• Title/Summary/Keyword: 마이크로 웨이브

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Extraction of Total Flavonoids from Lemongrass Using Microwave Energy: Optimization Using CCD-RSM (마이크로웨이브 에너지를 이용한 레몬그라스로부터 플라보노이드 성분의 추출: CCD-RSM을 이용한 최적화)

  • Yoo, Bong-Ho;Jang, Hyun Sick;Lee, Seung Bum
    • Applied Chemistry for Engineering
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    • v.32 no.2
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    • pp.168-173
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    • 2021
  • In this study, we measured total flavonoids after extracting the total flavonoids from lemongrass which is known to have a high content of antioxidant ingredients when using microwave energy. Also, optimal extraction conditions of active ingredients using central composite design-response surface methodology (CCD-RSM) were presented. Both ultrapure water and alcohol were used as extraction solvents and the volume ratio of ethanol/ultrapure water, microwave irradiation time, and microwave irradiation power were set as independence variables. And the extraction yield and total flavonoids were measured. The optimal extraction conditions using CCD-RSM were the volume ratio of ethanol/ultrapure water = 56.3 vol.%, the microwave irradiation time = 6.1 min, and the microwave irradiation power = 574.6 W. We could also obtain expected results of yield = 17.2 wt.% and total flavonoids = 44.7 ㎍ QE/mL dw under the optimum conditions. The comprehensive satisfaction degree of this formula was 0.8562. The P-value was calculated for the yield of 0.037 and the total flavonoids content of 0.002. The average error from actual experiments established for the verification of conclusions was lower than 2.5%. Therefore, a high favorable level could be obtained when the CCD-RSM was applied to the optimization of extraction process.

A Study on the Effect of Reducing the Saturation Magnetization by Substituting the Non magnetic Ion in Mg Mn Ferrites (Mg-Mn훼라이트의 비자성 이온첨가에 의한 포화자화 감소효과)

  • Yu, Byeong-Du;Kim, Jong-O
    • Korean Journal of Materials Research
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    • v.4 no.1
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    • pp.117-124
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    • 1994
  • The reduction of saturation magnetization in the Mg-Mn microwave ferrites was achieved by substituting the non-magnetic A1 ion for Fe ion. It is necessary for extending the operation frequencies that there is no change in other properties of the microwave ferrites. The electrical and magnetic properties are characterized where the composition of the ferrites studied was given by the general formula $(MgO)_{1.0}(MnO)_{0.1}(Al_xFe_{1.9-x}O_{2.85}$ with x ranging from 0.1 to 0.4. The saturation magnetization and the ferromagnetic resonance linewidth was decreased by the substituting amount of $Al_2O_3$. The value of coercive field was low enough over the composition of x=O.2 and the high squareness ratio was obtained all over the amount of substitution. It is feasible to select the proper application area with the combination of various properties ; that is, low coercive field, high squareness ratio, optimum saturation magnetization and ferromagnetic resonance linewidth.

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Space Diversity Combining Scheme Using Phase Difference between Main and Diversity Signals (메인과 다이버시티 신호사이 위상차를 이용한 공간 다이버시티 결합방법)

  • Jung, Gillyoung
    • The Journal of The Korea Institute of Intelligent Transport Systems
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    • v.14 no.5
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    • pp.44-51
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    • 2015
  • The deployment of high capacity backhaul is required due to explosive growth in mobile data services. For rapid backhaul deployment, point to point microwave is a much easier and cheaper technology. The space diversity scheme is used in point to point microwave links. The purpose of space diversity is to overcome fading by combining signals from two separate receiver antennas. For signal combining algorithm, maximum power and minimum distortion methods were used and these algorithms were reported not to be good enough for robustness in selective fading. In this paper, a more practically efficient signal combining scheme from the main and diversity branch is proposed and evaluated in selective fading channel. The proposed algorithm has shown significant performance improvement in terms of signal spectrum.

Implementation of a Resistive Ultra-Wideband Microwave Sensor (저항성 초광대역 마이크로웨이브 센서 구현)

  • Kang, Woong;Kim, Kang-Wook
    • Proceedings of the KAIS Fall Conference
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    • 2009.12a
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    • pp.1014-1017
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    • 2009
  • 본 논문에서는 저항성 초광대역 마이크로웨이브 센서의 설계이론과 구현 방법에 대해 설명하고, 시뮬레이션을 통하여 설계된 센서의 특성을 분석한다. 구현을 위하여 연속적인 저항 프로파일은 이산화되었으며 칩 저항을 이용하여 이산 저항을 실장한다. 시뮬레이션을 통해 칩 저항 8개로 약 8 GHz까지 연속적인 저항 프로파일과 유사한 성능을 보인다는 것을 보인다.

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Tetra Butyl Ammonium Chloride Catalyzed Synthesis of Substituted Benzimidazoles under Microwave Conditions (마이크로웨이브 반응조건에서 염화 테트라부틸암모늄을 촉매로 이용한 치환된 Benzimidazole화합물들의 합성)

  • Karuvalam, Ranjith. P.;Siji, M.;Divia., N.;Haridas, Karickal. R.
    • Journal of the Korean Chemical Society
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    • v.54 no.5
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    • pp.589-593
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    • 2010
  • TBACl (10 mol %) was found to be a useful catalyst for the synthesis of substituted benzimidazoles. The method was proved to be simple, convenient and the product was isolated with good yield.

