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Degree of Conversion and Polymerization Shrinkage of Low and High Viscosity Bulk-Fill Giomer-based and Resin-based composites

저점도 및 고점도 Bulk-fill Giomer 복합레진과 Bulk-fill 복합레진의 전환율과 중합수축

  • Kim, Heera (Department of Pediatric Dentistry, School of Dentistry, Kyungpook National University) ;
  • Lee, Jaesik (Department of Pediatric Dentistry, School of Dentistry, Kyungpook National University) ;
  • Kim, Hyunjung (Department of Pediatric Dentistry, School of Dentistry, Kyungpook National University) ;
  • Kwon, Taeyub (Department of Dental Biomaterials, School of Dentistry, Kyungpook National University) ;
  • Nam, Soonhyeun (Department of Pediatric Dentistry, School of Dentistry, Kyungpook National University)
  • 김희라 (경북대학교 치과대학 소아치과학교실) ;
  • 이제식 (경북대학교 치과대학 소아치과학교실) ;
  • 김현정 (경북대학교 치과대학 소아치과학교실) ;
  • 권태엽 (경북대학교 치과대학 치과생체재료학교실) ;
  • 남순현 (경북대학교 치과대학 소아치과학교실)
  • Received : 2018.10.01
  • Accepted : 2018.10.23
  • Published : 2019.02.28

Abstract

The aim of this study was to compare the degree of conversion and polymerization shrinkage of low and high viscosity bulk-fill giomer-based and resin-based composites. Two bulk-fill giomer (Beautifil Bulk Restorative (BBR), Beautifil Bulk Flowable (BBF)), two bulk-fill (Tetric N-Ceram Bulk-fill (TBF), SureFil SDR flow (SDR)) and two conventional resin composites (Tetric N-Ceram (TN), Tetric N-flow (TF)) were selected for this study. The degree of conversion was measured by using Fourier transform infrared spectroscopy. Polymerization shrinkage was measured with the linometer. For all depth, BBR had the lowest degree of conversion and SDR had the highest. At 4 mm, the degree of conversion of low and high viscosity bulk-fill giomer resin composites was lower than that of bulk-fill resin composites (p < 0.05). At the depth between 2 mm and 4 mm, there were significant difference with TBF, TN and TF (p < 0.05), while no significant difference in the degree of conversion was measured for BBR, BBF and SDR. Polymerization shrinkage of six resin composites decreased in the following order: TF > SDR > BBF > TBF > TN and BBR (p < 0.05). Polymerization shrinkage of bulk-fill giomer resin composites was lower than that of bulk-fill resin composites (p < 0.05). From this study, it is found that the bulk-fill giomer resin composites and TBF were not sufficiently cured in 4 mm depth. The degree of conversion of low and high viscosity bulk-fill giomer resin composites was significantly lower than bulk-fill resin composites in both 2 mm and 4 mm depths. Therefore, such features of bulk-fill giomer resin composites should be carefully considered in clinical application.

이번 연구에서는 저점도 및 고점도 bulk-fill giomer 복합레진의 전환율과 중합수축을 기존 bulk-fill 복합레진 및 전통적 복합레진과 비교 평가해보고자 하였다. Bulk-fill giomer 복합레진 2종류(Beautifil Bulk Restorative(BBR), Beautifil Bulk Flowable(BBF)), bulk-fill 복합레진 2종류(Tetric N-Ceram Bulk-fill(TBF), SureFil SDR flow(SDR)), 전통적 복합레진 2종류(Tetric N-Ceram(TN), Tetric N-flow(TF))를 사용하였다. 중합도 측정은 Fourier transform infrared spectroscopy을 사용하였으며, 중합수축은 linometer을 이용하여 측정하였다. 복합레진 하면의 전환율 측정 결과 2 mm와 4 mm 깊이 모두 BBR에서 가장 낮게 나왔으며, SDR에서 가장 높게 나왔다. 4 mm 깊이에서 고점도 및 저점도 bulk-fill giomer 복합레진의 전환율은 bulk-fill 복합레진에 비해 유의하게 낮은 값을 보였다(p < 0.05). 깊이에 따른 전환율 비교 시 TBF, TN, TF는 유의차를 보였으며(p < 0.05), BBR, BBF, SDR는 유의차를 보이지 않았다. 중합수축은 TF > SDR > BBF > TBF > TN, BBR 순서로 감소 했으며(p < 0.05), bulk-fill giomer 복합레진은 bulk-fill 복합레진보다 낮은 중합수축량을 보였다(p < 0.05). 이번 연구 결과 4 mm 깊이에서 bulk-fill giomer 복합레진 및 TBF는 불충분한 중합을 나타냈으며, 2 mm와 4 mm 모두에서 고점도 및 저점도 bulk-fill giomer 복합레진은 bulk-fill 복합레진에 비해 낮은 전환율을 보였다. 그러므로 bulk-fill giomer 복합레진의 임상적인 적용을 위해서는 이에 대한 충분한 고찰 및 주의가 필요할 것으로 생각된다.

Keywords

References

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