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Heat Treatment Effect on Super Duplex Stainless Steel UNS S32750 FCA Multipass Welds

슈퍼 듀플렉스 스테인리스강 UNS S32750의 FCA 다층 용접부의 용접 후 열처리 영향

  • Jang, Bok-Su (School of Energy.Materials.Chemical, Korea University of Technology and Education) ;
  • Moon, In-June (School of Energy.Materials.Chemical, Korea University of Technology and Education) ;
  • Lim, Myung-Jin (School of Energy.Materials.Chemical, Korea University of Technology and Education) ;
  • Kim, Se-Cheol (School of Energy.Materials.Chemical, Korea University of Technology and Education) ;
  • Kim, Soo-Sung (Research Reactor Development Division, Korea Atomic Energy Research Institute) ;
  • Lee, Jung-Won (Research Reactor Development Division, Korea Atomic Energy Research Institute) ;
  • Park, Hai-Woong (School of Energy.Materials.Chemical, Korea University of Technology and Education) ;
  • Koh, Jin-Hyun (School of Energy.Materials.Chemical, Korea University of Technology and Education)
  • 장복수 (한국기술교육대학교 에너지.신소재.화학공학부) ;
  • 문인준 (한국기술교육대학교 에너지.신소재.화학공학부) ;
  • 임명진 (한국기술교육대학교 에너지.신소재.화학공학부) ;
  • 김세철 (한국기술교육대학교 에너지.신소재.화학공학부) ;
  • 김수성 (한국원자력원구원 연구로개발부) ;
  • 이정원 (한국원자력원구원 연구로개발부) ;
  • 박해웅 (한국기술교육대학교 에너지.신소재.화학공학부) ;
  • 고진현 (한국기술교육대학교 에너지.신소재.화학공학부)
  • Received : 2014.01.28
  • Accepted : 2014.02.25
  • Published : 2014.04.30

Abstract

This study was carried out to investigate the effect of postweld heat treatment(PWHT, 930, 1080, $1230^{\circ}C$) on the microstructure, phase formation, pitting corrosion and mechanical properties such as hardness, tensile strength and impact values of super duplex stainless steel(UNS S32750) multipass welds. Based on the microstructural examination and X-ray diffraction analysis, it was found that the ${\sigma}$ phase was formed in the welds heat treated at $930^{\circ}C$ in which the ferrite content greatly decreased into 5~10% in the welds. The secondary austenite was formed in the reheated zone of welds and redissolved into ferrite with increasing heat treatment temperatures. The tensile strength and impact values of welds heat treated at $930^{\circ}C$ were the lowest and revealed the brittle fracture surface. The weight loss by pitting corrosion increased with test temperatures. It was confirmed that pitting corrosion occurred mainly in secondary austenite of reheated zones. The postweld heat treatment temperature is recommended to be in the range of $1050{\sim}1150^{\circ}C$.

Keywords

References

  1. Jong-Sub Lee and Sook Hwan Kim, A Study of Weld Fusion Zone Phenomena in Austenitic Stainless Steels(2)-Effect of Nitrogen on Microstructural Evolution and Hot Cracking Susceptibility of GTA Welds in STS 304-, Journal of KWJS, 18-1(2000), 59-69 (in Korean)
  2. Kotecki, D.J., 1997. Ferrite Determination in Stainless Steel Welds Advances since 1974, Welding Journal, 76, 24s-37s
  3. Gooch, T.G., 1983. Weldability of Duplex Ferritic-Austenitic Stainless Steels, Proc. Duplex Stainless Steels, 573-602
  4. J. M. Cabrera, A. Mateo, L. Llanes, J. M. Prado, and M. Anglada, Journal of materials processing technology 321-325 (2003)
  5. Seong-Kil Nam, Se-Jin Park, Hye-Sung Na and Chung-Yun Kang, Effect of Thermal Cycle on Microstructure and Pitting Corrosion Property of Multi-pass Weldment of Super-duplex Stainless Steel, Journal of KWJS, 28-4(2010), 18-25 (in Korean) https://doi.org/10.5781/KWJS.2010.28.4.018
  6. Calliari, I., Zanesco, M., Ramous, E., 2006. Influence of Isot hermal Aging on Secondary Phases Precipitation and Toughness of a Duplex Stainless Steel SAF 2205, Journal of Materials Science, 41, 7643-7649 https://doi.org/10.1007/s10853-006-0857-2
  7. Gunn, R.N., 1997b. Duplex Stainless Steels, Abington publishing, Cambridge, 135
  8. Gooch, T.G., 1991. Corrosion Resistance of Welds in Duplex Stainless Steels, Proc. Duplex Stainless Steels 91, 1, 325-335
  9. Bonnefois, B., Charles, J., Dupoiron, F., Soulignac, P., 1991. How to Predict Welding Properties of Duplex Stainless Steels?, Proc. Duplex Stainless Steels 91, 1, 347-361
  10. Atamert, S., King, J.E., Reed, R.C., 1992. Reheated Regions in Duplex Stainless Weldments, Proc. International Trends in Welding Science and Technology, 241-245
  11. Stekly, J.J.K., Scandella, J.-L., Salmon, K.A., 1991. Effects of Welding Techniques on the Properties of Super Duplex Stainless Steels, Proc. Duplex Stainless Steels 91, 1, 431-439
  12. ASTM G48-03, "Standard Test Methods for Pitting and Crevice Corrosion Resistance of Stainless Steels and Related Alloys by Use of Ferric Chloride Solution", West Conshohocken, PA: ASTM, 2007
  13. J. O. Nilsson, Mater. Sci. Technol. 8, 685 (1992) https://doi.org/10.1179/mst.1992.8.8.685
  14. G. H. Kwon, Y. S. Na, W. D. Yoo, J. H. LEE, and Y. H. Park, Korean J. Met. Mater, 50, 7 (2012)
  15. T. H. Chen, K. L. Weng, and J. R. Yang, Materials Science and Engineering, 259-270 (2002)
  16. Sieurin Henrik, Sandstrom Rolf. Sigma phase precipitation in duplex stainless steel 2205. Mater Sci Eng A 2007;444:271-6 https://doi.org/10.1016/j.msea.2006.08.107
  17. Yong-Soo Park, Soon-Tae Kim, In-Sung Lee and Chi-bok Shong: "Effects of Rare Earth Metals Addition and aging Treatment on the Corrosion Resistance and Mechanical Properties of Super Duplex Stainless Steels", METALS AND METERIALS International, 8-3(2002), 309-318 https://doi.org/10.1007/BF03186101
  18. Gi-Hyoun Kwon, Young-Sang Na, Wee-Do Yoo, Jong-Hoon Lee and Yong-Ho Park, Effects of the Cooling Rate after Annealing Treatment on the Microstructure and the Mechanical properties of Super-Duplex Stainless Steel, Korean J. Met. Mater. 50-10, 735-743 (in Korean)
  19. Nilsson, J.-O., Jonsson, P., and Wilson, A. 1994. Formation of secondary austenite in super duplex stainless steel weld metal and its dependence on chemical compostion, Paper 39 in Duplex Stainless Steels '94, 1, Abington Publishing, cambridge