• Title/Summary/Keyword: 반응 조건 최적화

Search Result 744, Processing Time 0.031 seconds

Optimization of Crude Papain Extraction from Papaya Latex Using Response Surface Methodology (반응표면 분석법에 의한 crude papain 추출 조건의 최적화)

  • Oh, Hoon-Il;Oh, Sang-Joon;Kim, Jeong-Mee
    • Korean Journal of Food Science and Technology
    • /
    • v.29 no.3
    • /
    • pp.509-515
    • /
    • 1997
  • Crude papain was extracted from papaya latex under various conditions. Extraction conditions of crude papain were optimized by the response surface methodology (RSM). Extraction yield of papain was affected by concentration of $NaHSO_3$, extraction time and pH. Three independent factors were chosen to determine their effects on the various responses and the function was expressed in terms of a quadratic polynomial equation, which measures the linear, quadratic and interaction effects. According to the results of RSM, the stationary point for quantitatively dependent variable was found to be the maximum point for extraction yield. Optimum conditions of papain extraction were 4% of $NaHSO_3$, 120 min of extraction time and pH 7.6. Under these conditions, 793.16 mg of papain per g latex was extracted from papaya latex.

  • PDF

소형 산화 장치를 이용한 공급 유량별 $UO_2$ Pellet 산화 연구

  • 엄재법;김영환;윤지섭;정운관
    • Proceedings of the Korean Radioactive Waste Society Conference
    • /
    • 2005.06a
    • /
    • pp.406-407
    • /
    • 2005
  • 사용후핵연료 차세대관리공정에서는 $UO_2$ 펠렛을 균질화된 $U_{3}O_8$의 분말 형태로 되어야만 금속 전환공정에서 반응효율을 높일 수 있다. 본 연구에서는 실증용 건식분말화 장치에서 분말의 비산을 방지하면서 산화 효율을 최대한 높일 수 있는 최적 조건을 찾는데 있다고 할 수 있다. 본 연구의 실험에서 $UO_2$ 펠렛(약 90 g)에 유량별 공정 변수를 주어 최적화된 산화 조건을 조사하였다. 그 결과, $500^{\circ}C$ 에서 유량은 이론 산화량의 2배(1640 cc/min)의 조건에서 최적의 산화 효율을 보여주었다. 따라서 본 연구에서 실증용 건식분말화 장치의 비산을 방지하면서 산화 효율을 최대한 높일 수 있는 최적 유량을 결정하였다.

  • PDF

Optimization of Supercritical Water Oxidation(SCWO) Process for Decomposing Nitromethane (Nitromethane 분해를 위한 초임계수 산화(SCWO) 공정 최적화)

  • Han, Joo Hee;Jeong, Chang Mo;Do, Seung Hoe;Han, Kee Do;Sin, Yeong Ho
    • Korean Chemical Engineering Research
    • /
    • v.44 no.6
    • /
    • pp.659-668
    • /
    • 2006
  • The optimization of supercritical water oxidation (SCWO) process for decomposing nitromethane was studied by means of a design of experiments. The optimum operating region for the SCWO process to minimize COD and T-N of treated water was obtained in a lab scale unit. The authors had compared the results from a SCWO pilot plant with those from a lab scale system to explore the problems of scale-up of SCWO process. The COD and T-N in treated waters were selected as key process output variables (KPOV) for optimization, and the reaction temperature (Temp) and the mole ratio of nitromethane to ammonium hydroxide (NAR) were selected as key process input variables (KPIV) through the preliminary tests. The central composite design as a statistical design of experiments was applied to the optimization, and the experimental results were analyzed by means of the response surface method. From the main effects analysis, it was declared that COD of treated water steeply decreased with increasing Temp but slightly decreased with an increase in NAR, and T-N decreased with increasing both Temp and NAR. At lower Temp as $420{\sim}430^{\circ}C$, the T-N steeply decreased with an increase in NAR, however its variation was negligible at higher Temp above $450^{\circ}C$. The regression equations for COD and T-N were obtained as quadratic models with coded Temp and NAR, and they were confirmed with coefficient of determination ($r^2$) and normality of standardized residuals. The optimum operating region was defined as Temp $450-460^{\circ}C$ and NAR 1.03-1.08 by the intersection area of COD < 2 mg/L and T-N < 40 mg/L with regression equations and considering corrosion prevention. To confirm the optimization results and investigate the scale-up problems of SCWO process, the nitromethane was decomposed in a pilot plant. The experimental results from a SCWO pilot plant were compared with regression equations of COD and T-N, respectively. The results of COD and T-N from a pilot plant could be predicted well with regression equations which were derived in a lab scale SCWO system, although the errors of pilot plant data were larger than lab ones. The predictabilities were confirmed by the parity plots and the normality analyses of standardized residuals.