Coalescence of Nanocrystalline Diamond Crystallites into Thin Film in Microwave Plasma (마이크로웨이브 플라즈마에서 나노결정다이아몬드 입자의 박막 성장 기구)

  • Jeong, Du-Yeong;Kang, Chan-Hyeong
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2009.10a
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    • pp.142-143
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    • 2009
  • Ar/$CH_4$ 마이크로웨이브 플라즈마 하에서 나노결정다이아몬드 박막의 미세구조 형성 과정에 대하여 연구하였다. 실리콘 기판 위에 불균일 핵생성을 위해 만든 스크래치 자리에 생성된 나노결정 크기의 다이아몬드 입자는 시간의 경과에 따라 성장하고 이웃하고 있는 입자들 간에 접촉이 일어나 표면을 완전히 채우게 되면 다이아몬드 박막이 형성되고 지속적인 박막 두께의 성장이 일어나게 된다. 입자들의 높이(혹은 직경)는 증착시간의 제곱근에 비례하는 것으로 나타났다.

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The Influence of Microwave Sintering Process on the Adaptation of CAD/CAM Zirconia Core (마이크로 웨이브 소결 과정이 CAD/CAM 지르코니아 코아의 적합도에 미치는 영향)

  • Kim, Keun Bae;Kim, Jee Hwan;Lee, Keun-Woo
    • Journal of Dental Rehabilitation and Applied Science
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    • v.25 no.2
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    • pp.95-107
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    • 2009
  • The purpose of this research was to examine the fitness of zirconia cores that were made by different sintering methods; generic electricity furnace and microwave furnace. Firstly, 12 cores for each group were made by using each different sintering process and attached them to a metal die with silicon. The internal and marginal gap of sintered zirconia was measured by using Skyscan 1076 micro-CT, then it was reorganized by CT-An software. To each samples, we extracted B-L image, M-D image of cutting side, and cross-sectional side of tooth long axis and calculated the mean value of marginal, axial, and occlusal gap each side. Results: 1. The mean marginal gap of sintered zirconia was $36.20{\mu}m$ for EVE, $47.67{\mu}m$ for LAV, $52.47{\mu}m$ for DEN, and $54.63{\mu}m$ for CER. 2. For the axial wall, the research showed the largest value of $63.49{\mu}m$ for EVE, but there were no statistical significance. 3. In related to the occlusal internal measurement, DEN showed the smallest value ($77.06{\mu}m$), EVE and CER showed significantly high value. From this study, it is suggested that CAD/CAM zirconia core which was made in the process of microwave sintering has clinically acceptable values in marginal and internal gap.

A Study on the Characteristics of Manufactured Mg Crown on the Calcining Conditions of Dolomite (백운석의 소성 조건에 따른 제조 Mg crown의 특성에 관한 연구)

  • Hwang, Dae Ju;Yu, Young Hwan;Lee, Jong Dae
    • Korean Chemical Engineering Research
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    • v.59 no.4
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    • pp.611-625
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    • 2021
  • Mg crowns were manufactured using domestic dolomite (Ca·Mg(CO3)2) (20~30 mm). In order to manufacture the calcined dolomite (CaO·MgO), (a) electric furnace (950 ℃, 480 min) and (b) microwave furnace (950 ℃, 60 min) processes were used. As a result of XRD analysis, it was analyzed as (a) CaO 56.9 wt%, MgO 43.1 wt% by electric furnace process and (b) CaO 55 wt%, MgO 45 wt% by microwave furnace process. Even when the decarbonation reaction time of dolomite was shortened by 1/8 in microwave furnace process compare with electric furnace process, the calcined dolomite could be produced. The hydration reaction (ASTM C 110) is a standard for the hydration reactivity of calcined dolomite, and the calcined dolomite produced by electric furnace process showed a high hydration reactivity (max temp 79.8 ℃/1.5 minutes). Such hydration reactivity was occurred by only CaO hydration reaction and that was confirmed by XRD analysis. The calcined dolomite produced by microwave furnace process showed low hydration reactivity (max temp 81.7 ℃/19.5 minutes). Such low hydration reactivity was occurred by CaO and MgO hydration reaction due to the hydration reaction of CaO thereafter occurring of the hydration reaction of MgO, and that was confirmed by XRD analysis. The prepared Mg crown were 58.8 g and 74.6 g by electric furnace and microwave furnace processes, respectively, under the reaction conditions of 1,230 ℃, 60 min, 5 × 10-2 torr by silicothermic reduction.

Effect of microwave radiation on physical special quality of normal, high amylose and waxy corn starches (마이크로웨이브를 조사한 옥수수전분의 물리적 특성변화)

  • Lee Su Jin;Choe Yeong Hui
    • Journal of Applied Tourism Food and Beverage Management and Research
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    • v.15 no.1
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    • pp.113-125
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    • 2004
  • Effect of microwave radiation on physico-chemical properties of cor'n starches was studied. Waxy com, com and high amylose com starches of varying moisture content(20~35%) were subjected to microwave processing(2450MHz) at $120^{\circ}$ and the experimental starch samples were examined by a X-ray diffractometry, rapid viscosity analyzer(RVA) and. with the samples in temperature was observed and the peaks of high amylose com starches at $2^{\circ}$=5.0, 15.0 and $23.0^{\circ}$, were disappeared indicating the melting of crystallines while those of com and waxy com had not changed. A change in gelatinization pattern was observed in the case of corn starches from type A with nearly no peak-viscosity and breakdown to type C. Except a decreased viscosity, no change was observed in those of waxy com starches.

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