• Title/Summary/Keyword: 면처리

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Determination of Oxycarboxin Residues in Agricultural Commodities Using HPLC-UVD/MS (HPLC-UVD/MS를 이용한 농산물 중 Oxycarboxin의 분석)

  • Choung, Myoung-Gun
    • Korean Journal of Environmental Agriculture
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    • v.37 no.2
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    • pp.117-124
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    • 2018
  • BACKGROUND: Oxycarboxin(5,6-dihydro-2-methyl-N-phenyl-1,4-oxathiin-3-carboxamide-4,4-dioxide) as oxanthiin is a systemic fungicide commonly used for control of various pathogens in agronomic and horticultural crops. In an effort to develop an analytical method to trace the fungicide, a method using HPLC equipped with UVD/MS was studied. METHODS AND RESULTS: Oxycarboxin was extracted with acetone from hulled rice, soybean, Kimchi cabbage, green pepper, and apple samples. The extract was diluted with saline water, followed by liquid-liquid extraction with methylene chloride. Florisil column chromatography was employed for the purification of the extracts. Oxycarboxin was determined on a Zorbax SB-AQ $C_{18}$ column by HPLC with UVD. Accuracy of the proposed method was validated by the recovery tests from crop samples fortified with oxycarboxin at 3 levels per crop. CONCLUSION: Mean recoveries ranged from 78.3% to 96.1% in five representative agricultural commodities. The coefficients of variation were less than 10%, and limit of quantitation of oxycarboxin was 0.04 mg/kg. A confirmatory technique using LC/MS with selected-ion monitoring was also provided to clearly identify the suspected residue. The method was reproducible and sensitive to determine the residue of oxycarboxin in agricultural commodities.

Towards Real Time Detection of Rice Weed in Uncontrolled Crop Conditions (통제되지 않는 농작물 조건에서 쌀 잡초의 실시간 검출에 관한 연구)

  • Umraiz, Muhammad;Kim, Sang-cheol
    • Journal of Internet of Things and Convergence
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    • v.6 no.1
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    • pp.83-95
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    • 2020
  • Being a dense and complex task of precisely detecting the weeds in practical crop field environment, previous approaches lack in terms of speed of processing image frames with accuracy. Although much of the attention has been given to classify the plants diseases but detecting crop weed issue remained in limelight. Previous approaches report to use fast algorithms but inference time is not even closer to real time, making them impractical solutions to be used in uncontrolled conditions. Therefore, we propose a detection model for the complex rice weed detection task. Experimental results show that inference time in our approach is reduced with a significant margin in weed detection task, making it practically deployable application in real conditions. The samples are collected at two different growth stages of rice and annotated manually

Modification of MUSCL Scheme for Application of Non-uniform Grid (비정형격자의 적용을 위한 MUSCL 기법의 수정)

  • Kim, Byung-Hyun;Han, Kun-Yeon
    • Journal of Korea Water Resources Association
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    • v.43 no.1
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    • pp.105-117
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    • 2010
  • This paper presents a new and simple technique to perform MUSCL reconstruction for solving 2D shallow water equations. The modified MUSCL scheme uses weighted area ratio to apply non-uniform grid in stead of the previous method that equally distributed the difference of conservation variables to each interface. The suggested method can physically reconstruct conservation variables in case of uniform grid as well as non-uniform grid. In this study, Unsplit scheme applicable to unstructured grid is used and efficient slope limiter of TVD scheme is used to control numerical oscillation which can be occurred in modified MUSCL scheme. For accurate and efficient treatment of bed slope term, the modified MUSCL scheme is coupled with the surface gradient method. The finite volume model applied to suggested scheme is verified through a comparison between numerical solution and laboratory measurements data such as the simulations of isolated building test case and Bellos's dam break test case.

