• Transactions of the Korean Society of Mechanical Engineers
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• v.18 no.4
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• pp.816-825
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• 1994

The purpose of this study is to develop the non-destructive material evaluation method of aluminum alloy base metal matrix composite(MMC) by ultrasonics. Five aluminum base MMC specimens were fabricated in which the fractional ratios of fiber were changed from 0% to 31%. Relations among acoustic properties, microstructural features and elastic constant were compared. The ultrasonic velocity method was useful for nondestructive elastic constant measurement of composite materials, since the method had as same accuracy as conventional strain measurement method. Furthermore, velocity, attenuation and backscattering behaviors for each specimen also related to fractional ratio of fiber and these relations could utilize ultrasonic non-destructive evaluation of fiber structure in MMC.

• Journal of the Korean Ceramic Society
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• v.50 no.6
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• pp.364-371
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• 2013

The sintering behavior of monolithic SiC is examined using the binary sintering additive of $Al_2O_3$-rare earth oxide ($RE_2O_3$, where RE = Sc, Nd, Dy, Ho, or Yb). Through hot pressing at 20 MPa and $1750^{\circ}C$ for 1 h in an Ar atmosphere for 52 nm fine ${\beta}$-SiC powder added with 5 wt% sintering additive, a SiC density of > 97% is achieved, which indicates the effectiveness of $Al_2O_3-RE_2O_3$ system as a sintering of additive for SiC. Based on this result, 7 wt% of $Al_2O_3-Sc_2O_3$ is tested as an additive system for the fabrication of a continuous SiC fiber-reinforced SiC-matrix composite ($SiC_f$/SiC). Electrophoretic deposition combined with the application of ultrasonic pulses is used to efficiently infiltrate the matrix phase into the voids of $Tyranno^{TM}$-SA3 fabric. After hot pressing, a composite density of > 97% is obtained, along with a maximum flexural strength of 443 MPa.

• Membrane Journal
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• v.32 no.2
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• pp.116-125
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• 2022

In this experiment, an α-Al₂O₃ ceramic hollow fiber was used as a support, and a hydrogen membrane plated with Pd and Pd-Ag was manufactured through electroless plating. The Pd-Ag membrane was annealed at 500℃ for 10 h to form an alloy of Pd and Ag. It was confirmed that it became a Pd-Ag alloy through EDS (Energy Dispersive X-ray Spectroscopy) analysis. Also, the thickness of the Pd, Pd-Ag plating layer was measured to be about 8.98 and 9.29 ㎛ through SEM (Scanning Electron Microscope) analysis respectively. Hydrogen permeation experiment was performed using the H₂ gas and mixed gas (H₂ and N₂) in the range of 350~450℃ and 1-4 bar using the prepared hydrogen membrane. Under the H₂ gas condition, the Pd and Pd-Ag membrane has a flux of up to 21.85 and 13.76 mL/cm²·min and also separation factors of 1216 and 361 were obtained in the mixed gas at 450℃ and 4 bar conditions respectively.

• Journal of Powder Materials
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• v.11 no.2
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• pp.118-123
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• 2004

A formation of aluminum hydroxide by hydrolysis reaction in the water has been studied by using nano aluminum powder fabricated by pulsed wire evaporation(PWE) method. The hydroxide type and morphology depending on temperature and pH were examined by structural analysis. The Boehmite($Al_2O_3$.$H_2O$ or AIO(OH)) was predominantly formed in high temperature region over 4$0^{\circ}C$, while the Bayerite($Al_2O_3$.$H_2O$ or $Al(OH)_3$) below $30^{\circ}C$ of hydrolysis temperature. The Boehmite formation was preferred to the Bayerite in acidic solution in the same hydrolysis temperature. The slowly formed Bayerite phase showed facet crystalline structure, while the fast formed Boehmite was fine fiber with a large aspect ratio of several nm in diameter and several hundred nm in length, and with much larger specific surface area(SSA) than that of Bayerite. The highest SSA was about $420m^2$/g.

• Korean Journal of Materials Research
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• v.9 no.3
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• pp.315-321
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• 1999

Metal matrix composites have been extensively studied because of their excellent characteristics for structural application. $Al_2O_3$ and SiC have been used as a common reinforcement owing to their good mechanical properties. However the manufacturing cost of these ceramic reinforcement is expensive, so the use of the composites has been restricted to special purposes. In this study, we tested the application possibility as a reinforcement of $Al_2O_3$-TiC powder synthesized by SHS(Self-propagating High-temperature Synthesis) process to Al alloy matrix composite. Also, $Al_2O_3$ short fibers were added with the synthesized powders in order to apply to the Al matrix hybrid composites. Squeeze infiltration casting process was used to make the composite with 25vol% of reinforcement. Microstructure and crystal structure were examined by SEM, OM and XRD, also the mechanical properties were studied by the compressive test and wear test.

