• Journal of the Korean Ceramic Society
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• v.38 no.1
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• pp.74-83
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• 2001

FHD(Flame Hydrolysis Deposition) 공정은 광통신에서 사용되는 수동형 집적광학소자를 제작하는 공정으로서, SiCl$_4$를 형성하는 방법이다. 이 FHD 공정은 화염 형성에 관여하는 장비의 조건에 따른 매우 다양한 공정인자에 의하여 박막의 조성이 결정되므로, 박막의 조성을 예측하는 것이 용이하지 않았다. 본 연구에서는 FHD 공정에서 첨가가스의 유량을 제어하여 박막의 조성 및 광학적 특성을 예측할 수 있는 공정 분석의 기초자료를 제공하기 위하여 FTIR과 ICP-AES를 이용하여 실리카 soot의 조성분석에 대한 연구를 수행하였다. FTIR 흡수스펙트럼을 통해 실리카 soot에 존재하는 Si-O, B-O, OH($H_2O$) 농도의 변화를 관찰할 수 있었으며, ICP-AES를 통해 B-O의 흡수스펙트럼의 변화를 B의 농도와 정량적으로 연관지을 수 있었다.

• Applied Biological Chemistry
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• v.25 no.3
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• pp.182-188
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• 1982

A fluorometric method is described which permits the assay of trypsin inhibitor contained in a sample in an extremely small amount, utilizing a novel reagent generally called fluorescamine. The fluorometric assay with an enzyme kinetic approach has been found to be at least 100 times more sensitive than the well-known Kunitz's spectrophotometric method, considerably taster and less complicated, when it was demonstrated with the anti tryptic activities of very dilute extracts from soybean, red-bean and mung bean. Details of experimental procedure as well as theoretical considerations will be discussed.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.11 no.5
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• pp.407-412
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• 1998

In this paper, we design PHASAR(Phased Array) WDM(Wavelength Dvision Division Multi- and Demultiplexing) filters and evaluate their performance. The PHASAR WDM filter is designed to have flat-passband characteristics by inserting the multimode waveguides between input waveguides and a first star coupler. BPM simulation results show that the excess loss is smaller than 6.5 dB, the crosstalk is less than -22 dB and the 1 dB passband is about 50 GHz. The effect of the path difference error is also investigated.

• Journal of the Korean Ceramic Society
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• v.37 no.1
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• pp.77-81
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• 2000

Silica glass films to utilize optical waveguides was fabricated by Aerosol Flame Deposition(AFD) method. As the amount of B2O3 increased in the sol solution of (92-x)SiO2-xB2O3-8P2O5, the thermophoretic deposition rate onto Si substrate was markedly lowered due to vaporizing out of B2O3 and P2O5 during the vaporization and reaction of the aerosol in the flame. GeO2 was added to 62SiO2-30B2O3-8P2O5 in order to control easily the refractive index of glass films. As the amount of GeO2 increased from 2 to 12 wt%, its refractive index increased from 1.4633 up to 1.4716.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2012.05a
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• pp.195-195
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• 2012

$Eu^{3+}$ 이온의 농도비를 변화시키면서 고상 반응법을 사용하여 적색 형광체 $Sr_{1-1.5x}MoO_4:Eu_x{^{3+}}$ 분말을 합성하였다. 제조한 형광체의 결정 구조는 X-선 회절 장치를 사용하여 정방정계임을 확인하였고, 광학 특성은 형광 광도계를 사용하여 상온에서 측정하였다. $Eu^{3+}$ 이온의 농도비가 0.01 mol인 형광체의 경우에, 파장 295 nm로 여기시켰을 때 주된 발광은 파장 619 nm에 최대 세기를 갖는 적색 형광을 나타내었으며, 최대 흡수 스펙트럼은 넓은 밴드를 갖고 파장 302 nm에서 관측되었다.

• Proceedings of the Optical Society of Korea Conference
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• 2003.07a
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• pp.278-279
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• 2003

광도의 기본 단위인 칸델라(Candela) 눈금은 물론 복사조도(irradiance), 조명도(illuminance)와 같은 유도 단위를 실현하기 위해서는 검출기의 시야를 한정하는 개구면적의 정밀한 측정이 필요하다. 여기에서는 가장자리의 광학적 검출방법에 의한 개구면적의 산출방식을 소개하고, 가우시안광에 의한 면적 측정법의 측정값과도 비교하여 그 결과를 보여준다. 기존의 개구 면적 측정방식으로 한가지 방법은 탐촉자를 물리적으로 접촉시켜서 개구의 가장자리를 결정하고, 개구의 기하학적 모양을 원으로 가정하여 면적을 산출하는 방식이 있는데, 이 방법을 사용하면 기계적인 접촉에 의하여 칼날과 같았던 개구의 가장자리가 손상을 입게 되기 때문에 측정이 잘못되는 것은 물론이고, 이렇게 측정된 개구를 사용하게되면 손상된 부위에 의한 면적의 변화와 이로 인한 산란이 증가하게 된다. (중략)

