• Title/Summary/Keyword: 관법

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Evaluation of Ground-Water Sampling Techniques for Analysis of Chlorofluorocarbons (지하수의 CFCs(Chlorofluorocarbons) 조사를 위한 시료 채취 방법의 평가)

  • 고동찬;이대하
    • Journal of Soil and Groundwater Environment
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    • v.8 no.2
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    • pp.1-8
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    • 2003
  • Two types of ground-water sampling techniques for CFCs (chlorofluorocarbons) analysis, the cold-welded copper tube method and flame-sealed borosilicate glass ampule method, were compared and evaluated. CFCs concentrations by the copper tube method showed a poor reproducibility among triplicates whereas those by the glass ampule method showed a good agreement and relative standard deviations of triplicates were less than 5%. The poor reproducibility of the copper tube method appears to be attributed to the incomplete sealing in connection between faucets of wellhead and the sampling apparatus. The copper tube method also showed higher CFCs concentrations than the glass ampule method, which is more pronounced for CFC-11 than for CFC-12. The plastic tubings and rubber gasket of faucets in case of the copper tube method possibly contaminated the samples with CFC-11 and CFC-12. The potential of CFCs contamination for the glass ampule method was eliminated by using stainless steel and Nylon only and by connecting the sampling equipment directly to the main discharge pipe of wellhead. The validity of the glass ampule method were also verified by detecting very low level of CFCs for the ground-water sample which is old enough to have negligible CFCs.

Fabrication of Microstructures with Nanocomposites by Capillary Effect (모세관법을 이용한 나노 복합재료 마이크로 구조 제작)

  • Han, Soo-Ho;Hwang, Hui-Yun
    • Composites Research
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    • v.31 no.4
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    • pp.171-176
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    • 2018
  • We proposed new and easy fabrication method of micro-nano hierarchical structures for synthetic dry adhesives and conducted feasibility tests of alignment characteristics of nano-materials in the microstructures by capillary effect. Candidates of fabrication conditions were selected based on the degree of cure and viscosity of mixtures of multiwall carbon nanotubes (MWCNTs) and polydimethylsiloxane (PDMS), which were measured with respect to the fabrication conditions. Scanning electron microscopy images of cross sections of MWCNT-PDMS microstructures were analyzed. MWCNT alignment in microstructures was better when fabrication temperature and degree of cure at fabricating start were lower, but areal density of MWCNTs was little affected by fabrication conditions.

The Activity of Succinic Dehydrogenase During the Metamorphosis on the Pine Moth, Dendrolimus spectabilis BUTLER (송충의 변태에 따른 Succinic Dehydrogenase 의 활성도)

  • 김창환;류종명
    • The Korean Journal of Zoology
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    • v.9 no.2
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    • pp.7-9
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    • 1966
  • 송충(Dendrolimus spectabilis)의 변태에 따른 succinic dehydrogenase 의 활성도를 Thunberg 관법을 이용하여 측정하였다. 일반적으로 생성도의 변동은 기관발생과 밀접한 관계를 가지고있으며 각 기관에 있어서의 활성도는 아래와같다. 1. Gut는 여러 기관중 제일 높은 활성도를 보여주며 fat body 와 더불어 U자 모양 curve의 활성도를 나타내고 있다. 2. Brain 과 testis 는 상승의 활성도를 보여주었다. 3. Body wall 과 verve cord의 활성도는 불규칙적이었다.

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A Study on the Toxic Gases Released from Fire Retardant Finishing Materials (가스검지관법에 의한 방염시료의 연소가스 독성평가)

