• Title/Summary/Keyword: 균질화처리

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자기조립박막 증착법을 이용한 영구적인 친수성 표면의 플루이딕스칩 제작에 관한 연구

  • Kim, Dong-Jin;Lee, Mun-Gwon;Lee, Jeong-Hwan;Im, Hyeon-U;Park, Jin-Gu;Sin, Sang-Taek;Kim, Jeong-Ho;Jo, Byeong-Gi
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.05a
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    • pp.49.2-49.2
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    • 2009
  • 최근, 플루이딕스칩 제작에 있어서 가격이 저렴하며 구조물 형성이 쉽다는 장점으로 인하여 유리 기판을 플라스틱 기판으로 대체하려는 연구가 많이 진행하고 있다. 하지만 플라스틱 기판은 유리 기판에 비하여 많은 장점을 갖고 있음에도 불구하고, 기판 표면이 소수성이기 때문에 유체의 흐름을 저하시키는 문제점이 있다. 기존의 플라스틱 기판을 친수성으로 개질하는 방법으로는 화학적처리, 자외선 조사, 산소플라즈마 처리 등의 방법이 있었으나, 화학적처리 방법은 공정의 민감성과 폐기물로 인한 양산적용의 한계가 있고, 자외선 조사법 및 산소 플라즈마 처리는 친수성이 영구적이지 않다는 결정적인 문제점이 있다. 이는 플라스틱 플루이딕스칩의 신뢰도를 크게 저해하여 상용화에 큰 문제점으로 작용한다. 이러한 문제점을 극복하기 위한 새로운 방법의 친수성 표면처리가 요구되어 지고 있다. 본 연구에서는, 기존 플라스틱 기판의 친수성 표면처리 방법들의 문제점들을 개선하고자 플라스틱 기판의 변형을 야기하지 않는 저온 PE-CVD 방식을 이용하여 균질한 두께의 $SiO_2$박막을 형성 하였으며, 형성된 박막을 liquid self-assembled monolayer(L-SAM)방식을 이용하여 아민 표면으로 개질하였다. 이를 통해, 플라스틱 채널 상에서 유체의 원활한 흐름, 형성된 아민 표면에 단백질 및 DNA와 같은 생체 물질 고정화의 용이성 및 영구적 표면개질의 특성을 얻을 수 있었다. 이뿐만 아니라, 플라스틱 기판 외에도 재료에 관계없이 모든 물질의 표면을 생체 안정성이 뛰어난 친수성 표면으로 개질 할 수 있으며, 알데히드 및 카르복시산 등의 다양한 작용기로 변형이 쉽다는 장점이 있다. 개질된 친수성 표면의 평가를 위하여 시간에 따른 접 촉각 및 형광 스캐너(Fluorescence Scanner)를 이용하여 영구적인 친수성 특성 및 생체물질 적합성을 파악하였다. 또한, L-SAM 조건에 따른 아민의 형성정도를 측정하기 위하여 XPS(X-ray Photoelectron Spectroscopy) 분석을 실시 하였다. 최적화된 표면처리를 실제 플라스틱 플루이딕스칩에 적용하여, 유체의 흐름을 관찰 하였다.

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Color Image Segmentation for Content-based Image Retrieval (내용기반 영상검색을 위한 칼라 영상 분할)

  • Lee, Sang-Hun;Hong, Choong-Seon;Kwak, Yoon-Sik;Lee, Dai-Young
    • The Transactions of the Korea Information Processing Society
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    • v.7 no.9
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    • pp.2994-3001
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    • 2000
  • In this paper. a method for color image segmentation using region merging is proposed. A inhomogeneity which exists in image is reduced by smoothing with non-linear filtering. saturation enhancement and intensity averaging in previous step of image segmentation. and a similar regions are segmented by non-uniform quantization using zero-crossing information of color histogram. A edge strength of initial region is measured using high frequency energy of wavelet transform. A candidate region which is merged in next step is selected by doing this process. A similarity measure for region merging is processed using Euclidean distance of R. G. B color channels. A Proposed method can reduce an over-segmentation results by irregular light sources et. al, and we illustrated that the proposed method is reasonable by simulation.

