 PP spherulite의 충돌 (impingment)등이 구조에 영향을 미쳤으며 porosity도 변화하였다. 또한 PP/TA system에서는 조성에 따라 상분리 mechanism이 달라져 현격한 구조의 차이를 보였다. 또한 냉각 속도에 따라 PP spherulitic structure가 변화함을 확인하였고, PP 결정화에 따른 희석제의 방출에 의하여 interspherulitic과 intraspherulitic pore를 갖는 2중 구조를 갖게 됨을 알 수 있다.

• Journal of the Korean Society for Nondestructive Testing
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• v.33 no.5
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• pp.436-442
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• 2013

Friction welding is a very useful joining process to weld metals which have axially symmetric cross section. In this paper, the feasibility of industry application was determined by analyzing the mechanical properties of weld region for a specimen of tube-to-tube shape for excavator hose nipple with friction welding, and optimized welding variables were suggested. In order to accomplish this object, friction heating pressure and friction heating time were selected as the major process variables and the experiment was performed in three levels of each parameter. An acoustic emission(AE) technique was applied to evaluate the optimal friction welding conditions nondestructively. AE parameters of accumulative count and event were analyzed in terms of generating trend of AE signals across the full range of friction weld. The typical waveform and frequency spectrum of AE signals which is generated by friction weld were discussed. From this study the optimal welding variables could be suggested as rotating speed of 1300 rpm, friction heating pressure of 15 MPa, and friction heating time of 10 sec. AE event was a useful parameter to estimate the tensile strength of tube-to tube specimen with friction weld.

• Polymer(Korea)
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• v.27 no.5
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• pp.449-457
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• 2003

The purposes of this work were the producing of a biodegradable poly($\varepsilon$-caprolactone) (PCL) / poly(ethylene oxide) (PEO) microcapsule and the analyzing of form and features for the manufacturing conditions which could be observed in a prospective drug delivery systems through drug release. The effects of emulsifier, emulsifier concentration, and stirring rate for the diameter and form of the microcapsules were observed using image analyzer and scanning electron microscope. The role of interfacial adhesion between PCL/PEO and drug was determined by contact angle measurements, and the drug release test of the microcapsules was characterized by UV/vis. spectra. As a result, the microcapsules were made in spherical fonns with a mean particle size of 170 nm∼68 $\mu$m. And the work of adhesion between water and PCL/PEO increased with increasing the content of PEO, probably due to the increased the hydrophilicity. It was also found that the drug release rate from the microcapsules significantly increased with increasing the content of PEO, which could be also attributed to the increasing of the hydrophilic groups or the degree of adhesion force at interfaces.

• Korean Journal of Weed Science
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• v.10 no.2
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• pp.122-129
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• 1990

The herbicide $^{14}C$-butachlot[N-(butoxymethyl)-2-chloro-2', 6'-diethylacetanilide] labelled uniformly in benzene ring was incorporated in alginate-based granules to get controlled release properties. The influence of kaoline addition on the formulation characteristics and release profiles were evaluated under a closed dark and an opened sunlight condition. Incorporation efficiency of $^{14}C$-butachlor in alginate-kaoline matrices was over 91.8%. Formulation yield was decreased with increase of kaoline concentration. The release rate from all the granules prepared with alginate was slower than that from the commercial granule impregnated in zeolite. The release rate from the granule containing kaoline was decreased as the kaoline content was increased under both conditions. Losses of butachlor from the leacheate solution of the alginate-kaoline matrices under an opened sunlight condition was diminished by increasing the kaoline content.