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Analysis of derivatized MX by Gas Chromatography/Mass Spectrometry  

Yoo, Eun-Ah (Department of Chemistry, Sungshin Women's University)
Park, Do-Yeon (Department of Chemistry, Sungshin Women's University)
Lee, Hyang-Ki (Department of Chemistry, Sungshin Women's University)
Myung, Seung-Woon (Doping Control Center, Korea Institute of Science and Technology)
Publication Information
Analytical Science and Technology / v.15, no.3, 2002 , pp. 221-228 More about this Journal
Abstract
AMX is one of extremely high mutagenic compound produced from the reaction of the chlorine and the organic compound during the disinfection of tap water. In this paper, the chemical derivatization of MX with 2% sulfuric acid-methanol, iso-propanol, sec-butanol and n-butanol derivatives for the GC/MS analysis were tested or compared. Limit of detection for the EI and NCI mode were 25 pg and 1.25 pg, respectively. The good linear calibration curve was obtained the range of 25~2500 pg by EI and NCI
Keywords
MX; mutagenicity; GC/MS;
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