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Synthesis of DyF3 paste and Magnetic Properties of GBDPed Nd-Fe-B Magnets

DyF3 paste 제조 및 이를 이용한 Nd-Fe-B 입계확산 자석의 특성 연구

  • Jeon, Kwang-Won (Powder&Ceramics Division, Korea Institute of Materials Science) ;
  • Cha, Hee-Ryoung (Powder&Ceramics Division, Korea Institute of Materials Science) ;
  • Lee, Jung-Goo (Powder&Ceramics Division, Korea Institute of Materials Science)
  • 전광원 (한국기계연구원 부설 재료연구소 분말/세라믹 연구본부) ;
  • 차희령 (한국기계연구원 부설 재료연구소 분말/세라믹 연구본부) ;
  • 이정구 (한국기계연구원 부설 재료연구소 분말/세라믹 연구본부)
  • Received : 2016.10.18
  • Accepted : 2016.12.17
  • Published : 2016.12.28

Abstract

Recently, the grain boundary diffusion process (GBDP), involving heavy rare-earth elements such as Dy and Tb, has been widely used to enhance the coercivity of Nd-Fe-B permanent magnets. For example, a Dy compound is coated onto the surface of Nd-Fe-B sintered magnets, and then the magnets are heat treated. Subsequently, Dy diffuses into the grain boundaries of Nd-Fe-B magnets, forming Dy-Fe-B or Nd-Dy-Fe-B. The dip-coating process is also used widely instead of the GBDP. However, it is quite hard to control the thickness uniformity using dip coating. In this study, first, a $DyF_3$ paste is fabricated using $DyF_3$ powder. Subsequently, the fabricated $DyF_3$ paste is homogeneously coated onto the surface of a Nd-Fe-B sintered magnet. The magnet is then subjected to GBDP to enhance its coercivity. The weight ratio of binder and $DyF_3$ powder is controlled, and we find that the coercivity enhances with decreasing binder content. In addition, the maximum coercivity is obtained with the paste containing 70 wt% of $DyF_3$ powder.

Keywords

References

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