DOI QR코드

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전기화학적 노이즈 저항 측정에서의 불확도 평가

Uncertainty evaluation in electrochemical noise resistance measurement

  • 김종집 (한국표준과학연구원 신기능재료 센터) ;
  • 강수연 (한국표준과학연구원 신기능재료 센터)
  • Kim, Jong Jip (Center for New Functional Materials Metrology, Korea Research Institute of Standards and Science) ;
  • Kang, Su Yeon (Center for New Functional Materials Metrology, Korea Research Institute of Standards and Science)
  • 투고 : 2013.10.14
  • 심사 : 2013.10.23
  • 발행 : 2013.10.31

초록

The uncertainty in statistical noise resistance measurement was evaluated for a type 316 stainless steel in NaCl solutions at room temperature. Sensitivity coefficients were determined for measurands or variables such as NaCl concentration, pH, solution temperature, surface roughness, inert gas flow rate and bias potential amplitude. The coefficients were larger for the variables such as NaCl concentration, pH, inert gas flow rate and solution temperature, and they were the major factors increasing the combined standard uncertainty of noise resistance. However, the contribution to the uncertainty in noise resistance measurement from the above variables was remarkably low compared to that from repeated measurements of noise resistance, and thus, it is difficult to lower the uncertainty in noise resistance measurement significantly by lowering the uncertainties related with NaCl concentration, pH, inert gas flow rate and solution temperature. In addition, the uncertainty in noise resistance measurement was high amounting to 17.3 % of the mean, indicating that the reliability in measurement of noise resistance is low.

키워드

참고문헌

  1. ISO, Guide to the Expression of Uncertainty in Measurement (1993).
  2. URAMET, Guidelines on the estimation of uncertainty in hardness Measurements, v2.0 (2011).
  3. W. Gabauer, The determination of uncertainties in tensile testing, Code of Practice, No 7, issue 1 (2000).
  4. J. J. Kim, Corros. and protect., 6, 54 (2007).
  5. J. J. Kim, Corros. Sci. Tech.. 8, 193 (2009).
  6. J. J. Kim, Met. Mat. Int., 15, 279 (2009). https://doi.org/10.1007/s12540-009-0279-1
  7. A. U. Malik, P. C. M. Kutty, N. A. Siddiqi. I. N. Anduani and S. Ahmed, Corros. Sci., 33, 1809 (1992). https://doi.org/10.1016/0010-938X(92)90011-Q