• Title/Summary/Keyword: 결함길이

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$Cr^{3+} :BeAl_2O_4$ 레이저 단결정 성장 및 $Cr^{3+}$이온의 특성

  • ;A.Yu.Ageyev
    • Proceedings of the Optical Society of Korea Conference
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    • 2000.02a
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    • pp.236-237
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    • 2000
  • 용액인상법에 의하여 Cr$^{3+}$ 이온이 0.1-0.2% 주입된 Alexandrite (Cr$^{3+}$ :BeAl$_2$O$_4$) 단결정을 성장하고, 성장한 단결정을 이용하여 레이저 소자를 제조하였다. 고품질의 단결정을 성장할 수 있는 결정성장조건을 규명하고, Cr$^{3+}$ 이온의 유효편석 계수를 계산하였으며, 결정 결함 및 분광 물성을 조사하였다. 결정성장 실험 결과, 유속 3 1/min의 질소분위기, 이리듐 도가니 및 <001>방위의 Alexandrite 단결정을 종자결정으로 사용하여 결정을 성장하는 경우 최적의 결정성장 조건은 인상속도 0.5-1.0 mm/hr와 회전속도 20-25 rpm이었다. 육성된 결정은 (100)면이 넓게 발달되었으며, (120)과 (010)면이 측면에 발달되는 판상의 직팔각기둥의 형태로 성장되었다. 결정결함으로써 parasite crystal의 형성과 경계면의 균열, striation, inclusion 등이 검출되었다. Alexandrite 단결정 내에 분포하는 Cr$^{3+}$ 이온의 유효편석계수 k$_{eff}$는 2.8로 계산되었다. 분광물성으로써 실온에서의 $^4$A$_2$$\longrightarrow$$^4$T$_2$(689.6-489.3 nm), $^4$A$_2$$\longrightarrow$$^4$T$_1$(489.3-311.33m) 천이에 의한 흡수를 확인하고, $^4$T$_2$$\longrightarrow$$^4$A$_2$(650-800 nm), $^2$E$\longrightarrow$$^4$A$_2$에 의한 nophonon line R$_1$, R$_2$(680.4, 678.5 nm) 및 $^2$T$_1$$\longrightarrow$$^4$A$_2$(655.7, 649.3, 645.2 nm)의 형광방출 스펙트럼을 얻었으며, 형광수명은 0.264 ms로 조사되었다. 제조된 레이저 발진봉은 직경 6.3 m, 길이 45 nm이었다.

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Application of Mechanical Crack Model to Numerical Study of Rock Mass Behavior (암석거동의 수치해석적 연구를 위한 균열모형의 적용)

  • Park, Do-hyun;Jeon, Seok-won
    • Journal of Korean Tunnelling and Underground Space Association
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    • v.2 no.2
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    • pp.72-85
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    • 2000
  • Rock is a very complex and heterogeneous material, containing structural flaws due to geologic generation process. Because of those structural flaws, deformation and failure of rock when subjected to differential compressive stresses is non-linear. To simulate the non-linear behavior of rock, mechanical crack models, that is, sliding and shear crack models have been used in several studies. In those studies, non-linear stress-strain curves and various behaviors of rock including the changes of effective elastic moduli ($E_1$, $E_2$, ${\nu}_1$, ${\nu}_2$, $G_2$) due to crack growth were simulated (Kemeny, 1993; Jeon, 1996, 1998). Most of the studies have mainly focused on the verification of the mechanical crack model with relatively less attempt to apply it to practical purposes such as numerical analysis for underground and/or slope design. In this study, the validity of mechanical crack model was checked out by simulating the non-linear behavior of rock and consequently it was applied to a practical numerical analysis, finite element analysis commonly used.