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A Study on the Statistical Representativeness of Samples taken from Radioactive Soil (방사성 토양폐기물 시료의 통계적 대표성에 관한 연구)

  • Cho Han-Seok;Kim T.K.;Lee K.M.;Ahn S.J.;Shon J.S.
    • Proceedings of the Korean Radioactive Waste Society Conference
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    • 2005.06a
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    • pp.151-157
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    • 2005
  • For the treatment of regulatory clearance of the soils, a procedure for the radionuclides and radioactivity concentration analysis is under development. A strategy for soil sampling including random sampling after homogenization and standardization was set up. Statistical representativeness is considered for not only sampling strategy but also sample size. In this study, designed sample size was designed with confidence interval and error bound of soil using the pilot samples which were taken following the sampling strategy.

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Feasibility Study on Vitrification for Rare Earth Wastes of PyroGreen Process (파이로그린공정 희토류폐기물 유리화 타당성 연구)

  • Kim, Cheon-Woo;Lee, Byeong Gwan
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.11 no.1
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    • pp.1-9
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    • 2013
  • The rare earth oxide wastes consisting of major 8 nuclides Y, La, Ce, Pr, Nd, Sm, Eu and Gd, are generated during the salt waste treatment of PyroGreen process. The final form of the rare earth is generated as the oxide state. In this study, six candidate glasses were developed to evaluate the feasibility for vitrifying the rare earth oxide wastes within the borosilicate glass system. The solubilities of the mixture of the rare earth oxide waste showed less than 25wt% at $1,200^{\circ}C$, less than 30wt% at $1,300^{\circ}C$, respectively. It means that solubility is increased with the temperature increment. The liquidus temperature of the homogeneous glass with 20wt% waste loading was determined as less than $950^{\circ}C$. In more than solubility of rare earth oxides glass, formation of rare earth-oxide-silicate crystal in glass-ceramic occurred as the secondary phase. As their viscosity at melting temperature $1,200{\sim}1,300^{\circ}C$ was less than 100 poise, electrical conductivity was higher than 1 S/cm, 20~25wt% waste loading glasses with good surface homogeneity are judged to have good operability in cold crucible induction melter. Other physicochemical properties of the developed glasses are going to be experimented in the future.

Monte Carlo Photon and Electron Dose Calculation Time Reduction Using Local Least Square Denoising Filters (국소 최소자승 잡음 감소 필터를 이용한 광자선 및 전자선 몬테칼로 선량 계산 시간 단축)

  • Cheong Kwang-Ho;Suh Tae-Suk;Cho Byung-Chul;Jin Hosang
    • Progress in Medical Physics
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    • v.16 no.3
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    • pp.138-147
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    • 2005
  • The Monte Carlo method cannot have been used for routine treatment planning because of heavy time consumption for the acceptable accuracy. Since calculation time is proportional to particle histories, we can save time by decreasing the number of histories. However, a small number of histories can cause serious uncertainties. In this study, we proposed Monte Carlo dose computation time and uncertainty reduction method using specially designed filters and adaptive denoising process. Proposed algorithm was applied to 6 MV photon and 21 MeV electron dose calculations in homogeneous and heterogeneous phantoms. Filtering time was negligible comparing to Monte Carlo simulation time. The accuracy was improved dramatically in all situations and the simulation of 1 $\%$ to 10$\%$ number of histories of benchmark in photon and electron dose calculation showed the most beneficial result. The empirical reduction of necessary histories was about a factor of ten to fifty from the result.

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Effect of Alloying Elements and Homogenization Treatment on Carbide Formation Behavior in M2 High Speed Steels (합금성분변화와 균질화처리에 따른 M2 고속도강의 탄화물 형성거동)

  • Ha, Tae Kwon;Yang, Eun Ig;Jung, Jae Young;Park, Shin Wha
    • Korean Journal of Metals and Materials
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    • v.48 no.7
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    • pp.589-597
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    • 2010
  • In the present study, the effect of variation in alloying elements on the carbide formation behavior during casting and homogenization treatment of M2 high speed steels was investigated. M2 high speed steels of various compositions were produced by vacuum induction melting. Contents of C, Cr, W, Mo, and V were varied from the basic composition of 0.8C, 0.3Si, 0.2Mn, 4.0Cr, 6.0W, 5.0Mo, and 2.0V in weight percent. Homogenization treatment at $1150^{\circ}C$ for 1.5 hr followed by furnace cooling was performed on the ingots. Area fraction and chemical compositions of eutectic carbide in as-cast and homogenized ingots were analyzed. Area fraction of eutectic carbide appeared to be higher in the ingots with higher contents of alloying elements the area fraction of eutectic carbide also appeared to be higher on the surface regions than in the center regions of ingots. As a result of the homogenization treatment, $M_2C$ carbide, which was the primary eutectic carbide in the as-cast ingots, decomposed into thermodynamically stable carbides, MC and $M_6C$. The latter carbide was found to be the main one after homogenization. Fine carbides uniformly distributed in the matrix was found to be MC type carbide and coarsened by homogenization.

