• Proceedings of the Materials Research Society of Korea Conference
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• 한국재료학회 1999년도 춘계학술발표강연 및 눈문개요집
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• pp.121-121
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• 1999

• Korean Journal of Materials Research
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• 제10권9호
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• pp.629-635
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• 2000

The texture evolution during isothermal forging and subsequent heat treatment in Ti-48.5at%Al-0.6at%Mo alloy was investigated. Especially, in the present study, research interest was focused on the interrelation between lamellar volume fraction and textures varied with the change of heat-treated time and temperature. It was found that texture components having ND┴{302) and TD$\perp${100} with minor TD$\perp${111} were developed by isothermal forging. In addition, when the followed heat-treatment time and temperature increased from $1330^{\circ}C$/10h to $1350^{\circ}C$/20h respectively, both the lamellar volume fraction and the intensity of textures mentioned above also gradually increased. However, the tensile elongation at room temperature decreased oppositely, as the lamellar volume fraction increased. These results suggested that tensile properties of $\gamma$-TiAl with the nearly lamellar microstructure at room temperature were affected more strongly by the microstructural features such as lamellar volume fraction rather than by textures.

• Korean Journal of Materials Research
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• 제11권6호
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• pp.502-507
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• 2001

The effect of solidification rate on the microstructure of directionally solidified IN792+ Hf superalloy has been studied. Solidification sequence and precipitation behavior of the alloy have been analysed by microstructural observation. The script carbide transformed to faceted carbide with decreasing solidification rates. The incorporation of ${\gamma}$ phase into the faceted carbide was due to dendritic growth of carbides. Some elongated carbide bars formed along the grain boundaries at a solidification rate of 0.5$\mu\textrm{m}$/s. Two zones, ${\gamma}$' forming elements enriched zone and depleted zone, were found in the residual liquid area. Eutectic ${\gamma}$/${\gamma}$' nucleated in the f forming elements enriched zone. Formation of eutectic ${\gamma}$/${\gamma}$' increased the ratio of (Ti+Hf+Ta+W)/Al and induced η phase precipitation. The ratio of (Ti+Hf+Ta+W)/Al decreased at lower solidification rates due to sufficient back diffusion in the residual liquid area. Hence, the Precipitation of the η Phase efficiently suppressed at the lower solidification rate.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 한국소성가공학회 2001년도 춘계학술대회 논문집
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• pp.172-175
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• 2001

The high temperature deformation behavior of two-phase gamma TiAl alloy has been investigated with the variation of temperature and ${\gamma}/{\alpha}_2$ volume fraction. For this purpose, a series of load relaxation tests and tensile tests have been conducted at temperature ranging from 800 to $1050^{\circ}C$. In the early stage of the deformation as in the load relaxation test experimental flow curves of the fine-grained TiAl alloy are well fitted with the combined curves of two processes (grain matrix deformation and dislocation climb) in the inelastic deformation theory. The evidence of grain boundary sliding has not been observed at this stage. However, when the amount of deformation is large (${\epsilon}{\approx}$ 0.8), flow curves significantly changes its shape indicating that grain boundary sliding also operates at this stage, which has been attributed to the occurrence of dynamic recrystallization during the deformation. With the increase in the volume fraction of ${\alpha}_2$-phase, the flow stress for grain matrix deformation increases since ${\alpha}_2$-Phase is considered as hard phase acting as barrier for dislocation movement. It is considered that cavity initiation is more probable to occur at ${\alpha}_2/{\gamma}$ interface rather than at ${\gamma}/{\gamma}$ interface.

• Journal of Korea Foundry Society
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• 제37권6호
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• pp.199-206
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• 2017

In this study, the variations of microstructures and tensile properties of Ti-(44-54)at.%Al binary alloys were investigated. The heat-treated microstructure depended greatly on their solidification structure and annealing temperature. We measured the variations of volume fractions of primary and secondary lamellar structure as a function of the heat treatment temperature in a Ti-47at.%Al alloy. The variation of ductility as a function of Al content was in good agreement with the change of fracture mode in the tensile fracture surface. It can be inferred that the variations of yield stress and hardness of ${\gamma}$ phase in a single ${\gamma}$-phase field region are enhanced by anti-site defects created by deviations from the stoichiometric composition. In a Ti-47at.%Al alloy within the (${\alpha}_2+{\gamma}$) two-phase field, the yield stress tended to be the maximum at a near equal volume fraction of lamellar and ${\gamma}$ grains. The ductility depended sensitively on the overall grain size and Al content. The calculation of fracture strain using Chan's model indicated that the change of ductility as a function of annealing temperature was primarily determined by the variations in the overall grain size and lamellar volume fraction.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 한국소성가공학회 2006년도 춘계학술대회 논문집
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• pp.429-433
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• 2006

High Temperature deformation behavior of newly developed beta-gamma TiAl alloy was investigated in this study. The optimum processing condition was investigated with the aid of Dynamic Materials Model (DMM). Processing maps representing the efficiency of power dissipation for microstructural evolution and instability were constructed utilizing the results of hot compression test at temperatures ranging from $1000^{\circ}C$ to $1200^{\circ}C$ and strain rate ranging from $10^{-4}/s$ to $10^2/s$. The Artificial Neural Network (ANN) simulation was adopted to consider the deformation heating. With the help of processing map and microstructural analysis, the optimum processing condition was presented and the role of $\beta$ phase was also discussed in this study.

