• Journal of the Korean Ceramic Society
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• v.15 no.3
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• pp.127-134
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• 1978

탄도충격에 의하여 파괴된 단결정 alumina의 파면조직을 광학 및 투과 전자현미경으로 연구 분석하였다. 파면의 주된 파괴 양상은 결정 입개면의 분리 또는 결정입내 파괴로 구성되어 있고 이러한 파괴과정은 복잡한 cleavage 양상과 결정입자 내에서의 소성변형을 수반하고 있다. 미세조직 관찰 결과에 의하면 alumina ceramics의 충격 파괴과정에서 에너지의 흡수가 국부적인 소성변형으로 나타나고 있음을 알 수 있었다.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.30 no.4
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• pp.136-142
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• 2020

Crystallization of zinc crystalline glaze requires demanding conditions such as the formation of a nucleating agent and the amount of nucleating agent, and growth of crystalline. Zinc crystalline glaze is hard to utilize in the industry because of its narrow range of the firing temperature, and the crystallization's dependency on the quality of zinc. Stimulation of zinc crystallization and formation of frit enable zinc crystalline glaze to be reconstituted in a various range of firing schedules, leading to the development of a competitive industrial glaze.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2001.10a
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• pp.309-312
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• 2001

FEM simulating system of the cross-rolling texture formation offers a systematic and efficient way of exploring the relationship between the process variables and the state of plastic anisotropy of sheet product. Cross-rolled sheets possess higher average plastic strain ratios and lower planer anisotropy than those of the straight-rolled sheets. The employed model is a finite-element polycrystal model which each element used in FEM is assumed to be a crystal having different orientation by Takahashi. Texture development, deformation textures due to cross-rolling are predicted for face-centered cubic sheet metal. Crystal orientations are assigned on the basis of the pole figures obtained by X-ray diffraction. Development of anisotropy during cross rolling of an fcc sheet material is predicted theoretically with respected to flow stress and R-value in tensile test.

• Journal of the Korean Ceramic Society
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• v.37 no.12
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• pp.1178-1186
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• 2000

타일의 내마모성과 내산성을 향상시키기 위해 결정화유리가 최근에 새로운 유약 재료로서 소개되고 있다. 신 유약의 연구에 사용된 조성은 $Ca_2$ZrSi$_4$O$_{12}$ 상에 근접하는 CaO-ZrO$_2$-SiO$_2$계의 유리조성의 분말로, 마이크로파 가열 (2.45 GHz)에 의해서 900-120$0^{\circ}C$의 0-20분간 소성되어 평가되었다. 그 결과, 100$0^{\circ}C$ 이상에서 소성한 시편은 내부 결정화를 나타내었으며, 결정상은 미세(5$mu extrm{m}$)한 크기를 갖는 $Ca_2$ZrSi$_4$O$_{12}$가 주 결정상이며, $Ca_2$ZrSi$_4$O$_{12}$, CaSiO$_3$, SiO$_2$의 세 상이 나타났다. 소결체의 미세구조는 사용한 유리분말의 입도의 영향을 받았다. 미세분말 (<38$\mu\textrm{m}$)을 이용한 소결체의 조직이 조세분말 (45-150$\mu\textrm{m}$)의 경우보다 수축율면에서 높았으며 낮은 기공도를 갖는 미세구조를 가졌다. 마이크로파에 의한 유리분말의 소성은 1000-120$0^{\circ}C$ 구간에서 10분 이내 결정화가 완료되는 급속 가열 공정이었으며 CaO-ZrO$_2$-SiO$_2$계 결정화 유리 제조에 균일한 체적가열을 할 수 있었다.

• Journal of the Korean Society for Precision Engineering
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• v.15 no.5
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• pp.167-175
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• 1998

A mathematical formulation is presented to model anisotropy from the deformation textures developed in a forming process. In this work, a micro-mechanical-based polycrystalline analysis is implemented into a consistent finite element method for the anisotropic, viscoplastic deformation of polycrystalline metals. As suggested by Taylor, the deformation of each grain in an aggregate is assumed to be same as the macroscopic deformation of an aggregate or a macro-continuum point. Algorithms are developed to represent the plastic anisotropy, such as the anisotropic yield surface and R-value, from the predicted deformation texture. As applications, the evolution of texture in rolling, upsetting and drawing/extrusion processes are simulated and the corresponding changes of mechanical properties such as yield surface and R-value are predicted.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.33 no.6
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• pp.234-243
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• 2023