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Effects of Cdc31, a component of TREX-2 complex, on growth and mRNA export in fission yeast (분열효모에서 TREX-2 복합체의 구성요소인 Cdc31이 생장과 mRNA export에 미치는 영향)

  • Koh, Eun-Jin;Yoon, Jin Ho
    • Korean Journal of Microbiology
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    • v.52 no.3
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    • pp.383-387
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    • 2016
  • In fission yeast, Schizosaccharomyces pombe, the cdc31 gene encodes a member of the conserved $Ca^{2+}$-binding centrin/CDC31 family, which is a component of spindle pole body. Here, we demonstrate that the S. pombe cdc31p is also a component of TREX-2 complex, which influences mRNA export from the nucleus to the cytoplasm. Repression of the cdc31 gene expression caused growth defect with accumulation of $poly(A)^+$ RNA in the nucleus. On the other hand, over-expression of cdc31 exhibited no defects of both growth and bulk mRNA export, but showed somewhat longer cell morphology. Yeast two-hybrid analysis showed that Cdc31 interacted with Sac3 and Pci2, the subunits of TREX-2 complex. These results suggest that S. pombe Cdc31 is also involved in mRNA export as a component of TREX-2 complex.

Elastic Wave Detection using Fiber Optic FBG Sensor (광섬유 FBG 센서를 이용한 탄성파 검출)

  • Seo, Dae-Cheol;Kwon, Il-Bum;Yoon, Dong-Jin;Lee, Seung-Suk;Lee, Jung-Ryul
    • Journal of the Korean Society for Nondestructive Testing
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    • v.30 no.1
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    • pp.1-5
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    • 2010
  • Acoustic emission(AE) has emerged as a powerful nondestructive tool to detect or monitor preexisting defects and leaks in the vessel structures. A Bragg grating based acoustic emission sensor system is developed. Various type of fiber Bragg grating sensor including the variable length of sensing part was fabricated and prototype sensor system was tested by using PZT pulser and pencil lead break sources. Two types of sensor attachment were used. First, the fiber Bragg grating sensor was attached fully to the surface using bonding agent. Second one is that one part of fiber was attached to the surface partly by bonding and the other part of fiber will be act as a cantilever. That is, the resonant frequency of the fiber Bragg grating sensor will depend on the length of sensing part. The final goal of the sensor system is to provide on-line monitoring of cracks or leaks in reactor vessel head penetration of nuclear power plants.

Evaluation of Influences of Artificial Defect of Wood Deck Using Non-destructive Ultrasonic Testing (목재 데크재의 초음파 비파괴시험에 의한 인위적인 결함의 영향평가)

  • Oh, Sei-Chang
    • Journal of the Korean Wood Science and Technology
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    • v.44 no.1
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    • pp.1-8
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    • 2016
  • Non-destructive ultrasonic testing was applied to evaluate the performance of wood deck material with hole as artificial defect. Ultrasonic velocities and modulus of elasticity were measured according to different diameters and numbers of holes, and comparative analysis to each data were done. From the results, ultrasonic velocities and modulus of elasticity decreased with an increase in the hole size and showed a negative linear correlation with the size of hole, respectively. As the hole size increased, ultrasonic velocities decreased, but their difference was small in the case of the hole size under 15 mm. Also, ultrasonic velocities and modulus of elasticity decreased with increasing the number of holes and showed a strong negative linear correlation to the number of holes. As the number of holes increased, ultrasonic velocities decreased to 3.5%, but modulus of elasticity decreased to 27%. Therefore, the number of holes showed greater influence to modulus of elasticity than ultrasonic velocity. Overall, the size and number of holes influenced to ultrasonic velocity and modulus of elasticity, and their influence will be greater as the size and number of holes increases. These results suggested that several ultrasonic parameters rather than a single ultrasonic velocity should be applied to detect small defects in wood decking materials.