• Journal of Korea Foundry Society
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• v.21 no.3
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• pp.163-178
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• 2001

The squeeze infiltration process is potentially of considerable industrial importance. The performance enhancements resulting from incorporation of short alumina fiber into aluminum are well documented. These are particularly significant for certain automobile components. Aluminum matrix composite automotive parts, such as diesel engine pistons or engine blocks are produced using squeeze casting apparatus or pressure die-casting apparatus. But the solidification process gets complicated with manufacturing parameters and the factors for porosity formation have not fully understood yet. In this study the formation of porosity during squeeze infiltration has been studied experimentally to achieve an improved understanding of the squeeze infiltration process for manufacture of short-fiber-reinforced components, particularly the mechanism of porosity formation. Al-based MMCs produced under a range of conditions were examined metallographically and the porosity characterised;a kind of matrix, an initial temperature of melt, and a volume fraction of reinforcement. The densimetry and the microscopic image analysis were done to measure the amount of porosity. A correlation between manufacturing parameters and defects was investigated through these.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.5 no.2
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• pp.103-107
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• 2004

This paper was studied the properties of materials for treatment of anionic chromate$(CrO4^{-2})$ in industrial wastewater. Ion exchange fiber, poly(acryloamidino diethylene diamine) with ion exchange and adsorption was prepared PAN fiber and diethylenetriamine under $AlC1_3$ catalyst at $120^\circ{C}$ and was analyzed $^{{13}/C-NMR$}$ and FT-IR spectroscopy. The maximum adsorption and the coordination of chromate on chelating fiber were analyzed FT-IR spectra. We proposed the coordination structure with inter/intramolecular bond.

• Proceedings of the Korea Association of Crystal Growth Conference
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• 1999.06a
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• pp.403-418
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• 1999

Fiber growth of Al2O3/R-Al-O(R=Y, Gd, Dy, Ho, Er) eutectic by the micro-pulling down methods is described. The thermal stability and strength at elevated temperature of each material is evaluated in relation to the microstructure. PACS: 81.05 Mh, 81.10 Fq, 81.30-t.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2003.04a
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• pp.46-49
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• 2003

Aluminum based metal matrix composites(MMCs) are well known for their high specific strength, stiffness and hardness. They are gaining further importance because of their high wear resistance. In this study, Al/Saffil-20%, Al/Saffil-5%/Al2O3(particle type)-15% and Al/Saffil-5%/SiC(particle type)-15% hybird MMCs' wear behavior were characterized by the pin-on-disk test under various normal load The superior wear resistance was exhibited at Al/Saffil-5%/SiC(particle type)-15% MMCs. And this MMCs' predominant wear mechanism is subsurface cracking in the low load wear regime. Others(Al/Saffil-20%, Al/Saffil-5%/Al2O3(particle type)-15%) showed the similar wear resistance with each other at the same test condition. In the low load & room temperature condition, the wear resistance was improved due to the high hardness of the ceramic reinforcements. As the test load increased, the wear properties were governed by the wear properties of matrix.

• Composites Research
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• v.22 no.5
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• pp.15-23
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• 2009

The lubricant tribological characteristics of $Al_2O_3$ fiber and SiC particle hybrid metal matrix composites (MMCs) fabricated by squeeze casting method was investigated using a pin-on-disk wear tester. The wear tests of the MMCs were performed according to fiber/particle hybrid ratio in the planar-random (PR) and normal (N) orientations sliding against a counter steel disk at a fixed speed and $25\;kg_f$ loading under different sliding distances and temperatures. The test results showed that the wear behavior of MMCs varied with fiber orientation and hybrid ratio. At room temperature, the lubricant wear behavior of F20P0 unhybrid PR-MMCs was superior to that of N-MMCs while the hybrid composites exhibited the reverse lubricant wear behavior. It was also revealed that the wear resistance of PR-MMCs was superior to that of the N-MMCs due to the joint action of reinforcements and lubricant film between the friction surfaces at an elevated temperature of $100^{\circ}C$ for both fiber only and hybrid cases. In case of $150^{\circ}C$, although the trend of weight loss was similar to that of others, the wear resistance of PR-MMCs was better than that of N-MMCs for hybrid MMCs.