• Title/Summary/Keyword: $MgB_4$ addition

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Degradation and mineralization of violet-3B dye using C-N-codoped TiO2 photocatalyst

  • Putri, Reza Audina;Safni, Safni;Jamarun, Novesar;Septiani, Upita;Kim, Moon-Kyung;Zoh, Kyung-Duk
    • Environmental Engineering Research
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    • v.25 no.4
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    • pp.529-535
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    • 2020
  • The present study investigated the photodegradation of synthetic organic dye; violet-3B, without and with the addition of C-N-codoped TiO2 catalyst using a visible halogen-lamp as a light source. The catalyst was synthesized by using a peroxo sol-gel method with free-organic solvent. The effects of initial dye concentration, catalyst dosage, and pH solution on the photodegradation of violet-3B were examined. The efficiency of the photodegradation process for violet-3B dye was higher at neutral to less acidic pH. The kinetics reaction rate of photodegradation of violet-3B dye with the addition of C-N-codoped TiO2 followed pseudo-first order kinetics represented by the Langmuir-Hinshelwood model, and increasing the initial concentration of dyes decreased rate constants of photodegradation. Photodegradation of 5 mg L-1 violet-3B dye achieved 96% color removal within 240 min of irradiation in the presence of C-N-codoped TiO2 catalyst, and approximately 44% TOC was removed as a result of the mineralization.

Physicochemical Properties of Mucilage from Domestic Molokhia (Corchorus olitorius) (몰로키아(Corchorus olitorius) 잎에서 추출한 mucilage의 이화학적 특성)

  • Jung, Chang-Hwa;Choi, In-Wook;Kim, Heung-Man;Seog, Ho-Moon
    • Korean Journal of Food Science and Technology
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    • v.34 no.5
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    • pp.757-761
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    • 2002
  • Proximate composition, phenolic compounds, and amino acid composition of molokhia (Corchorus olitorius) and molecular weight distribution of its mucilage were determined. Concentrations of dietary fibers and protein were 37.4 and 24.4% of the total dry weight, respectively. Mucilage was obtained by extracting dry molokhia leaves with hot water, followed by the addition of 55% ethanol. Although about 50% of the mucilage was lost during the extration, it was still rich in polyphenol compounds. In mucilage, proteins were composed of glutamic acid, glycine, alanin, and aspartic acid, and molecular weight of most polysaccarides ranged from $40,000{\sim}500,000$ daltons based on gel filtration chromatography.

Comparison of Quality Characteristics of Korean Cabbage Kimchi Added with Germinated Brown Rice Extracts and Korean Cabbage Kimchi on the Market (발아현미 추출물 첨가 배추김치와 시판배추김치의 품질특성 비교)

  • Woo, Seung-Mi;Wool, Sang-Chul;Jeong, Yong-Jin
    • Food Science and Preservation
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    • v.13 no.6
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    • pp.789-795
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    • 2006
  • This study was designed to investigate quality characteristics of Korean cabbage kimchi added with germinated brown rice extracts (GBRC; (A) and CBREP; (B)) and Korean cabbage kimchi on the market mom the result pH and total acidity were shown to be similar in all samples. In the case of Korean cabbage kimchi added with (A) and (B), content of total sugar and reducing sugar were higher than those of Korean cabbage kimchi on the market. Color values (L, b) were shown to be similar in all samples in which a value was lower than that of Korean cabbage kimchi on the market. The amounts of total amino acid and free amino acid of Korean cabbage kimchi added (A) and (B) were higher than those of Korean cabbage kimchi on the market. But the amount of $\gammma$-aminobutyric acid (GABA) in main functional components of germinated brown rice was shown to be low. Total phenol content and other antioxidant and anticoagulant activities of Korean cabbage kimchi fortified with (A) and (B) were higher than those of Korean cabbage kimchi on the market. In conclusion, Korean cabbage kimchi added with (A) and (B) were shown to be similar in fermentation tendency compared to Korean cabbage kimchi on the market and, the functional properties could be enhanced by the addition of (A) and (B).

Warm Tensile Deformation Behavior and Constitutive Equation of Supersaturated Solid-Solutionized Al-9Mg Extruded Alloy

  • Seung Y. Yang;Bong H. Kim;Da B. Lee;Kweon H. Choi;Nam S. Kim;Seong H. Ha;Young O. Yoon;Hyun K. Lim;Shae Kim;Young J. Kim
    • Archives of Metallurgy and Materials
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    • v.66 no.4
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    • pp.1013-1018
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    • 2021
  • In this paper, as a purpose to apply the supersaturated solid-solutionized Al-9Mg alloy to the structural sheet parts of automotive, tensile tests were conducted under the various conditions and a constitutive equation was derived from the tensile test results. Al-9Mg alloy was produced using a special Mg master alloy containing Al2Ca during the casting process and extruded into the sheet. In order to study the deformation behavior of Al-9Mg alloy in warm temperature forming environments, tensile tests were conducted under the temperature of 373 K-573 K and the strain rate of 0.001/s~0.1/s. In addition, by using the raw data obtained from tensile tests, a constitutive equation of the Al-9Mg alloy was derived for predicting the optimized condition of the hot stamping process. Al-9Mg alloy showed uncommon deformation behavior at the 373 K and 473 K temperature conditions. The calculated curves from the constitutive equation well-matched with the measured curves from the experiments particularly under the low temperature and high strain rate conditions.

