Korean Journal of Dental Materials (대한치과재료학회지)

Korean Society For Dental Materials (대한치과재료학회)
권호 표지
DOI QR코드

DOI QR Code

Shear bond strength between universal adhesives with various pH and dual-cured resin cements

다양한 pH를 가지는 Universal adhesives와 이원 중합 레진 세멘트 간의 전단결합강도

  • Kwon, Sung-Joo (Department of conservative dentistry, School of Dentistry, Pusan National University) ;
  • Park, Jeong-Kil (Department of conservative dentistry, School of Dentistry, Pusan National University) ;
  • Son, Sung-Ae (Department of conservative dentistry, School of Dentistry, Pusan National University)
  • 권성주 (부산대학교 치의학전문대학원 치과보존학교실) ;
  • 박정길 (부산대학교 치의학전문대학원 치과보존학교실) ;
  • 손성애 (부산대학교 치의학전문대학원 치과보존학교실)
  • Received : 2018.11.08
  • Accepted : 2018.12.04
  • Published : 2018.12.30
⟨ Previous Next ⟩

Abstract

The purpose of this study is to evaluate the compatibility of universal adhesives with two dual-cured resin cements. Eighty human molars were divided into eight groups. Tooth was embedded in self-curing acrylic resin and sectioned horizontally to exposure dentine surface. After polishing with 600-grit SiC paper, adhesives were applied. All-Bond Universal (Bisco), G-premio bond (GC), Scotch-bond universal (3M ESPE), Scotch-bond Multipurpose (3M ESPE) were used in this study. Calibra (Dentsply) as a conventional dual-curing resin cement and RelyX Ultimate (3M ESPE) as an amine free resin cement were used. The adhesives and the cements were applied according to the manufacturer's instructions. Final specimens were cylinder (diameter 2mm, height 3mm) shape. After storing in distilled water at $37^{\circ}C$ for 7 days the shear bond strength (SBS) test was performed. There was no significant difference in shear bond strength between the adhesives when RelyX Ultimate was used (p>0.05). However, when Calibra used with Scotch-bond Multipurpose and All-Bond Universal were used, statistically higher SBS was observed, as compared to the groups which Calibra cements with G-premio bond and Scotch-bond universal adhesive (p<0.05) were used. Within the limitations of this study, RelyX Ultimate resin cement was compatible with universal adhesives of various pH. All-Bond Universal adhesive was compatible with a resin cement containing the tertiary amine.

이 연구의 목적은 현재 쓰임이 증가하고 있는 여러 종류의 범용 상아질 접착제와 삼차 아민을 포함 혹은 포함하지 않는 레진시멘트 간의 호환성을 평가하기 위함이다. 총 80개의 사람 대구치를 선정해 레진 블럭에 매몰하여 상아질을 노출시키고 600-grit SiC paper로 연마한 후 3종류의 범용 상아질 접착제 Scotchbond universal (3M ESPE, pH 2.6), G-premio bond (GC, pH 1.5), All bond universal (Bisco, pH 3.2) 및 대조군으로 3-step etch and rinse system인 Scotchbond multipurpose (3M ESPE)를 제조사의 지시대로 적용한 후 광중합 시행하였다. 그 위에 직경 2 mm, 높이 3 mm의 몰드를 이용해 삼차아민을 포함한 레진 시멘트인 Calibra(Dentsply) 혹은 삼차 아민을 포함하지 않는 레진시멘트인 RelyX Ultimate (3M ESPE)를 적용하고 20초간 광중합하였다. 그 후 $37^{\circ}C$ 증류수에 7일간 보관 후 미세전단강도를 측정하였다. 각 결과값을 ANOVA와 Tukey test로 분석하였다. 실험 결과 Calibra를 사용한 경우 Scotchbond Multipurpose와 All bond Universal adhesive 적용시 G-premio bond 및 Scotchbond universal adhesive를 적용했을 때에 비해 유의하게 높은 미세전단강도를 나타냈다(p<0.05) RelyX Ultimate를 사용한 경우 adhesive간의 유의한 차이가 관찰되지 않았다(p>0.05).

