DOI QR코드

DOI QR Code

Synthesis of TiCx Powder via the Underwater Explosion of an Explosive

  • Tanaka, Shigeru (Institute of Pulsed Power Science (IPPS), Kumamoto University) ;
  • Bataev, Ivan (Material Science, Novosibirsk State Technical University) ;
  • Hamashima, Hideki (Manufacturing Division, Kumamoto Industrial Research Institute) ;
  • Tsurui, Akihiko (Graduate School of Science and Technology, Kumamoto University) ;
  • Hokamoto, Kazuyuki (Institute of Pulsed Power Science (IPPS), Kumamoto University)
  • 투고 : 2018.01.24
  • 심사 : 2018.04.23
  • 발행 : 2018.11.20

초록

In this study, a novel approach to the explosive synthesis of titanium carbide (TiC) is discussed. Nonstoichiometric $TiC_x$ powder was produced via the underwater explosion of a Ti powder encapsulated within a spherical explosive charge. The explosion process, bubble formation, and synthesis process were visualized using high-speed camera imaging. It was concluded that synthesis occurred within the detonation gas during the first expansion/contraction cycle of the bubble, which was accompanied by a strong emission of light. The recovered powders were studied using scanning electron microscopy and X-ray diffraction. Submicron particles were generated during the explosion. An increase in the carbon content of the starting powder resulted in an increase in the carbon content of the final product. No oxide byproducts were observed within the recovered powders.

키워드

참고문헌

  1. H. Ding, X. Fan, K. Chu, B. Du, J. Wang, Int. J. Hydrog. Energy 39, 9363 (2014)
  2. H. Ding, X. Fan, C. Li, X. Liu, D. Jiang, C. Wang, J. Alloys Compd. 551, 67 (2013) https://doi.org/10.1016/j.jallcom.2012.10.067
  3. Y.C. Woo, H.J. Kang, D.J. Kim, J. Eur. Ceram. Soc. 27, 719 (2007) https://doi.org/10.1016/j.jeurceramsoc.2006.04.090
  4. S. Mohapatra, D.K. Mishra, S.K. Singh, Powder Technol. 237, 41 (2013) https://doi.org/10.1016/j.powtec.2013.01.018
  5. J.H. Lee, N.N. Thadhani, Scr. Mater. 37, 1979 (1997) https://doi.org/10.1016/S1359-6462(97)00393-X
  6. J.H. Lee, N.N. Thadhani, J. Mater. Process. Technol. 85, 79 (1999) https://doi.org/10.1016/S0924-0136(98)00265-9
  7. J.H. Lee, N.N. Thadhani, J. Mater. Process. Technol. 85, 83 (1999) https://doi.org/10.1016/S0924-0136(98)00266-0
  8. M.B. Rahaei, R. Yazdani rad, A. Kazemzadeh, T. Ebadzadeh, Powder Technol. 217, 369 (2012) https://doi.org/10.1016/j.powtec.2011.10.050
  9. J. Rohrer, P. Hyldgaard, Phys. Rev. B 82, 045415 (2010) https://doi.org/10.1103/PhysRevB.82.045415
  10. Y.G. Jung, S.W. Park, S.C. Choi, Mater. Lett. 30, 5 (1997)
  11. C.J. Kang, D.W. Kim, C.O. Park, J.S. Chun, Mater. Manuf. Process. 5, 1 (1990) https://doi.org/10.1080/10426919008953225
  12. K. Wang, Q. Guo, G. Zhang, J. Shi, L. Liu, Surf. Coat. Technol. 201, 16 (2007)
  13. B. Debalina, M. Kamaraj, B.S. Murthy, S.R. Chakravarthi, R. Sarathi, J. Alloys Compd. 496, 122 (2010) https://doi.org/10.1016/j.jallcom.2010.01.140
  14. S. Tanaka, N. Kawaji, N. Wada, K. Hokamoto, Sci. Technol. Energ. Ma. 75, 106 (2014)
  15. A.P. Ilyin, O.B. Nazarenko, J. Optoelectron. Adv. Mater. 9, 1521 (2007)
  16. E.M. Abdelkader, P.A. Jellaiss, S.W. Buckner, Inorg. Chem. 54, 5897 (2015) https://doi.org/10.1021/acs.inorgchem.5b00697
  17. Y.L. Zhu, T.C. Li, J.T. Liu, X.D. Han, D.Z. Yang, Scr. Metall. Mater. 30, 775 (1994) https://doi.org/10.1016/0956-716X(94)90198-8
  18. K. Yamada, J. Am. Ceram. Soc. 81, 1941 (1998)
  19. T. Sekine, J. Am. Ceram. Soc. 85, 113 (2002)
  20. Z. Martins, M.C. Price, N. Goldman, M.A. Sephton, M.J. Burchell, Nat. Geosci. 6, 1045 (2013) https://doi.org/10.1038/ngeo1930
  21. Y. Nakayama, S. Oinuma, K. Tanaka, Sci. Tech. Energ. Mater. 50, 179 (1989)
  22. K. Tanaka, S. Oinuma, Sci. Technol. Energ. Mater. 47, 196 (1986)
  23. K. Tanaka, Sci. Technol. Energ. Mater. 36, 11 (1975)
  24. R. Rajendran, K. Narasimhan, J. Strain Anal. Eng. 41, 417 (2006) https://doi.org/10.1243/03093247JSA120
  25. G. Barras, M. Souli, N. Aquelet, N. Couty, Ocean Eng. 41, 53 (2012) https://doi.org/10.1016/j.oceaneng.2011.12.015
  26. C.Y. Hsu, C.C. Liang, A.T. Nguyen, T.L. Teng, Ocean Eng. 81, 29 (2014) https://doi.org/10.1016/j.oceaneng.2014.02.018
  27. J.C. Fernandes, C. Anjinho, P.M. Amaral, L.G. Rosa, J. Rodriguez, D. Martinez, F.A.C. Oliveira, N. Shohoji, Mater. Chem. Phys. 77, 711 (2002)
  28. J.C. Fernandes, P.M. Amaral, L.G. Rosa, D. Martinez, J. Rodriguez, N. Shohoji, Int. J. Refract. Met. Hard Mater. 17, 437 (1999) https://doi.org/10.1016/S0263-4368(99)00036-0