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Effects of special heat treatment on changes in the hardness of a metal-ceramic alloy during the firing process

금속-도재 보철용 합금의 열처리가 소성과정 중 경도 변화에 미치는 영향

  • Sung-Min Kim (Department of Dental Laboratory Technology, Jinju Health College)
  • Received : 2023.08.07
  • Accepted : 2023.09.13
  • Published : 2023.09.30

Abstract

Purpose: This study aimed to evaluate the effects of a special heat treatment on Pd-Au-Ag metal-ceramic alloy after degassing treatment and on changes in the hardness of the alloy during the firing process. Methods: Specimen alloys were cast and subjected to degassing at 900℃ for 10 minutes. These specimens were then subjected to a special heat treatment at 600℃ for 15 minutes in a dental porcelain furnace. Further, the specimens were subjected to simulated firing in the porcelain furnace. The resulting specimens were then tested for hardness, and changes in the microstructure were observed. Results: There was a decrease in the hardness of the alloy during the simulated firing of the cast alloy due to the coarsening of the particles. Meanwhile, additional heat treatment after degassing was found to play a crucial role in preventing a decrease in hardness. This treatment effectively suppressed the coarsening of the precipitates during repeated firing at high temperatures. Conclusion: Specific heat treatment of the Pd-Au-Ag metal-ceramic alloy prevented a decrease in its hardness and extended the lifespan of the metal-ceramic prosthesis.

Keywords

References

  1. Anusavice KJ, Shen C, Rawls HR. Phillips' science of dental materials. 12th ed. Elsevier, 2013. 
  2. Park WJ, Cho IH. Fatigue fracture of different dental implant system under cyclic loading. J Korean Acad Prosthodont. 2009;47:424-434.  https://doi.org/10.4047/jkap.2009.47.4.424
  3. Skalak R. Biomechanical considerations in osseointegrated prostheses. J Prosthet Dent. 1983;49:843-848.  https://doi.org/10.1016/0022-3913(83)90361-X
  4. Yasuda K, Udoh K, Hisatsune K, Ohta M. Structural changes induced by ageing in commercial dental gold alloys containing palladium. Dent Mater J. 1983;2:48-58.  https://doi.org/10.4012/dmj.2.48
  5. Hisatsune K, Hasaka M, Sosrosoedirdjo BI, Udoh K. Age-hardening behavior in a palladium-base dental porcelain-fused alloy. Mater Charact. 1990;25:177-184.  https://doi.org/10.1016/1044-5803(90)90008-8
  6. Bertolotti RL, Moffa JP. Creep rate of porcelain-bonding alloys as a function of temperature. J Dent Res. 1980;59:2062-2065.  https://doi.org/10.1177/00220345800590120601
  7. Kim SM, Yu YJ, Cho MH, Kwon YH, Seol HJ, Kim HI. Hardening mechanism associated with additional heat treatment after degassing treatment by various cooling rates in a metal-ceramic alloy of Pd-Au-Ag system. Korean J Dent Mater. 2015;42:271-278.  https://doi.org/10.14815/kjdm.2015.42.4.271
  8. Tuccillo JJ, Nielsen JP. Creep and sag properties of a porcelain-gold alloy. J Dent Res. 1967;46:579-583.  https://doi.org/10.1177/00220345670460032101
  9. Fischer J, Fleetwood PW. Improving the processing of high-gold metal-ceramic frameworks by a pre-firing heat treatment. Dent Mater. 2000;16:109-113.  https://doi.org/10.1016/S0109-5641(99)00086-X
  10. Dental Implant Industry-University Research Association. Dental implant laboratory sciences. 3rd ed. Jiseong Book Publishing, 2010. 
  11. Jeon BW, Lee GY, Kwon YH, Kim HI, Seol HJ. Hardness change by simulated firing condition in an AgPd-In metal-ceramic alloy. Korean J Dent Mater. 2013;40:185-194. 
  12. Cho SY, Lee GY, Jeong JI, Kwon YH, Kim HI, Seol HJ. Microstructural changes in grain interior and grain boundary by formation of metastable and stable phases related to age-hardening in an Au-Cu-Ag-Pd alloy. J Mater Res. 2013;28:1211-1217. https://doi.org/10.1557/jmr.2013.77