Keywords

Acknowledgement

Supported by : Pusan National University Dental Hospital

References

  1. El Mowafi OM, Fenton AH, Forrester N, Milenkovic M. Retention of metal ceramic crowns cemented with resin cements: effects of preparation taper and height. J Prosthet Dent. 1996;76:524-29. https://doi.org/10.1016/S0022-3913(96)90012-8
  2. Schittly E, Bouter D, Le Goff S, Degrange M, Attal JP. Compatibility of five self-etching adhesive systems with two resin luting cements. J Adhes Dent. 2010;12:137-42.
  3. Van Meerbeek B, De Munck J, Yoshida Y, Inoue S, Vargas M, Vijay P Van Landuyt K, Lambrechts P, Vanherle G. Buonocore memorial lecture. Adhesion to enamel and dentin: Current status and future challenges. Oper Dent. 2003;28:215-35.
  4. Luhrs AK, Guhr S, Schilke R, Borchers L, Geurtsen W, Gunay H. Shear bond strength of self-etch adhesives to enamel with additional phosphoric acid etching. Oper Dent. 2008;33:155-62. https://doi.org/10.2341/07-63
  5. De Goes M.F., Shinohara M.S., Freitas, M.S. Performance of a new one-step multi-mode adhesive on etched vs non-etched enamel on bond strength and interfacial morphology. J Adhes Dent. 2014;16:243-50.
  6. El Bradawy WA, El Mowafi OM. Chemical versus dual curing of resin inlay cements. J Prosthet Dent. 1995;73:515-24. https://doi.org/10.1016/S0022-3913(05)80109-X
  7. Franco EB, Lopes LG, Dalpino PH, Pereira JC, Mondelli RF, Navarro MF. Evaluation of compatibility between different types of adhesives and dual-cured resin cement. J Adhes Dent. 2002;4:271-5.
  8. Sanares AM, Itthagarun A, King NM, Tay FR, Pashley DH. Adverse surface interactions between one-bottle light-cured adhesives and chemical-cured composites. Dent Mater. 2001;17:542-46. https://doi.org/10.1016/S0109-5641(01)00016-1
  9. Schittly E, Bouter D, Le Goff S, Degrange M, Attal JP. Compatibility of five self-etching adhesive systems with two resin luting cements. J Adhes Dent. 2010;12:137-42.
  10. Suh BI, Feng L, Pashley DH, Tay FR. Factors contributing to the incompatibility between simplifiedstep adhesives and chemically-cured or dual-cured composites. Part III. Effect of acidic resin monomers. J Adhes Dent. 2003;5:267-82.
  11. Tay FR, King NM, Suh BI, Pashley DH. Effect of delayed activation of light-cured resin composites on bonding of all-in-one adhesives. J Adhes Dent. 2001;3:207-25.
  12. King NM, Tay FR, Suh BI, Pashley DH. Compromised bonding of all-in-one adhesives upon delayed activation of light-cured composites. J Dent Res. 2001;80:639.
  13. Chen L, Suh BI. Effect of hydrophilicity on the compatibility between a dual-curing resin cement and one-bottle simplified adhesives. J Adhes Dent. 2013;15:325-31.
  14. Yamauchi J. Study of dental adhesive containing phosphoric acid methacrylate monomer. Jap J Dent Mater. 1986;5:144-54.
  15. Ikemura K, Endo T. Effect of adhesion of new polymerization initiator systems comprising 5- monosubstituted barbituric acids, sulfinate amides, and terbutyl peroxymaleic acid in dental adhesive resin. J Appl Polym Sci. 1999;72:1655-68. https://doi.org/10.1002/(SICI)1097-4628(19990624)72:13<1655::AID-APP2>3.0.CO;2-0

Cited by

  1. Adhesion strategy and curing mode of a universal adhesive influence the bonding of dual-cured core build-up resin composite to dentin vol.35, pp.1, 2021, https://doi.org/10.1080/01694243.2020.1786907