• Journal of Advanced Marine Engineering and Technology
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• 제27권3호
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• pp.453-459
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• 2003

In this study, the effect of heat treatment to the electrochemical polarization resistance for the Ti-6Al-4V alloy was measured. The solution heat treatments were carried out at $1066^{circ}E, 966^{\circ}$E$, followed by aging heat treated $550^{circ}E, 600^{circ}E, and 650^{circ}E$. The electrochemical polarization resistance behavior was measured by potentio-dynamic polarization in the 1N $HNO_3$ + 15ppm HF solution. The obtained results were as follows. 1. As solution heat temperature increased. the corrosion potential was increased, whereas passive current density and critical current density were decreased. 2. As aging heat temperature increased, the corrosion potential was almost constant, but passive current density was decreased 3. The results of composition test measured by EDS at grain boundary and near $\gamma'$ precipitates indicated that S, Cl. and Si which originated from base metal were segregated at the grain boundaries Al and Ti which were the main alloying element in $\gamma'$ were depleted at the $\gamma'$ precipitated. The depletion of Al and Ti in $\gamma'$ was caused to early breakdown of passive film.

• Journal of Powder Materials
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• 제9권6호
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• pp.455-462
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• 2002

The microstructures and properties of TiC dispersed nickel-base alloy were studied in this work. The alloy prepared by powder metallurgical processing was solution treated, 1st-aged at $880^{\circ}C$ for 16 hours, and then 2nd-aged at $760^{\circ}C$ for 4 hours. Microstucture of sintered specimen showed that TiC particles are uniformly dispersed in Ni base alloy. In the specimen aged at $880^{\circ}C$ for 8 hours, the fine $\gammaNi_3$(Al,Ti) precipitates with round shape are observed and the very fine $\gammaNi_3$(Al,Ti) particles with round shape are precipitated in the specimen aged at $760^{\circ}C$ for 4 hours. The presence of ${\gamma}$precipitates in TiC/Ni base alloy increased the hardness and wear resistance of the specimen. The hardness and wear resistance of the Ni-base with TiC are higher than those of conventional Ni-base superalloy X-750 because of dispersion strengthening of TiC particles. The hardness, transverse rupture strength and resistance of the specimen 2nd-aged at $760^{\circ}C$ for 4 hours are higher than those of 1st-aged specimen due to ultrafine $\gammaNi_3$(Al,Ti) precipitates.

• Transactions of Materials Processing
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• 제11권6호
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• pp.529-537
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• 2002

A series of load-relaxation tests and tensile tests were conducted to study the high temperature deformation mechanism of fine duplex gamma TiAl alloy at temperatures ranging from 800 to 105$0^{\circ}C$. Results of load relaxation test showed that deformation behavior at a small imposed strain ($\varepsilon$≒0.05) was dominated by dislocation glide and dislocation climb. To investigate the deformation behavior at a large amount of strain, the processing map was constructed using a dynamic materials model. Two domains were characterized in the processing map obtained at a strain level of 0.6. One domain was found at the region of 98$0^{\circ}C$ and $10^{-3}/sec$ with a peak efficiency of 48%, which was identified as a domain of dynamic recrystallization from the microstructural observation. The order was observed at the region of 125$0^{\circ}C$ and $10^{-4}/sec$ with a peak efficiency of 64%. The strain rate sensitivity measured indicates that the material was deformed by the superplasticity in the region.

• Journal of the Korean Crystal Growth and Crystal Technology
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• 제27권5호
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• pp.229-234
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• 2017

In this study, TiAl alloy was fabricated by a centrifugal casting method for turbo charge of automotive. Optimum conditions for defectless morphology using various ceramic mold were investigated. The crystal structure, microstructure, and chemical composition of the TiAl prepared by centrifugal casting were studied by X-ray diffractometer (XRD), optical microscopy (OM), field emission scanning electron microscopy (FE-SEM) and energy dispersive spectroscopy (EDS), microvickers hardness analyzer (HV). Two kinds of dendrite structures were observed with 4-fold and 6-fold symmetries. The FE-SEM, EDS and HV examinations of the as-cast TiAl showed that the thickness of the oxide layer (${\alpha}$-case) was typically less than $50{\mu}m$.