Plastic Behaviro of Two Phase Intermetallic Compounds Based on $Li_2$-type$(Ai, Cr)_3$/Ti ($Li_2$$(Ai, Cr)_3$/Ti기 2상 금속간화합물의 소성거동)

  • Park, Jeong-Yong;O, Myeong-Hun;Wi, Dang-Mun;Miura, S.;Mishima, Y.
    • Korean Journal of Materials Research
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    • v.4 no.8
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    • pp.906-914
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    • 1994
  • Plastic behavior of two-phase intermetallic compounds based on $LI_{2}$-type $(Al, Cr)_3$ Ti was investigated using compression test at R.T. and 77K. $LI_{2}$ single phase alloys and two-phase alloys consisting of mainly $LI_{2}$ phase and a few or 20% second phases were selected from AI-Ti-Cr phase diagram. In general, compared with Llz single phase, two-phase alloys consisting of 20% second phase showed relatively high yield strength and poor ductility. Among the alloys, however, AI-21Ti-23Cr alloy consisting of 20% $Cr_{2}Al$ phase showed available ductility as well as high yield strength. Plastic behavior of $LI_{2}$ single phase alloys and two-phase alloys consisting of a few% $Cr_{2}Al$ was also investigated. Homogenization of arc melted ingots substantially reduced the amount of second phases but introduced extensive pore. When Cr content increased in $Ll_{2}$ single phase alloys after the homogenization, the volume fraction of pore in the alloys decreased, and no residual pore was observed in two-phase alloys consisting of a few% $Cr_{2}Al$ phase. Environmental effect on the ductility of the alloys was investigated using compression test at different strain rates($1.2 \times 10^{-4}/s$ and $1.2 \times 10^{-2}/s$). Environmental embrittlement was least significant in A1-25Ti-10Cr alloy consisting of LIZ single phase among the alloys tested in this study. However, based on the combined estimation of the pore formation, environmental embrittlement and ingot cast structure, AI-21Ti-23Cr alloy consisting of 20% $Cr_{2}Al$ as the second phase is expected to show the best tensile elongation behavior.

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Changes and Improvements of the Standardized Eddy Covariance Data Processing in KoFlux (표준화된 KoFlux 에디 공분산 자료 처리 방법의 변화와 개선)

  • Kang, Minseok;Kim, Joon;Lee, Seung-Hoon;Kim, Jongho;Chun, Jung-Hwa;Cho, Sungsik
    • Korean Journal of Agricultural and Forest Meteorology
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    • v.20 no.1
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    • pp.5-17
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    • 2018
  • The standardized eddy covariance flux data processing in KoFlux has been updated, and its database has been amended accordingly. KoFlux data users have not been informed properly regarding these changes and the likely impacts on their analyses. In this paper, we have documented how the current structure of data processing in KoFlux has been established through the changes and improvements to ensure transparency, reliability and usability of the KoFlux database. Due to increasing diversity and complexity of flux site instrumentation and organization, we have re-implemented the previously ignored or simplified procedures in data processing (e.g., frequency response correction, stationarity test), and added new methods for $CH_4$ flux gap-filling and $CO_2$ flux correction and partitioning. To evaluate the effects of the changes, we processed the data measured at a flat and homogeneous paddy field (i.e., HPK) and a deciduous forest in complex and heterogeneous topography (i.e., GDK), and quantified the differences. Based on the results from our overall assessment, it is confirmed that (1) the frequency response correction (HPK: 11~18% of biases for annually integrated values, GDK: 6~10%) and the stationarity test (HPK: 4~19% of biases for annually integrated values, GDK: 9~23%) are important for quality control and (2) the minimization of the missing data and the choice of the appropriate driver (rather than the choice of the gap-filling method) are important to reduce the uncertainty in gap-filled fluxes. These results suggest the future directions for the data processing technology development to ensure the continuity of the long-term KoFlux database.

