DOI QR코드

DOI QR Code

A Study of Simple α Source Preparation Using a Micro-coprecipitation Method

  • Lee, Myung Ho (Nuclear Chemistry Research Division, Korea Atomic Energy Research Institute) ;
  • Park, Tae-Hong (Nuclear Chemistry Research Division, Korea Atomic Energy Research Institute) ;
  • Song, Byung Chul (Nuclear Chemistry Research Division, Korea Atomic Energy Research Institute) ;
  • Park, Jong Ho (Nuclear Chemistry Research Division, Korea Atomic Energy Research Institute) ;
  • Song, Kyuseok (Nuclear Chemistry Research Division, Korea Atomic Energy Research Institute)
  • Received : 2012.07.29
  • Accepted : 2012.08.21
  • Published : 2012.11.20

Abstract

This study presents a rapid and simple ${\alpha}$ source preparation method for a radioactive waste sample. The recovery of $^{239}Pu$, $^{232}U$ and $^{243}Am$ using a micro-coprecipitation method was over 95%. The ${\alpha}$-peak resolution of Pu and Am isotopes through the micro-coprecipitation method is enough to discriminate the Pu and Am isotopes from other Pu and Am isotopes. The determination of the Pu and Am isotopes using the micro-coprecipitation method was applied to the radioactive waste sample, so that the activity concentrations of the Pu and Am isotopes using the micro-coprecipitation method in the radioactive waste sample were similar to those using the electrodeposition method.

Keywords

References

  1. Maxmann, S. H. Nucl. Instrum. Meth. Phys. