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http://dx.doi.org/10.4150/KPMI.2003.10.6.390

Synthesis of Ultrafine Titanium Carbide Powder by Novel Thermo-Reduction Process  

S.V. Alexandrovskii (Nano P/M Group, Department of Materials Technology, Korea Institute of Machinery and Materials (KIMM))
Publication Information
Journal of Powder Materials / v.10, no.6, 2003 , pp. 390-394 More about this Journal
Abstract
Ultra fine titanium carbide particles were synthesized by novel metallic thermo-reduction process. The vaporized TiC1$_4$+$CCl_4$ gases were reacted with liquid magnesium and the fine titanium carbide particles were then produced by combining the released titanium and carbon atoms. The vacuum treatment was followed to remove the residual phases of MgC1$_2$ and excess Mg. The stoichiometry, microstructure, fixed and carbon contents and lattice parameter were investigated in titanium carbide powders produced in various reaction parameters.
Keywords
Carbides; Nanocrystalline materials; Metal-Thermal reduction;
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