Studies on the Mulberry Sapling 1. Soil Characteristics of Nursery Garden Producing Nonsprouting Sapling. (뽕나무 접목묘에 관한 연구 I. 활착불량상묘 발생 묘포지의 토양특성에 관한 연구)

  • Lee, Won-Ju;Jeong, Gwang-Yeong;Kim, Yeong-Taek
    • Journal of Sericultural and Entomological Science
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    • v.27 no.1
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    • pp.12-17
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    • 1985
  • soil survey and chemical analysis on mulberry nursery garden were carried out to study the causes of the non-sprouting phenomenon occured seriously in Buy and Ogchun in 1983 and Sangju in 1984. In addition, 115 nursery garden soils taken from 21 sapling produsers in Chungbuk province were analyzed in 1984. The results were as follows, 1. Symptom of dead saplings was the highest in boron deficiency by 59% and the lowest in rot symptom. The rest of saplings by 34.9% were not detected any symptom. 2. The nursery gardens showen non-sprouting phonomenon were located along the stream. As the result, soil depth was shallow, around 20cm deep and subsoil composed with coarse sand and gravels. 3. Nursery soils were mostly strong acid, low in Ca and Mg content, especially B, whereas available phosphorus and potassium were abundant at some gardens, and deficient at others. 4. Application of red earth or borax to nursery garden, especially to paddy, increased sprouting rate. 5. Paddy nursery garden occupied by 52.8% of 60.8ha of total garden area in Chungbuk province. Ninty point five percent of the nursery garden was lower in pH than 6.5, 87.0% lower in K than 0.5me/100g, 40.8% lower in Ca than 6.5me/100g, 94.8% lower in Mg the 2.00me/100g 99.1% lower in B than 0.3ppm.

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Hepatoprotective Effect of Flavonol Glycosides Rich Fraction from Egyptian Vicia calcarata Desf. Against $CCl_4$-Induced Liver Damage in Rats

  • Singab, Abdel Nasser B.;Youssef, Diaa T.A.;Noaman, Eman;Kotb, Saeed
    • Archives of Pharmacal Research
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    • v.28 no.7
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    • pp.791-798
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    • 2005
  • The hepatoprotective activity of flavonol glycosides rich fraction (F-2), prepared from 70% alcohol extract of the aerial parts of V calcarata Desf., was evaluated in a rat model with a liver injury induced by daily oral administration of $CCl_4$ (100 mg/kg, b.w) for four weeks. Treatment of the animals with F-2 using a dose of (25 mg/kg, b.w) during the induction of hepatic damage by $CCl_4$ significantly reduced the indices of liver injuries. The hepatoprotective effects of F-2 significantly reduced the elevated levels of the following serum enzymes: alanine aminotransferase (ALT), aspartate aminotransferase (AST), alkaline phosphatase (ALP) and lactate dehydrogenase (LDH). The antioxidant activity of F-2 markedly ameliorated the antioxidant parameters including glutathione (GSH) content, glutathione peroxidase (GSH-Px), superoxide dismutase (SOD), plasma catalase (CAT) and packed erythrocytes glucose-6-phosphate dehydrogenase (G6PDH) to be comparable with normal control levels. In addition, it normalized liver malondialdehyde (MDA) levels and creatinine concentration. Chromatographic purification of F-2 resulted in the isolation of two flavonol glycosides that rarely occur in the plant kingdom, identified as quercetin-3,5-di-O-$\beta$-D-diglucoside (5) and kaempferol-3,5-di-O-$\beta$-D-diglucoside (4) in addition to the three known compounds identified as quercetin-3-O-$\alpha$-L-rhamnosyl- (${\rightarrow}6$)-$\beta$-D-glucoside [rutin, 3], quercetin-3-O-$\beta$-D-glucoside [isoquercitrin, 2] and kaempferol-3-O-$\beta$-D-glucoside [astragalin, 1]. These compounds were identified based on interpretation of their physical, chemical, and spectral data. Moreover, the spectrophotometric estimation of the flavonoids content revealed that the aerial parts of the plant contain an appreciable amount of flavonoids (0.89%) calculated as rutin. The data obtained from this study revealed that the flavonol glycosides of F-2 protect the rat liver from hepatic damage induced by $CCl_4$ through inhibition of lipid peroxidation caused by $CCl_4$ reactive free radicals.