Optimization of Performances in GaN High Power Transistor Package (질화갈륨 고출력 트랜지스터 패키지의 성능 최적화)

  • Oh, Seong-Min;Lim, Jong-Sik;Lee, Yong-Ho;Park, Chun-Seon;Park, Ung-Hee;Ahn, Dal
    • Journal of the Korea Academia-Industrial cooperation Society
    • /
    • v.9 no.3
    • /
    • pp.649-657
    • /
    • 2008
  • This paper describes the optimized output performances such as output power and the third order intermodulation in GaN high power transistor packages which consist of chip die, chip capacitors, and wire bonding. The optimized output power according to wire bonding techniques, and third order intermodulation performances according to wire bonding and bias conditions are discussed. In addition, it is shown through the nonlinear simulation that how the output performances are sensitive to the inductance values which are realized by wire bonding for matching network in the limited package area.

Calibration of Parameters in QUAL2E using the Least-squares Method (최소지승법에 의한 QUAL2E 모델 반응계수 보정)

  • Kim, Kyung-Sub;Yoon, Dong-Gu;Lee, Gi-Young
    • Journal of Korea Water Resources Association
    • /
    • v.37 no.9
    • /
    • pp.719-727
    • /
    • 2004
  • Water quality models can be applied to manage the regional water quality problems and to estimate the target and allowable pollution load in watershed effectively. The optimization of state variables in the given water quality model Is necessary to build up more effective model. The least-squares method is applied to fit field observations in QUAL2E developed by U.S. EPA, which is most widely used one in the world to simulate the stream water quality, and the optimization model with constraints is constructed to estimate the parameters. The objective function of the optimization model is solved by Solver in Microsoft Excel and Monte Carlo simulation is conducted to know the influence of parameter in conventional pollutants. It is found that this technique is easily implemented and rapidly convergent computational procedure to calibrate the parameters after appling this approach in Anyang stream located in Kyonggi province mainly.

Development of an Automated Aero-Structure Interaction System for Multidisciplinary Design Optimization for the Large AR Aircraft Wing (가로세로비가 큰 항공기 날개의 다분야 통합 최적설계를 위한 자동화 공력-구조 연계 시스템 개발)

  • Jo, Dae-Sik;Yoo, Jae-Hoon;Joh, Chang-Yeol;Park, Chan-Woo
    • Journal of the Korean Society for Aeronautical & Space Sciences
    • /
    • v.38 no.7
    • /
    • pp.716-726
    • /
    • 2010
  • In this research, design optimization of an aircraft wing has been performed using the fully automated Multidisciplinary Design Optimization (MDO) framework, which integrates aerodynamic and structural analysis considering nonlinear structural behavior. A computational fluid dynamics (CFD) mesh is generated automatically from parametric modeling using CATIA and Gambit, followed by an automatic flow analysis using FLUENT. A computational structure mechanics (CSM) mesh is generated automatically by the parametric method of the CATIA and visual basic script of NASTRAN-FX. The structure is analyzed by ABAQUS. Interaction between CFD and CSM is performed by a fully automated system. The Response Surface Method (RSM) is applied for optimization, helping to achieve the global optimum. The optimization design result demonstrates successful application of the fully automated MDO framework.

A Study on Optimization of Welding Process Variables in MIG Welding of Aluminum Alloy Sheets for automotive door (자동차 Door용 박판 알루미늄합금의 MIG 용접공정변수 최적화에 관한 연구)

  • Lee, Young-Gi;Han, Hyun-Uk;Kim, Jae-Seong;Lee, Bo-Young;Kim, Cheol-Hee
    • Proceedings of the KWS Conference
    • /
    • 2009.11a
    • /
    • pp.28-28
    • /
    • 2009
  • 최근 전세계적으로 유가 상승 및 배기가스 배출 저감과 관련된 각종 환경규제에 대응하기 위하여 선진 자동차회사들은 $CO_2$ 배출 저감 기술과 기존 내연기관 차량의 연비향상을 위해 엔진성능 개선, 구동시스템의 최적화, 차량 경량화, 공기저항 감소 등에 초점을 맞춰 차량의 연비향상과 배기가스 규제에 대응하고 있다. 특히, 자동차 중량의 30%를 차지하는 차체의 경량화는 엔진효율을 높여 자동차의 성능향상을 극대화시키고, 그로 인해 연비향상을 도모할 수 있으므로 환경오염 방지와 연료절감에 가장 적합하고 효과적인 방법이다. 이에 기존의 강재에 비해 비중이 낮으면서 유사한 강도와 내식성이 뛰어난 알루미늄 합금의 차체 적용에 대한 연구가 진행되고 있다. 본 연구에서는 자동차 Door에 알루미늄 합금(Al 5052)의 적용 가능성을 판단하기 위해 반응표면분석법(Response surface methodology)을 이용하여 저입열 Pulse MIG 용접 공정변수를 최적화하였다. 첫째, 저입열 Pulse MIG 용접에서 용접 공정 변수(용접전압, 용접속도, Gap)의 변화가 비드 형상에 미치는 영향에 대해 평가하였다. 요인분석법을 이용하여 용접 공정 변수와 비드 형상 변수와의 주효과와 교호작용효과를 분석하였고, 이를 통해 비드 형상 변수에 영향을 크게 미치는 용접 공정변수를 선별하여 다중회귀분석을 통해 용접 공정 변수 변화에 따른 비드형상 예측 회귀모델을 제안하였다. 둘째, 자동차 Door 생산 현장에서 박판 알루미늄 합금 겹치기 용접 이음부의 0~1 mm 갭 발생에 대해 강건한 용접조건을 제시하기 위해 반응표면법(Response surface methodology)을 이용하여 저입열 Pulse MIG 용접 공정 변수를 최적화하였고, 그 적용 가능성을 확인하였다.