효과적인 일함수 조절을 위한 그래핀-고분자의 적층 구조

  • Cha, Myeong-Jun;Kim, Yu-Seok;Jeong, Min-Uk;Song, U-Seok;Jeong, Dae-Seong;Lee, Su-Il;An, Gi-Seok;Park, Jong-Yun
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.210-210
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    • 2013
  • 그래핀은 뛰어난 기계적, 화학적, 광학적, 전기적 특성을 가지고 있는 2차원 물질로, 대면적 합성법과 전사 공정을 통해 다양한 기판에서의 사용이 가능해지면서 차세대 전자 소자로 활용하기위한 활발한 연구가 이루어지고 있다. 디스플레이, 태양전지의 전극과 전계 효과 트랜지스터의 채널로 적용한 연구에서 우수한 결과들을 보이고 있다. 특히, 금속/금속 산화물 전극은 염료 감응형 태양전지와 유기 발광 다이오드 구조에서 화학적으로 불안정할 뿐 아니라 일함수가 고정되어 쇼트키 접촉이 형성되면 저항을 낮추기 어렵지만, 그래핀은 금속/금속 산화물 전극보다 화학적으로 안정하고 일함수의 조절이 가능해 옴 접촉 형성에 용이하다. 그래핀의 일함수를 조절하는 연구는 크게 공유결합과 비공유 결합을 이용한 방법이 시도된다. 공유 결합을 이용한 방법은 합성과정에서 그래핀의 구조에 내재된 결함 혹은 새로운 결함을 형성하여 다른 원소를 첨가하는 방법이다. 이러한 방법은 그래핀의 결함 영역에서 작용하기 때문에 그래핀 전자 구조의 높은 수준 조절을 위해선 그래핀 구조의 파괴가 동반된다. 반면, 비공유 결합을 이용한 방법은 전하 이동 도핑 효과를 이용해 그래핀의 전자 구조를 제어하는 방법으로, 금속/금속산화물/기능기와 그래핀의 적층으로 복합 구조를 형성하는 방법이다. 금속/금속 산화물과의 복합구조는 안정적인 p-형 도핑이 보고되었지만, n-형 도핑은 대기중의 수분, 산소 그리고 기판과의 상호작용에 의해 대기중에서 불안정해 추가적인 피막공정이 요구된다. 기능기를 이용한 적층 구조는 그래핀과 기판사이의 상호작용 혹은 그래핀 전자 구조를 다양한 기능기를 이용해 제어하는 것으로, 이극성을 가진 자기정렬 단일층(self-assembled monolayers)이 대표적인 방법이다. 공간기(spacer)의 길이나 말단기(end group)의 종류로 p-형과 n-형의 도핑 수준을 제어할 수 있지만, 흡착기(chemisorbing groups)의 반응성이 기판의 화학적, 물리적 표면상태에 의존하기때문에 기판 선택이 제약되며 전처리 공정이 요구될 수 있는 한계가 있다. 본 연구에서는 다양한 기판에 적용가능한 용액 공정을 이용해 그래핀과 고분자를 적층하였고, 안정적이고 효과적으로 일함수를 낮추는 구조를 확인하였다.

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Transient neonatal diabetes mellitus with macroglossia diagnosed by methylation specific PCR (MS-PCR) (메틸화 특이 PCR로 진단된 거설증을 동반한 일과성 신생아 당뇨병)

  • Jin, Hye Young;Choi, Jin-Ho;Kim, Gu-Hwan;Yoo, Han-Wook
    • Clinical and Experimental Pediatrics
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    • v.53 no.3
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    • pp.432-436
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    • 2010
  • Transient neonatal diabetes mellitus (TNDM) has been associated with paternal uniparental isodisomy of chromosome 6, paternally inherited duplication of 6q24, or a methylation defect at a CpG island of the ZAC or HYMAI gene. We experienced a case of TNDM in which the patient presented with hyperglycemia, macroglossia, and intrauterine growth retardation, caused by a paternally derived HYMAI. An 18-day-old female infant was admitted to the hospital because of macroglossia and recurrent hyperglycemia. In addition to the macroglossia, she also presented with large fontanelles, micrognathia, and prominent eyes. Serum glucose levels were 200-00 mg/dL and they improved spontaneously 2 days after admission. To identify the presence of a maternal methylated allele, bisulfite-treated genomic DNA from peripheral blood was prepared and digested with BssHII after polymerase chain reaction (PCR) amplification with methylation-specific HYMAI primers. PCR and restriction fragment length polymorphism analysis showed that the patient had only the paternal origin of the HYMA1 gene. TNDM is associated with a methylation defect in chromosome 6, suggesting that an imprinted gene on chromosome 6 is responsible for this phenotype.