A Study on the Educational material Using Integrated Media (인터그레이티드 미디어 교육교재에 관한 연구)

  • 이영희
    • Archives of design research
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    • v.12 no.3
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    • pp.5-14
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    • 1999
  • In this competitive environment which changes rapidly na extensively we can perceive that the role of education is getting important more and more. The challenge that we face is how we can handle the information and convert it to the knowledge. A lot of schools have already tried to improve the effect of education by using the computers. Besides providing the content of education newly and interestingly the educational use of the integrated Media has a strong point in terms of efficiency and effectiveness that it is excellent in storage, communication, control and handling enormous information as well as in a peculiarity of reciprocity, the high usefulness of communicative education using the experience of vision, audition and simulation in the method of participating of students themselves in education that the previous media systems didn't have. This thesis brought up a substantial problem in producing the consequences of education for children by investigating the psychological and recognitional abilities of children and by understanding the essence of the Integrated Media. And this study provided the solution in terms of the content and the viewpoint in design to raise the educational efficiency and effectiveness of the Integrated Media even though it is just a partial solution.

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A Study on the Effects of Retardation with Pb in the Biofilter (생물여과층에 의한 납의 이동억제효과에 관한 연구)

  • 이문현;이재영;최상일
    • Journal of Korea Soil Environment Society
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    • v.5 no.2
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    • pp.99-105
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    • 2000
  • The purpose of this study was to show the application of the Biofilter for treatment of the soil contaminated by lead and to investigates the effect of the biofilter on the retardation of lead with pilotplants that were simulated with different media and the number of bed. and to testify the inoculation by seeding microbes. The ratio of the degradation of soil contaminant was verified as CODcr/TOC in order to find a variation of the stabilization index in soil. The Biofiltration was one of biological processing methods for treatment. The contaminants were transported through the biofilter that was filled with the media. The surface of media formed biofilm which was surrounded by microbes and through its boundary, some materials were exchanged and migrated into the cell of microbes in an orderly manner. To investigate the effect of the Biofiltration, contaminated soil with lead nitrate of 1000mg/kg in dry was made artificially. The tests were simulated such as compost, Bioceramic and compost with bioceramic by 7:3 in weight. The bed consisted of three layers in order to find effect of the number of bed. Aspergillus niger was used as a biosorbent could probe the effect on the retardation of lead.

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Effect of temperature on fractional precipitation for paclitaxel purification

  • Jeon, Soon-Yim;Kim, Jin-Hyun
    • 한국생물공학회:학술대회논문집
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    • 2005.04a
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    • pp.355-359
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    • 2005
  • Fractional precipitation is a simple, efficient method for pre-purifying paclitaxel from plant cell cultures. The storage temperature of factional precipitation was optimized in terms of the yield and purity of paclitaxel with a fixed methanol concentration in water (61.5%, v/v), paclitaxel content in the crude extract (0.5%, w/v), and storage time (3 days). The greatest yield $({\sim}84%)$ was obtained with storage at a constant temperature $(0^{\circ}C)$ for 3 days. Conversely, the highest purity $({\sim}79%)$ was obtained with stepwise reduction in temperature over 3 days. For a constant storage temperature, the maximum purity $({\sim}67%)$ was obtained at $0^{\circ}C$. There was little difference in the yield of paclitaxel between -20 and $12^{\circ}C$. This pre-purification process serves to minimize solvent usage, and the size and complexity of the high-performance liquid chromatography (HPLC) operation required for paclitaxel purification.

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A Study on the Thermal Coefficient Measurements of Special Steel by ESPI at High Temperature (고온에서 ESPI에 의한 특수강의 열팽창계수 측정에 관한 연구)

  • Kim, K.S.;Yang, S.P.;Kim, H.S.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.13 no.2
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    • pp.20-30
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    • 1993
  • Electric Speckle Pattern Interferometry (ESPI) using a CW-laser, a video system and an image processor was applied to the thermal coefficient measurements on free thermal expansions at high temperatures : ESPI provides the distribution of in-plane displacement resolved in a preselected direction. ESPI retains the merits of little or no surface preparation, no contact with the surface and the real-time presentation of interference fringes. Appling ESPI at high temperatures, several problem which caused the reduction of fringe visibility were encountered. The problem on the turbulence in the hot air surrounding high temperature objects will be solved by using a vacuum chamber. The background radiations from the objects were suppressed considerably by an interference filter. The problem on the oxidation of the object surface could't be solved. The interference fringe, whose spacings were calculated by FFT to avoid human error, were observable up to $800^{\circ}C$. The results measured by ESPI were nearly equal to the data which have already been published, up to about $800^{\circ}C$.

