Journal of Industrial and Engineering Chemistry

  • Volume 68
  • /
  • Pages.87-98
  • /
  • 2018
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  • 1226-086X(pISSN)
  • /
  • 1876-794X(eISSN)
The Korean Society of Industrial and Engineering Chemistry (한국공업화학회)
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Effect of activated carbon modified with oxalic acid on the production of IPA from MX catalyzed by H3PW12O40@carbon and cobalt

  • Fang, Zhou-wen (State Key Laboratory of Chemical Engineering, East China University of Science and Technology) ;
  • Liu, Hua-jie (State Key Laboratory of Chemical Engineering, East China University of Science and Technology) ;
  • Wang, Zhi-hao (State Key Laboratory of Chemical Engineering, East China University of Science and Technology) ;
  • Wen, Di (State Key Laboratory of Chemical Engineering, East China University of Science and Technology) ;
  • Long, Xiang-li (State Key Laboratory of Chemical Engineering, East China University of Science and Technology)
  • Received : 2018.02.20
  • Accepted : 2018.07.24
  • Published : 2018.12.25
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Abstract

The production of IPA from the oxidation of MX is completed under the catalysis of $H_3PW_{12}O_{40}$ (HPW) loaded on carbon and cobalt. Oxalic acid is tried to modify the carbon to upgrade the catalytic activity of HPW@C catalyst. The experiments show that the best carbon is acquired by carbonizing the carbon at $450^{\circ}C$ for 2 h in $N_2$ after being soaked in a $0.20mol\;l^{-1}$ oxalic acid solution for 16 h. The IPA produced by the HPW@C catalysts prepared with the carbon modified is 58.9% over that obtained by the catalysts prepared with the original carbon.

Keywords

Acknowledgement

Supported by : NSFC

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