A Strategy of a Gap Block Design in the CFRP Double Roller to Minimize Defects during the Product Conveyance (제품 이송 시 결함 최소화를 위한 CFRP 이중 롤러의 Gap block 설계 전략)

  • Seung-Ji Yang;Young-june Park;Sung-Eun Kim;Jun-Geol Ahn;Hyun-Ik Yang
    • Composites Research
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    • v.37 no.1
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    • pp.7-14
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    • 2024
  • Due to the structural characteristic of a double roller, the double roller can have various deformation behaviors depending on a gap block design, even if dimensions and loading conditions for the double roller are the same. Based on this feature, we propose a strategy for designing the gap block of the carbon-fiber reinforced plastic (CFRP) double roller to minimize defects (e.g., sagging and wrinkling), which can be raised during the product conveying process, with the pursue of the lightweight design. In the suggested strategy, analysis cases are first selected by considering main design parameters and engineering tolerances of the gap block, and then deformation behaviors of these selected cases are extracted using the finite element method (FEM). Here, to obtain the optimal gap block parameters that satisfy the purpose of this study, deformation deviations in the contact area are calculated and compared using the extracted deformation behaviors. Note that the contact area in this work is located between the product and the roller. As a result, through the design method of the gap block proposed in this work, it is possible to construct the CFRP double roller that can significantly decrease the defects without changing the overall sizes of the roller. A detailed method is suggested herein, and the results are evaluated in a numerical way.

MBE 법으로 선택적 성장된 GaN 나노선의 광/구조 특성 조사

  • Lee, Sang-Tae;Jeon, Seung-Gi;Choe, Hyo-Seok;Kim, Mun-Deok;O, Jae-Eung;Kim, Song-Gang;Yang, U-Cheol
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.08a
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    • pp.355-355
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    • 2012
  • Si (111) 기판 위에 polystyrene (PS) bead를 사용하여 만들어진 약 100 nm 나노 구멍에 GaN나노선을 molecular beam epitaxy 법으로 성장하였다. 성장 온도와 III/V 비율 변화에 대하여 성장된 GaN 나노선의 모양과 광학적 특성은 scanning electron microscopy (SEM)와 photoluminescence (PL) 등으로 조사하였으며, InN/GaN 이종접합 및 InGaN p-n 다이오드구조를 성장하여 atomic force microscopy의 tip 접촉방법으로 전기적 특성을 조사하였다. PL 측정 결과 성장온도가 높아지면 Ga 빈자리와 관계된 3.28 eV의 donor acceptor pair (DAP) 신호와 3.42 eV의 stacking faults (SF) 결함에 기인된 발광 신호세기가 감소하는 결과를 SEM으로부터 나노선 폭 및 길이는 좁아지면서 짧아지는 것을 관측하였다. 또한 nitrogen 원자양이 증가하면서 Ga 빈자리와 관련된 3.28 eV DAP 신호가 증가하는 것을 관측하였다. 이들 결과로부터 GaN 나노선의 SF 발광 신호관련 원인에 대하여 논의 하였다. AFM을 이용한 I-V 측정으로부터 성장조건 변화에 따른 GaN 나노선 및 p-n 접합 나노선의 전도 특성을 조사하여 나노선의 소자 응용에 대한 기본적인 물리특성을 규명하였다.

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Crystal Growth and Photoluminescence Property of Stoichiometric LiNbO3 Single Crystal Fiber by Addition of Nd2O3 (Nd\2O3 첨가에 따른 화학양론조성 LiNbO3 단결정의 성장 및 형광특성)

  • Shur, Joong-Won;Yoon, Seok-Gyu;Lee, Sung-Mun;Yoon, Dae-Ho
    • Journal of the Korean Ceramic Society
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    • v.39 no.10
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    • pp.977-980
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    • 2002
  • Using the micro-pulling down method, $Nd_2O_3$ doped crack-free stoichiometric $LiNbO_3$ single crystals were grown in 1 mm diameter and 30∼35 mm length. The homogeneous distributions of $Nd_2O_3$ concentration were confirmed by the electron probe micro analysis. The absorption and photoluminescence spectra were measured with respect to the $Nd_2O_3$ doping.