• Title/Summary/Keyword: 메타미포프

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The Occurrence of the Weeds on the Lawn and the Effective Control System (잔디밭잡초 발생현황과 방제기술)

  • Lee, In-Yong;Kim, Chang-Seok;Lee, Jeongran;Park, Nam-Il;Park, Jae-Eup
    • Weed & Turfgrass Science
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    • v.2 no.2
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    • pp.111-121
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    • 2013
  • Literatures were reviewed to understand the weeds occurring on the lawn and the effective control methods of them. Thirty-seven species of 16 families including three species of Cyperaceae for example Cyperus sanguinolentus, nine species of Poaceae including Digitalis ciliaris, Poa repens, etc., and 25 species of broad-leaved weeds such as Artemisia princeps, Draba nemorosa, Hydrocotyle sibthorpioides were occurred on the lawns. One hundred ninety-six weed species of 53 families were occurred on a tomb graveyard adjacent to the mountain. Therefore, it is possible to be infested by the weeds occurring on the graveyard on the golf course adjacent to the mountains. There are 67 items, 32 kinds of the soil treatment herbicides including dichlobenil GR, methiozolin EC, oxaziclomefone SC, imaxaquin GR et al, and 35 kinds of the foliar treatment herbicides including metamifop EC, bifenox flucetosulfuron WG, flazasulfuron WP, trifloxysulfuron-sodium WG et al. registered at the end of May 2012 for efficient management of the weeds occurring on the lawn. For effective management of the weeds, the herbicide can be generally applied twice a year on March to April and August to September for soil treatment and once a year on June to July for the foliage treatment.

Development of a Residue Analysis Method for Metamifop in Paddy Water, Soil, and Rice with HPLC (HPLC를 이용한 농업용수, 논토양, 및 현미 중 metamifop의 잔류분석법 개발)

  • Park, Hee-Woon;Moon, Joon-Kwan
    • The Korean Journal of Pesticide Science
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    • v.21 no.1
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    • pp.68-74
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    • 2017
  • An analytical method for detecting metamifop residue in paddy water, soil, and rice with high performance liquid chromatography (HPLC) was developed. Water was extracted with ethyl acetate before analyzing by HPLC. Soil residues were extracted with acetone under acidic condition and after purifying with $Extrelut^{(R)}$ NT, and silica SPE, the residue was analyzed by HPLC. For residue analysis in rice, the procedure involved extraction with acetone, purification with $Extrelut^{(R)}$ NT, partitioning between acetonitrile/hexane, purification with silica SPE cartridge, and analysis by HPLC. The limit of detection (LOD) was 1.0 ng, limit of quantitation (LOQ) was 3.0 ng, and method limit of quantitation (MLOQ) were 0.001 mg/L for paddy water, 0.01 mg/kg for rice and soil, respectively. Standard calibration curve shows linearity from 0.05 mg/kg to 5.0 mg/kg ($R^2=0.9999$). The recoveries in fortified paddy water were $91.3{\pm}3.5%$ (0.01 mg/L level) and $93.2{\pm}6.3%$ (0.05 mg/L level). The recoveries in fortified paddy soils were $92.5{\pm}4.0%$ (0.1 mg/kg level) and $92.7{\pm}4.0%$ (0.5 mg/kg level) in soil A, while, $102.3{\pm}4.4%$ (0.1 mg/kg level) and $98.9{\pm}7.9%$ (0.5 mg/kg level) in soil B, respectively. The recoveries in fortified rice were $93.0{\pm}6.9%$ (0.1 mg/kg level) and $85.0{\pm}3.5%$ (0.5 mg/kg level). This method was proved to be effective and can be used to determine the metamifop residue in paddy water, paddy soil, and rice.