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Establishment of Pre-Harvest Residue Limits (PHRLs) of Fungicide Fenarimol and Insecticide Flufenoxuron in Peaches during Cultivation Period

복숭아 재배기간 중 살균제 Fenarimol과 살충제 Flufenoxuron의 생산단계 잔류허용기준 설정

  • Moon, Hye-Ree (Department of Biological Environment Chemistry, Chungnam National University) ;
  • Park, Jae-Hoon (Department of Biological Environment Chemistry, Chungnam National University) ;
  • Yoon, Ji-Yeong (Department of Biological Environment Chemistry, Chungnam National University) ;
  • Na, Eun-Shik (Korea Ginseng Corp.Safety Research Center) ;
  • Lee, Kyu-Seung (Department of Biological Environment Chemistry, Chungnam National University)
  • 문혜리 (충남대학교 생물환경화학과) ;
  • 박재훈 (충남대학교 생물환경화학과) ;
  • 윤지영 (충남대학교 생물환경화학과) ;
  • 나은식 ((주)한국인삼공사 안전성연구센터) ;
  • 이규승 (충남대학교 생물환경화학과)
  • Received : 2013.02.25
  • Accepted : 2013.05.02
  • Published : 2013.06.30

Abstract

BACKGROUND: This study was performed to establishment the PHRLs of peach during cultivation period, and also to estimate biological half-lives for residues of fenarimol and flufenoxuron. METHODS AND RESULTS: The extracted samples of fenarimol were analyzed by GC-ECD and the flufenoxuron extracted samples were analyzed by HPLC-DAD. Recoveries of fenarimol at two fortification levels of 0.1 mg/kg, 0.5 mg/kg were $93.69{\pm}6.56$(%) and $94.45{\pm}1.60$ (%), respectively. And recoveries of flufenoxuron at two fortification levels of 0.1 mg/kg, 0.5 mg/kg were $106.73{\pm}5.90$(%) and $96.37{\pm}6.66$(%), respectively. CONCLUSION(S): The biological half-lives of fenarimol in single treatment and triple treatment were 3.5day and 3.8day. that of Flufenoxuron was also 7.1day and 4.9day, respectively. The PHRL of fenarimol were recommended as 1.5 mg/kg for 10day before harvest and the PHRL of flufenoxuron were recommended as 1.4 mg/kg for 10day before harvest.

Keywords

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