• Restorative Dentistry and Endodontics
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• v.32 no.1
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• pp.28-36
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• 2007

The purpose of this study was to compare the effect of exponential curing method with conventional curing and soft start curing method on polymerization shrinkage of composite resins. Three brands of composite resins (Synergy Duo Shade, Z250, Filtek Supreme) and three brands of light curing units (Spectrum 800, Elipar Highlight, Elipar Trilight) were used. 40 seconds curing time was given. The shrinkage was measured using linometer for 90 seconds. The effect of time on polymerization shrinkage was analysed by one-way ANOVA and the effect of curing modes and materials on polymerization shrinkage at the time of 90s were analysed by two-way ANOVA. The shrinkage ratios at the time of 20s to 90s were taken and analysed the same way. The results were as follows : 1. All the groups except Supreme shrank almost within 20s Supreme cured by soft start and exponential curing had no further shrinkage after 30s (p < 0.05). 2. Statistical analysis revealed that polymerization shrinkage varied among materials (p = 0.000) and curing modes (p = 0.003). There was no significant interaction between material and curing mode. 3. The groups cured by exponential curing showed the statistically lower polymerization shrinkage at 90s than the groups cured by conventional curing and soft start curing (p < 0.05). 4. The initial shrinkage ratios of soft start and exponential curing were statistically lower than conventional curing (p < 0.05). From this study, the use of low initial light intensities may reduce the polymerization rate and, as a result, reduce the stress of polymerization shrinkage.

• Journal of Navigation and Port Research
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• v.28 no.1
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• pp.43-49
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• 2004

Defects inspection of commodities are very important with those design and manufacturing process and essential to strengthen the competitiveness of those. If on-line automatic defects detection is performed without damaging to products, the production cost shall be curtailed through the reducing man-power, economical management of Q.C(Quality Control). In this paper, it is suggested three spatial filtering methods which can extract the necessary information in case of defects being on the surface of object like iron plate. In addition, the dependence of filtering characteristics on parameters such as the pitch and width of slits is analyzed and the surface defect detection system is constructed. Several experiments were carried out for determining the adequate spatial filtering method through comparing and analyzing effects of parameters like defect's size and shape, intensity of light, noise of coherent source and slit number.

• Journal of the Korean Chemical Society
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• v.54 no.5
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• pp.556-566
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• 2010

A new kinetic spectrophotometric method is developed for the measurement of Mn(II) in natural water samples. The method is based on the catalytic effect of Mn(II) with the oxidation of Gallocyanin by $KIO_4$ using nitrilotriacetic acid (NTA) as an activation reagent at 620 nm. The optimum conditions obtained are $4.00{\times}1^{-5}\;M$ Gallocyanin, $KIO_4$, $1.00{\times}10^{-4}\;M$ NTA, 0.1 M HAc/NaAc buffer of pH = 3.50, the reaction time of 5 min and the temperature of $30^{\circ}C$. Under the optimum conditions, the proposed method allows the measurement of Mn(II) in a range of $0.1\;-\;4.0\;ng\;mL^{-1}$ and with a detection limit of down to $0.025\;ng\;mL^{-1}$. The recovery efficiency in measuring the standard Mn(II) solution is in a range of 98.5 - 102%, and the RSD is in a range of 0.76 - 1.25%. The newly developed kinetic method has been successfully applied to the measurement of Mn(II) in both some environmental water samples and certified standard reference river water sample, JAC-0031 with satisfying results. Moreover, few cations and anions interfere with the measurement of Mn(II). Compared with the other catalytic-kinetic methods and instrumental methods, the proposed kinetic method shows fairly good selectivity and sensitivity, low cost, cheapness, low detection limit and rapidity. It can easily and successfully be applied to the real water samples with relatively low salt content and complex matrices such as bottled drinking water, cold and hot spring waters, lake water, river water samples.

• Analytical Science and Technology
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• v.29 no.6
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• pp.277-282
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• 2016

British Pharmacopoeia (BP 2013), the United States Pharmacopoeia (USP 39) and the Korean Pharmacopoeia (KP XI) contain monographs for the quality control of raw diosmin using high performance liquid chromatography (HPLC). However, official monographs detailing pharmaceutical formulations for diosmin are not available in foreign pharmacopoeias. In the KP XI, ultraviolet-visible (UV-Vis) spectroscopy-which is less specific than HPLC-is reported for the testing of diosmin capsules. In this study, we present an alternative HPLC assay for such testing that is more specific than UV-Vis methods. Method validation was performed to determine linearity, precision, accuracy, system suitability, and robustness. The linearity of calibration curves in the desired concentration range was high ($r^2$>0.999), while the RSDs for intra- and inter-day precision were 0.15-0.29 % and 1.05-1.74%, respectively. Accuracies ranged from 101.2-103.2 %, while the retention time and peak area RSDs were 0.37 % and 0.06 %, respectively. Additionally, the plate number and asymmetry factor values for diosmin were 3591.293 and 1.35, respectively. Since the intermediate-precision and robustness of the assay were satisfactory, this method will be a valuable addition to the Korean Pharmacopoeia (KP XI).