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Measurement of Dose Distribution in Small Beams of Philips 6 and 8 MVX Linear Accelerator (Philips LINAC 6 MV와 8 MV X선 소조사연에 대한 선량분포 측정)

  • Suh Tae-suk;Yoon Sei Chul;Shinn Kyung Sub;Park Yong Whee
    • Radiation Oncology Journal
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    • v.9 no.1
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    • pp.143-152
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    • 1991
  • The work suggested in this paper addresses a method for collecting beam data for small circular fields. Beam data were obtained from philips 6 and 8 MV LINAC at Dept. Radiation Therapy at Gainesville Incorporated and Shands Teaching Hospital. Specific quantities measured include tissue maximum ratio (TMR), off-axis ratio (OAR) and relative output factor (ROF) In small field irradiation, special collimators were used to produce circular fields of 1 cm to 3 cm diameter in 2 mm steps, measured at SAO (soura axis distance) of 100 cm. Diode detector was chosen for primary beam measurement and compared with measurements made with photographic film and TLD dosimeters. The measured TMRs and OARs were formulated from limited measurements to generate basic beam data for reference set-up. The empirical formula were later, extended and generalized for any possible set-up using the trends of fitting parameters. The measured TMRs and OARs were well represented by the fitting formula developed.

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Effects of Seeding Times on the Growth Characteristics and Seed Productivity of Orchardgrass (Dactylis glomerata L.) (파종시기가 오차드그라스의 생육특성 및 종자생산에 미치는 영향)

  • 최기준;정의수;임용우;임영철;김기용;성병렬;김맹중;박근제
    • Journal of The Korean Society of Grassland and Forage Science
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    • v.23 no.2
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    • pp.101-106
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    • 2003
  • This experiment was carried out to investigate the growth characteristics and seed productivities of orchardgrass "Hwabsung 2 ho" according to seeding times in the NLRI from 2001 to 2002. The experimental design was a randomized block arrangement with three replications. Seed was sown on 10th, 20th, and 30th of Aug. and 10th, 20th, and 30th of Sept. in 2000 and 2001, respectively. Establishment of seedling was worse in seeding of Aug. 10th because of rainfall. Number of panicles per $1\textrm{m}^2$ was numerous in seeding of Aug. 20th and was fewer according as seeding time was later. But panicle did not nearly appear in seeding after Sept. 20th. Seeding of Aug. 20th produced seed yield of 759kg/ha and have most seed yield components. But according as seeding times were later than Aug. 20th, the seed yield was linearly decreased with seed yield components worse.nts worse.

Adaptive Spatio-Temporal Prediction for Multi-view Coding in 3D-Video (3차원 비디오 압축에서의 다시점 부호화를 위한 적응적 시공간적 예측 부호화)

  • 성우철;이영렬
    • Journal of Broadcast Engineering
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    • v.9 no.3
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    • pp.214-224
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    • 2004
  • In this paper, an adaptive spatio-temporal predictive coding based on the H.264 is proposed for 3D immersive media encoding, such as 3D image processing, 3DTV, and 3D videoconferencing. First, we propose a spatio-temporal predictive coding using the same view and inter-view images for the two TPPP, IBBP GOP (group of picture) structures 4hat are different from the conventional simulcast method. Second, an 2D inter-view direct mode for the efficient prediction is proposed when the proposed spatio-temporal prediction uses the IBBP structure. The 2D inter-view direct mode is applied when the temporal direct mode in B(hi-Predictive) picture of the H.264 refers to an inter-view image, since the current temporal direct mode in the H.264 standard could no: be applied to the inter-view image. The proposed method is compared to the conventional simulcast method in terms of PSNR (peak signal to noise ratio) for the various 3D test video sequences. The proposed method shows better PSNR results than the conventional simulcast mode.