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Preparation and Characterization of a Layered Organic-inorganic Composite by the Electrophoretic Deposition of Plate-shaped Al2O3 Particles and Electrophoretic Resin

전기영동적층법을 통한 판상 알루미나 입자와 전기영동 수지의 배향 유무기 복합체 제조 및 물성평가

  • Park, Hee Jeong (Energy & Environmental Division, Korea Institute of Ceramic Engineering and Technology) ;
  • Lim, Hyung Mi (Energy & Environmental Division, Korea Institute of Ceramic Engineering and Technology) ;
  • Choi, Sung-Churl (Department of Materials Science & Engineering, Hanyang University) ;
  • Kim, Younghee (Energy & Environmental Division, Korea Institute of Ceramic Engineering and Technology)
  • 박희정 (한국세라믹기술원 에너지환경소재본부) ;
  • 임형미 (한국세라믹기술원 에너지환경소재본부) ;
  • 최성철 (한양대학교 신소재공학과) ;
  • 김영희 (한국세라믹기술원 에너지환경소재본부)
  • Received : 2013.09.30
  • Accepted : 2013.11.21
  • Published : 2013.11.30

Abstract

Plate-shaped inorganic particles are coated onto a stainless steel substrate by the electrophoretic deposition of a precursor slurry which includes the inorganic particles of $Al_2O_3$ and polymer resin in mixed solvents to mimic the abalone shell structure, which is a composite of plate-shaped inorganic particles and organic interlayer binding materials with a layered orientation. The process parameters of the electrophoretic deposition include the voltage, coating time, and conductivity of the substrate. In addition, the suspension parameters are the particle size, concentration, viscosity, conductivity, and stability. We prepared an organic-inorganic composite coating with a high inorganic solid content by arraying the plate-shaped $Al_2O_3$ particles and electrophoretic resin via an electrophoretic deposition method. We analyzed the effect of the slurry composition and the electrophoretic deposition process parameters on the physical, mechanical and thermal properties of the coating layer, i.e., the thickness, density, particle orientation, Young's modulus and thermogravimetric analysis results.

Keywords

References

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