• Title/Summary/Keyword: $ZrO_2$ Monolithic Ceramics

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Determining Mechanical Properties of ZrO2 Composite Ceramics by Weibull Statistical Analysis (와이블 통계 해석에 의한 ZrO2 복합 세라믹스의 기계적 특성)

  • Kim, Seon Jin;Kim, Dae Sik;Nam, Ki Woo
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.39 no.10
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    • pp.955-962
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    • 2015
  • The Vickers test can be used for all types of materials, and it has one of the widest scales among hardness tests. The hardness may be considered as a probability variable when evaluating the mechanical properties of materials. In this study, we investigate the statistical properties of the bending strength and Vickers hardness in $ZrO_2$ monolithic and $ZrO_2/SiC$ composites depending on the amount of $TiO_2$ additives. The bending strength and Vickers hardness were found to agree well with the Weibull probability distribution. We evaluate the scale parameter and shape parameter in as-received $ZrO_2$ and $ZrO_2/SiC/TiO_2$ ceramics, as well as their heat treated ceramics. We also evaluate the parameters in accordance with the increase in in the indentation load.

Electrical properties of Low Fired Pb(Mg,Te,Mn,Nb)$O_3-Pb(Zr,Ti)O_3$ Ceramics (저온에서 소결한 Pb(Mg,Te,Mn,Nb)$O_3-Pb(Zr,Ti)O_3$세라믹스의 전기적 특성)

  • 정수태;조상희
    • Electrical & Electronic Materials
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    • v.9 no.7
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    • pp.652-659
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    • 1996
  • Sintering characteristics and electrical properties of xPb(Mg$_{1}$8/Te$_{1}$8/Mn$_{1}$4/Nb$_{1}$2/) $O_{3}$-(1-x) Pb (Zr$_{1}$2/ $Ti_{1}$2/) $O_{3}$ (x=0.075, 0.1, 0.125) ceramics are investigated. A sintering temperature of ceramics could be reduced to 950.deg. C by a reaction between PbO and B site compound material. The physical properties of 0.1Pb(Mg, Te, Mn, Nb) $O_{3}$ - 0.9Pb(Zr, Ti) $O_{3}$ bulk ceramic with 3wt% glass frit(0.857PbO-0.143W $O_{3}$) were following : den = 7.95 g/cm$^{3}$, T$_{c}$=340.deg. C, .epsilon.$_{33}$= 754, k$_{31}$=0.3 and Q.=1780. The 3-layer piezoelectric transformer by using a tape casting method showed a good monolithic structure, and its voltage setup ratio was 2.5 times higher than that of a single device by using bulk ceramics.s.s.

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Mechanical Characteristics and Crack-Healing of ZIRCONIA(ZrO2) Composite Ceramics with SiC and TiO2 (SiC와 TiO2 첨가에 따르는 ZrO2의 기계적 특성 및 균열 치유)

  • Nam, Ki Woo
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.40 no.3
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    • pp.267-273
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    • 2016
  • This study evaluated the mechanical properties and crack-healing abilities of zirconia composite ceramics. The six kinds of specimens used were: partially stabilized zirconia (Z) and five zirconia composite (ZS, ZST1, ZST2, ZST3, and ZST5) with SiC and $TiO_2$. There was not a large difference between the Vickers hardness of the six types of zirconia ceramics. The bending strength of the ZS specimen degraded rapidly, but the zirconia specimens with $TiO_2$ (ZST1, ZST2, ZST3, and ZST5) showed improved strength. Therefore, it was determined that the bending strength is affected by the crystallization, which is due to the addition of SiC and $TiO_2$. From the crack-healing conditions having the highest bending strength, monolithic zirconia retained its cracks, while the specimens of four types with SiC healed their cracks.

Microstructure and EDM Processing of $MoSi_2$ Intermetallic Composite ($MoSi_2$ 금속간화합물 복합재료의 미세구조와 방전가공특성)

  • Yoon, Han-Ki;Lee, Sang-Pill;Yoon, Kyong-Wok;Kim, Dong-Hyun
    • Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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    • 2002.05a
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    • pp.23-28
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    • 2002
  • This paper describes the machining characteristics of the $MoSi_2$ based composites by electric discharge drilling with various tubular electrodes, besides, Hardness characteristics and microstructures of $Nb/MoSi_2$ laminate composites were evaluated from the variation of fabricating conditions such as preparation temperature, applied pressure and pressure holding time. $MoSi_2$ -based composites has been developed in new materials for jet engine of supersonic-speed airplanes and gas turbine for high- temperature generator. Achieving this objective may require new hard materials with high strength and high temperature-resistance. However, With the exception of grinding, traditional machining methods are not applicable to these new materials. Electric discharge machining (EDM) is a thermal process that utilizes a spark discharge to melt a conductive material, the tool electrode being almost non-unloaded, because there is no direct contact between the tool electrode and the workpiece. By combining a nonconducting ceramics with more conducting ceramic it was possible to raise the electrical conductivity. From experimental results, it was found that the lamination from Nb sheet and $MoSi_2$ powder was an excellent strategy to improve hardness characteristics of monolithic $MoSi_2$. However, interfacial reaction products like (Nb, Mo)$SiO_2$ and $Nb_2Si_3$ formed at the interface of $Nb/MoSi_2$ and increased with fabricating temperature. $MoSi_2$ composites which a hole drilling was not possible by the conventional machining process, enhanced the capacity of ED-drilling by adding $NbSi_2$ relative to that of SiC or $ZrO_2$ reinforcements.

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