• Title/Summary/Keyword: $SF_6$ Refinement

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Installation and Test Run of Comprehensive Analysis System for SF6 in Power Equipment

  • Lee, Jeong Eun;Kim, Kwang Sin;Kim, Ah Reum;Park, Seoksoon;Kim, Kyeongsook
    • KEPCO Journal on Electric Power and Energy
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    • v.3 no.1
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    • pp.41-47
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    • 2017
  • After $SF_6$, which is being used in power equipment as an insulating material, is classified as one of the 6 major greenhouse gases, the maintenance and the refinement of used $SF_6$ started to get attention. In regard to this, KEPCO Research Institute (KEPRI) is developing $SF_6$ recovery and refinement technology starting with establishing a comprehensive $SF_6$ analysis system. With the analysis system, qualitative and quantitative analyses of the purity and the impurities of $SF_6$ before and after recovery, and before and after refinement have been carried out. The analysis system is comprised of GC-DID (Gas Chromatograph -Discharge Ionization Detector) for trace impurities analysis, GC-TCD (Thermal Conductivity Detector) for analyses of $SF_6$ purity and major impurities concentration from several hundred ppm up to percent range, GC-MSD (Mass Selective Detector) for analyses of impurities not included in standard gas, FT-IR (Fourier Transform-Infrared) Spectrometer for analysis of HF and $SO_2$, and moisture analyzer for analysis of moisture below 100 ppm. With this analysis system, complete analysis method of $SF_6$ has been established. This analysis system is being used in the maintenance of power equipment and the development of $SF_6$ recovery and refinement technologies. In this paper, the analysis results of four samples - gas and liquid phase $SF_6$ samples from a $SF_6$ refinement system before and after refinement are presented.

Improved sulfur hexafluoride(SF6) gas analysis method for quality management of cryogenic refinement system (극저온 정제시스템의 품질관리를 위한 SF6 가스 분석방법 개선)

  • Lee, Jeong Eun;Cho, Min-ho;Lee, Won Seok
    • KEPCO Journal on Electric Power and Energy
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    • v.8 no.1
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    • pp.37-41
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    • 2022
  • Because sulfur hexafluoride(SF6) is classified as one of the six major greenhouse gases, SF6 handling in power plant such as recovery, purification, and reuse is considered to be important. KEPCO has focused to develop the advanced recovery and purification technology of SF6 reuse. SF6 analysis includes the on-site analyses and on-line analyzer; i.e., (1) on-site analysis has an error rate of ±0.5% and (2) on-line analysis has an error rate of ±0.1%, which is possible to adjust operating conditions and to make the work more conveniently by analyzing SF6 concentration before and after purification step. This paper presents an online analysis method in the SF6 purification and reuse system. In addition, the analysis results and quality guarantees for each section of the analysis system were presented.

Effect of Cerium on the Microstructure and Room Temperature Tensile Properties of Mg-4Al-2Sn-1Si Alloys (Mg-4Al-2Sn-1Si 합금의 조직 및 상온 인장 특성에 미치는 Ce의 영향)

  • Kim, Jung-Hoon;Cho, Dae-Hyun;Park, Ik-Min
    • Journal of Korea Foundry Society
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    • v.32 no.6
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    • pp.289-295
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    • 2012
  • Mg-Al-Sn-Si system alloy, as a promising cheap heat-resistant Mg alloy for automobile engine part, has been investigated. Refinement of microstructure and precipitation of thermally stable secondary phases are important goal for the design of heat-resistant Mg alloy. In this study, the effect of Ce on the microstructure and room temperature mechanical properties of Mg-Al-Sn-Si alloy was investigated. High thermally stable $Mg_2Si$ phases in Mg-Al-Sn-Si alloy is very useful intermetallic compound. However, the $Mg_2Si$ phases often result in poor mechanical properties due to the coarse chinese type $Mg_2Si$ phases. The experimental specimens were fabricated by fluxless melting under $CO_2+SF_6$ atmosphere and poured into the permanent pre-heated at $200^{\circ}C$. It was told that Ce addition can modify $Mg_2Si$ phases and refine microstructure and improve the tensile strength, yield strength and elongation.

Mechanical Properties of 0.25-0.65wt% CaO added AM60B Eco-Mg Diecastings at room and Elevated Temperatures (0.25-0.65wt% CaO 첨가 AM60B Eco-Mg 다이캐스팅 부품의 상온 및 고온 기계적 특성)

  • Seo, Jung-Ho;Kim, Shae-K.
    • Journal of Korea Foundry Society
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    • v.31 no.1
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    • pp.11-17
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    • 2011
  • The effect of CaO addition to AM60B Mg alloy on tensile properties has been investigated, with focus on strength and ductility at room and elevated temperatures. The 0.25-0.65wt% CaO added AM60B Eco-Mg diecastings were prepared by high pressure die casting using Buhler 1,450-ton cold chamber machine without $SF_6$ and $SO_2$ gases. The microstructures and tensile properties of each alloy were tested. The results show that the grains of AM60B are refined and the mechanical properties increase with CaO addition at room temperature. The improvement of strength and ductility is prominent at 0.45-0.55wt% CaO addition. Also, improved mechanical properties are maintained at elevated temperature of $150^{\circ}C$. CaO addition results in $Al_2Ca$ phase formation mostly on the grain boundaries. This phase leads to the refinement of grain structures and improvement of ductility as well as strength. The suppression of ${\beta}-Mg_{17}Al_{12}$ phase as well as the decrease of fracture surface porosity and other casting defects caused by melt cleanliness also contribute to the enhancement of mechanical properties of AM60B Eco-Mg at room and elevated temperature.