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http://dx.doi.org/10.7317/pk.2013.37.3.302

Curing Behaviors of Transparent Aliphatic Epoxy Acrylate by Electron Beam Irradiation  

Park, Sang-Yul (Department of Nano Science and Technology, Sejong University)
Son, Hyemi (Department of Nano Science and Technology, Sejong University)
Myung, Dongshin (Department of Chemistry and Nano Science, Ehwa Woman's University)
Kim, Myung-Hwa (Department of Chemistry and Nano Science, Ehwa Woman's University)
Seo, Young-Soo (Department of Nano Science and Technology, Sejong University)
Publication Information
Polymer(Korea) / v.37, no.3, 2013 , pp. 302-307 More about this Journal
Abstract
We synthesized aliphatic epoxy acrylate monomer by the reaction of glycerol diglycidyl ether and acrylic acid. The reaction was monitored by FTIR, Raman spectroscopy and $^1H$ NMR. Electron-beam (E-beam) curing behaviors of the synthesized monomer were studied by spectroscopic analysis, glass transition temperature, and tensile properties. We found that curing reaction was complete in a low dosage of ca. 30 kGy. The viscosity of monomer was a low enough for coating without using diluents and the cured sample was highly transparent, indicating that the monomer can be used for an E-beam curable coating material on transparent optical films.
Keywords
electron beam curing; aliphatic epoxy acrylate; transparent optical films; FTIR; raman spectroscopy;
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