  • Lee, Hae Pyeong;Park, Young Ju;Lim, Suk Hwan;Kim, Jung In
    • 한국방재학회:학술대회논문집
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    • 2011.02a
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    • pp.195-195
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    • 2011
  • 본 연구는 방염성능시험에 의한 필름 및 도료처리 시료를 대상으로 화재 시 발생하는 연소가스 중의 독성에 대하여 NES 713 방법에 의해 분석하고, 독성지수를 확인함으로써 연소 시 인체에 미치는 영향을 간접적으로 확인해 보고자 하였다. 기존 방염제품 중 필름과 도료처리 그리고 도료처리 후 기간이 경과한 시료의 3가지로 실험군을 구분하였으며, NES 713 방법으로 연소가스를 분석하고 독성지수를 평가하였으며, 추가로 기존의 국내 노출기준과의 비교를 수행하였으며, 국내 NES 713 방법을 활용한 선행연구들을 참조하였다. 발암가능 추정물질인 아크릴로니트릴은 총 18개의 시료에서 검출되었으며, 포름알데히드는 9개의 시료에서 검출되었다. 염화수소와 브롬화수소는 각각 5개의 시료들에서 검출된 반면에 도료처리된 시료에서는 각각 1개만이 검출되었다. 그 외 일산화탄소와 이산화탄소 그리고 질소산화물은 모든 시료에서 공통적으로 검출되었다. 독성지수는 최소 3.5에서 최고 9.4의 값을 갖는 것으로 나타났다. 본 연구에서 수행한 NES 713 분석결과와 독성지수 산출 및 기존 국내 노출기준과의 비교를 수행해 본 결과는 다음과 같았다. 첫째, 현행 국내 기준 상 방염제품의 독성시험 등에 관한 기준이 없고, 둘째, 방염제품에 대한 연소가스 독성 등을 평가한 선행연구가 제한적이라는 점에서 의미가 있을 것으로 사료된다. 하지만 독성지수의 적용이 국내에서 이루어지고 있지 않은 현실에서 산출도나 독성지수의 위해정도를 평가하기 어렵고, 시료의 수량이 총 18개로서 많지 않았다는 점에서 전체 방염제품의 연소가스 독성의 잠재적인 위험성을 추정할 수는 있지만 대표성을 갖기에는 문제점이 있다는 한계성을 벗어날 수 없었다. 따라서 향후 후속 연구에서는 보다 많은 방염제품들을 대상으로 무작위 선정을 통한 연구 설계 및 실험 연구가 수행된다면 보다 객관적이고 대표성을 지닌 연구결과를 도출할 수 있을 것으로 기대한다.

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Thixoforming Characteristics of Metal Matrix Composites (Phase identification of $SiC_p/AZ91HP$ Mg composite) (금속기 복합재료의 틱소포밍 특성 ($SiC_p/AZ91HP$ Mg 복합재료의 상분석을 중심으로))

  • Lee, Jung-Il;Kim, Young-Jig
    • Applied Microscopy
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    • v.29 no.3
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    • pp.281-289
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    • 1999
  • The stirred and thixoformed $SiC_p/AZ91HP$ Mg composites are studied on the basis of microstructural analysis using transmission electron microscopy (TEM). The products of interfacial reaction are identified as $Mg_2Si$, MgO and $Mg_{17}Al_{12}$ phases and the crystallized phases are found to be orthorhmbic $Al_6Mn$ and decagonal T phases. It is shown that $Mg_2Si$ and $Mg_{17}Al_{12}$ phases are found at the surface of $SiC_p$ and $Al_6Mn$ is found near interface and crystallized on the matrix. Phase identification is carried out by crystallographic work based on primitive cell volume, zero order Laue zone (ZOLZ) patterns and single convergent beam electron diffraction (CBED) patterns containing higher order Laue zone ring from a nanosized region.

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Sound Transmission Loss Measurement for Sound Isolation Sheets by Two-Microphone Impedance Tube Method (두 개의 마이크로폰의 부착된 임피던스관법을 이용한 차음시트의 음향투과손실 측정)

  • Lee, Dong-Hoon;Yong, Ho-Taek;Lee, Seung
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.14 no.1
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    • pp.63-72
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    • 2002
  • The main objective of this study is to propose a practical two-microphone impedance tube method to measure the sound transmission loss for flexible sound isolation sheets without the use of the time-consuming and expensive reverberation room. This method was based on the sound decomposition theory developed by Seybert using the spectral density functions of the incident and reflected sound waves. In order to verify the validity of the experimental results, the measured sound transmission losses from the proposed method were compared with the measured data from the reverberation room method and the calculated data from the theory satisfying the mass law of sound isolation material. The resulted trends of the sound transmission losses versus frequencies for several different sound isolation sheets were almost same for each other and agreed quite well in both methods except at some low frequency region. From the experimental results, it was found that the accuracy of sound isolation capability obtained by two-microphone impedance tube method depends upon the microphone spacing, the distance from the first microphone to the test sample surface and the test sample location.