BOF Refining of Fluorspar Substitute Using Iron Oxide Based By-product (산화철계 형석대체제의 전로 정련특성)

  • Keum, C.H.;Hur, B.Y.
    • Korean Journal of Materials Research
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    • v.16 no.5
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    • pp.336-340
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    • 2006
  • Fluorspar has been essential flux in steelmaking process. The main effects of fluorspar addition are lowering of the viscosity and melting temperature of slag. In recent years, due to the increasing price and environmental problem of fluorspar, various types of fluorspar substitute have been investigated. In this study, iron oxide by-products such as sinter dust, basic oxygen furnace (BOF) sludge and mill scale were developed as a substitute in terms of waste recycling. Several plant trials were carried out by addition of briquetted substitutes of $4{\sim}6$ kg/ton to compare with the fluorspar of $0.7{\sim}1$ kg/ton. The substitutes showed a similar behavior of slag formation, phosphorus removal and MgO saturation content.

A Study for the Effects of Sb Addition on the Wear Resistance of Ductile Cast Iron (구상흑연주철(球狀黑鉛鑄鐵)의 내마모성(耐磨耗性)에 미치는 Sb첨가(添加)의 효과(效果)에 관한 연구(硏究))

  • Lee, B.Y.;Lee, K.W.
    • Journal of Korea Foundry Society
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    • v.6 no.2
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    • pp.93-103
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    • 1986
  • It is very important to obtain wear resistant ductile iron by adding more economical alloying elements. In this study, 10 heat of Mg-treated ductile iron were made according to Sb content (0-0.1% Sb). Each melt was tasted to 30 ${\o}test$ bars in $CO_2$ mold under the same condition and inspected wear characteristics, mechanical properties and microstructures. The results obtained from this study are as follows; 1. It is confirmed that Sb should be a simple and useful additive for improving wear resistance in ductile iron. 2. Hardness of ferrite and pearlite is improved with increasing Sb amount in ductile iron. 3. For ductile iron, the recommended ladle addition of Sb amount is to 0.02-0.03%. 4. Sb has adverse influence on spheroidizing of graphite if the amount is over 0.04%.

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Effects of Undaria pinnatifida on the Physicochemical Properties of Egg (미역첨가 사료가 계란의 이화학적 성질에 미치는 영향)

  • Jo, Kil-Suk
    • Food Science and Preservation
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    • v.12 no.2
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    • pp.117-122
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    • 2005
  • This study was performed to investigate the effects of Undaria pinnatifida on the hysicochemical properties in egg from laying hens fed with $5\%,\;10\%$and $15\%$ supplementation, respectively. The increased amount of Undaria pinnatifida resulted in the decreased weight of egg, expecially in white ones. Darkness, greenness, and blueness of egg yolk and white were increased with the addition of Undanria pinnatifida, and such color changes were predominantly observed in egg york. Among the analyzed minerals, the contents of Ca, Fe and K were increased to $286.6\;mg\%$, $72\;mg\%$ and $430.6\;mg\%$, respectively. But amount of p was reduced to $134.2\;mg\%$. Total cholesterol contents were not significantly changed. Major fatty acids were palmitic, oleic and linoleic acid The contents of omega-3, omega-6 and essential fatty acids were increased to $2.5\%,\;17.6\%$, and $18.4\%$, respectively.

Studies on Constituents of Higher Fungi of Korea(LVI) -General Constituents and lmmunostimulation of Ganoderma lucidum- (한국산(韓國産) 고등(高等) 균류(菌類)의 성분(成分) 연구(硏究)(제(第)56보(報)) -영지(靈芝)의 성분(成分) 및 면역촉진작용(免疫促進作用)-)

  • Lee, Myung-Hee;Kim, Ha-Won;Shim, Mi-Ja;Toh, Sang-Hak;Choi, Eung-Chil;Kim, Byong-Kak
    • The Korean Journal of Mycology
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    • v.14 no.2
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    • pp.149-163
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    • 1986
  • To determine contents of general constituents of Ganoderma lucidum in Korea, the dried carpophores were analyzed. The contents of water, ash, crude lipid, crude protein and crude cellulose were 14.6, 2.0, 3.3, 23.6, and 59.0%, respectively. Among reducing sugars, maltose was the most abundant. Seventeen free amino acids were detected, showing alanine the highest value. The pH of hot water extract was 4.1-4.2. The spores of Ganoderma lucidum was flat and ovoidal long. Their size was $6.3-7.1{\times}3.5-4.3{\times}2.0-2.5\;{\mu}m$ long. To examine effects of life span against sarcoma-180 cells, Fractions A, B and C, were obtained from the extract of Ganoderma lucidum. The survival rates of Fractions A, B and C were 131.7, 162.5, and 141.7 %, respectively. In addition, to examine effects of Fraction B on cell-mediated immunity, delayed type hypersensitivity (=DTH) test was conducted. It restored the suppressed DTH in the sarcoma-180 bearing group up to 66.7%.

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