  • PDF

Optimization on the Stability of Coconut Oil in Water Emulsion Using Response Surface Methodology (반응표면분석법을 이용한 Coconut Oil 원료 O/W 유화액의 유화안정성 최적화)

  • Yoo, Bong-Ho;Zuo, Chengliang;Lee, Seung Bum
    • Applied Chemistry for Engineering
    • /
    • v.30 no.5
    • /
    • pp.530-535
    • /
    • 2019
  • In this study, an optimization for the emulsification process with coconut oil and sugar ester was performed in conjunction with the central composite design (CCD) model of response surface methodology (RSM). Response values for the CCD model were the viscosity of the emulsion, mean droplet size, and emulsion stability index (ESI) after 7days from the reaction. On the other hand, the emulsification time, emulsification rate, and amount of emulsifier were selected as quantitative factors. According to the result of CCD, optimum conditions for the emulsification were as follows; the emulsification time of 22.63 min, emulsification speed of 6,627.41 rpm, and amount of emulsifier of 2.29 wt.%. Under these conditions, the viscosity, mean droplet size, and emulsion stability index (ESI) after 7 days from reaction were estimated as 1,707.56 cP, 1877.05 nm, and 93.23%, respectively. The comprehensive satisfaction of the CCD was indicated as 0.8848 with an average error of $1.2{\pm}0.1%$ from the experiment compared to that of the theoretical one. Overall, a very low error rate could be obtained when the central composite model was applied to the optimized coconut oil to water emulsification.

Optimization and Characteristics of Removal Condition of Livestock Wastewater Using a Photocatalytic Process (광촉매공정 적용시 축산폐수의 처리특성 및 최적화)

  • Park, Jae-Hong
    • Clean Technology
    • /
    • v.13 no.3
    • /
    • pp.222-227
    • /
    • 2007
  • The photocatalytic degradation of livestock wastewater has been investigated over $TiO_2$ photocatalysts irradiated with a ultraviolet (UV) light. The effect of operational parameters, i.e., distance, reaction area, concentration of suspended solids(SS), and column diameter on the degradation of livestock wastewater has been performed in lab-scale. The optimal conditions for livestock wastewater were determined: distance was 3 cm (less than 7 cm), reaction area was $3.6\;m^2$, SS concentration was 40 mg/L (less than 300 mg/L) and column diameter was 5 mm (less than 10 mm). Under the optimal conditions, COD, color and coliform removal efficiencies were approximately 49%, 53% and 100%, respectively. Non-biodegradable COD removal efficiency increased with 57% using by photocatalysis process. Therefore, it is shown that photocatalysis has an effect on degradation of non-biodegradable organic matter.

  • PDF

Emulsion Grafting of Glycidyl Methacrylate onto Plasma-treated Polypropylene Surface (플라즈마 처리된 폴리프로필렌 표면 위에 글리시딜메타크릴레이트의 에멀젼 그래프팅)

  • Ji, Han-Sol;Liu, Xuyan;Choi, Ho-Suk;Kim, Jae-Ha;Park, Han-Oh
    • Polymer(Korea)
    • /
    • v.36 no.1
    • /
    • pp.65-70
    • /
    • 2012
  • Glycidyl methacrylate (GMA) was used to introduce epoxy groups on the surface of polypropylene (PP) plate, used as a substrate, through plasma-induced graft copolymerization. Emulsion polymerization was applied for graft copolymerization of GMA and was compared with conventional solution polymerization to confirm its effect. Plasma treatment conditions under one atmospheric pressure were fixed as follows; the RF power of 200 W, the treatment time of 30 sec, the Ar gas flow rate of 6 LPM, and the exposure time of treated PP samples in air of 5 min. For graft-copolymerization, GMA concentration, reaction temperature, and reaction time was optimized to maximize the grafting degree of GMA. The maximum grafting degree of GMA was obtained at the condition of 12%-GMA concentration, $90^{\circ}C$ reaction temperature, and 5 hr-reaction time. Analysis results supported that the emulsion polymerization was more effective than the solution polymerization for grafting more GMAs on the surface of PP plate under the same reaction conditions.