• Title/Summary/Keyword: 딥-코팅법

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Synthesis and Characterization of Sol-Gel Derived Mesoporous Titania/Alumina Membranes (솔젤법에 의한 메조기공 티타니아/알루미나 막의 제조 및 기체투과 특성)

  • Kwon, Hyuk-Taek;Kim, Jin-Soo
    • Membrane Journal
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    • v.21 no.3
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    • pp.229-235
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    • 2011
  • In this study, mesoporous titania/alumina membranes were prepared by sol-gel method. Pore structure and phase composition of titania/alumina membranes could be changed by calcination temperature. The addition of alumina into titania membranes retarded anatase-to-rutile phase transformation, resulting in stabilization of pore structures. The 5 time dip-coated membrane calcined at $450^{\circ}C$ is about $10.3{\mu}m$ in thickness with an average pore size of 5 nm. Hydrogen and nitrogen permeances through the membrane were $17.1{\times}10^{-7}mol/m^2{\cdot}s{\cdot}Pa$ and $4.7{\times}10^{-7}mol/m^2{\cdot}s{\cdot}Pa$, respectively. These data were explained by the Knudsen diffusion mechanism.