Zinc crystals of ZnO and SiO₂ in glaze raw materials, developed according to composition and firing requirements, are preferred because of their high decorative properties. However, most zinc crystal glazes have a high firing temperature and a narrow firing temperature range, making it difficult to use them as commercial glazes in ceramics. Therefore, in this study, it was expected that the firing temperature of a typical zinc crystal glaze could be lowered to below 1270℃ by using the eutectic effect through mixing frit, the main raw material used in manufacturing zinc crystal glaze. As a result, not only was the formation temperature of zinc crystals lower in the mixed frit glaze, but also the firing temperature range was widened to 1230~1270℃, making it possible to develop a glaze that produces crystals stably. The firing temperature was lowered to 1230~1250℃ and the holding temperature during cooling was lowered to about 950℃, resulting in the development of an economically effective glaze. When using a combination of frit, it has been shown that the holding temperature during cooling affects the recrystallization of zinc crystals depending on the composition of the glaze, and the crystal structure can be adjusted at this time. Additionally, the amount and shape of crystals can be controlled by using a nucleating agent.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.05a
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• pp.282-284
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• 2007

The hardening and the constitutive equation based on the crystal plasticity are introduced for the numerical simulation of hemispherical sheet metal forming. For calculating the deformation and the stress of the crystal, Taylor's model of the crystalline aggregate is employed. The hardening is evaluated by using the Taylor factor, the critical resolved shear stress of the slip system, and the sum of the crystallographic shears. During the hemispherical forming process, the texture of the sheet metal is evolved by the plastic deformation of the crystal. By observing the texture evolution of the BCC sheet, the texture evolution of the sheet is traced during the forming process. Deformation texture of the BCC sheet is represented by using the pole figure. The comparison of the strain distribution and punch force in the hemispherical forming process between crystal plasticity and experiment shows the verification of the crystal-based formulation and the accuracy of the hardening and constitutive equation obtained from the crystal plasticity.

• Transactions of Materials Processing
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• v.5 no.4
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• pp.297-304
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• 1996

A process model is formulated considering the effect of crystallographic texture developed in forming process. The deformation induced plastic anisotropy can be predicted by capturing the evolution of texture during large deformation in the polycrystalline aggregate. The anisotropic stiffness matrix for the aggregate is derived and implemented in Eulerian finite element code using a Consistent Penalty method. As an application the evolution of texture in rolling drawing and extrusion processes are simulated. The numerical results show good agreements with report-ed experimental textures.

• Journal of the Korean Society for Precision Engineering
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• v.29 no.8
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• pp.818-823
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• 2012

In order to predict necking behaviour of aluminium sheets, a crystal plasticity model is introduced in the finite element analysis of tensile test. Due to the computational limits of time and memory, only a small part of tensile specimen is subjected to the analysis. Grains having different orientations are subjected to numerical tensile tests and each grain is discretized by many elements. In order to predict the sudden drop of load carrying capacity after necking, a well-known Cockcroft-Latham damage model is introduced. The mismatch of grain orientation causes stress concentration at several points and damage is evolved at these points. This phenomenon is similar to void nucleation. In the same way, void growth and void coalescence behaviours are well predicted in the analysis. For the comparison of prediction capability of necking, same model is subjected to finite element analysis using uniform material properties of polycrystal with and without damage. As a result, it is shown that the crystal plasticity model can be used in prediction of necking and fracture behavior of materials accurately.

• Journal of the Mineralogical Society of Korea
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• v.21 no.2
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• pp.209-224
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• 2008

Various types of high-purity limestone, which occurred in the Pungchon Formation, are examined to understand applied-mineralogical factors controlling their calcination characters with respect to the ore characters. To do this work, systematic characterization and determination were carried out for the limestone ores and their calcination products in a fixed heating condition, and the results were correlated and discussed. During the calcination experiment, a phase transition from calcite to quicklime begins to occur selectively in the physical weak zones such as grain boundary, cleavage and twin planes. All the fabrics of original limestones are preserved in the resultant quicklime. In addition, crystallinity of the quicklime was advanced, as the aging time of calcination was increased. Major controlling factors on the calcination effects of the high-purity limestone are elucidated to be the degree of development of cleavage and twin, together with crystallinity and textures in the limestone ore. Especially, lower crystallinity and dense interlocking fabrics obviously play advantageous role in all the calcination characters. But the development of cleavage and twin affects negatively on the calcination characters on account of favoring decrepitaion of quicklime in the lime manufacturing. Thus, the high-purity limestones characteristic of marble fabrics and relatively lower crystallinity are comparatively advantageous for the uses of lime manufacture.