The Effect of Storage Container Types on Odor Emission and Quality of Piggery Liquid Slurry Fertilizer in the farms (농가의 돈분액비 저장형태가 악취발생과 액비품질에 미치는 영향)

  • Park, Moo-Eon;Kang, An-Seok;Kim, Si-Chang
    • Korean Journal of Soil Science and Fertilizer
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    • v.39 no.3
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    • pp.136-143
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    • 2006
  • The study was carried out to evaluate odor emission during storage time and quality of liquid slurry fertilizer along with three storage container types installed at farmer's fields in Cheorwon. Liquid slurry manure stored in the liquid-circulated or the air-injected tank was very homogeneous in concentration of nutritional elements because of well mixing operation, while nutritional concentration of the manure stored in the non-treated tank was significantly different from top to bottom in the tank, which may bring about partially irregular growth of plant after its application. The potential capacity of offensive odor emitted from liquid slurry manure stored in the liquid-circulated or the air-injected tank was much lower than that emitted from manure stored in the non-treated tank. Low potential capacity may less emit offensive odor after application of piggery liquid slurry on the field. The efficiency in oder to reduce odor emission from liquid manure was slightly higher in the liquid-circulated tank than the air-injected tank

Corrsion behavior of Al-Mg-Zn Alloys by homogenization heat treatment (균질화 처리에 따른 Al-Mg-Zn 합금의 내식성 거동)

  • Jo, Yu-Sin;Choe, In-Gyu;Kim, Sang-Ho
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2017.05a
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    • pp.139-139
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    • 2017
  • 최근 환경오염 문제로 인한 연비 규제 강화 속도가 빨라지고 있으며 이에 따른 연비 향상 기술이 크게 대두 되고 있다. 연비 향상 기술 중 경량화 방안소재로 알루미늄(Al), 마그네슘(Mg) 등의 비철금속을 주로 사용하고 있으며, 이중 알루미늄은 다른 경량화 금속소재보다 우수한 경쟁력을 가지고 있다. 하지만 경제적인 측면에서 철 대비 비용적인 어려움을 가지고 있고 용접성이 떨어지기 때문에, 자동차 부품의 일부만 알루미늄 소재를 선택하여 사용하고 있는 실정이며 알루미늄의 높은 이온화 경향으로 인해 기존 자동차 철강 소재와 접촉 시 쉽게 부식되는 단점을 가지고 있다. 이러한 문제점을 해결하기 위해서는 알루미늄의 금속원소를 첨가하는 연구가 지속적으로 개발 되고 있다. 알루미늄 합금에서 마그네슘의 첨가는 좋은 용접성과 내식성, 강도를 향상시킨다. 하지만 3%이상의 마그네슘 첨가는 입계에 ${\beta}(Al_xMg_y)$석출상이 석출되게 되며, 입계에 연속적으로 형성된 ${\beta}(Al_xMg_y)$석출상은 응력 부식 균열 (Stress corrsion cracking)과 입계 부식(Intergranular corrosion)을 야기하는 결과를 가져온다고 알려져 있다. 이 문제를 해결하기 위해 Al 5000계열 합금의 Zn의 첨가를 통해 ${\tau}(Al_xMg_yZn_z)$을 입계에 석출시켜서 입계에 ${\beta}(Al_xMg_y)$상의 석출을 방지함으로써 내식성을 향상시키거나 Al 5000계열 합금의 열처리를 통해 ${\beta}(Al_xMg_y)$석출상을 고용시킴으로써 응력부식균열의 발생을 억제하는 연구도 있다. 하지만 열처리 후 Polarization test를 이용한 내식성 연구는 잘 안 알려져 있다. 따라서 이번 연구에서는 Al5000계열의 주조한 합금을 DSC분석을 통하여 ${\beta}(Al_xMg_y)$석출상의 고용 온도가 약 $470^{\circ}C$라는 것을 확인한 후, 실온에서 $100^{\circ}C/hr$으로 가열하고 조건에 따라 $450^{\circ}C$에서 3시간, 6시간, 12시간, 24시간, 30시간 항온 유지시킨 후 공냉을 진행하였다. 열처리를 마친 시편은 에폭시를 이용하여 마운팅 하였으며, 시편표면을 2000#까지 연마 후 증류수로 세척한 다음 질소를 이용하여 건조 후 분극 시험을 진행하였다. 3.5wt% NaCl 용액에서 분극 곡선을 통해 부식거동을 확인한 결과 24시간까지 시간이 증가 할수록 내식성이 우수해지는 것을 확인하였으며, 추가적으로 조직사진, SEM & EDS 분석과 XRD, TEM 분석을 통해 내식성은 입계에 존재하는 Mg의 조성이 감소하게 되면 내식성이 향상되는 것을 관찰하였다.

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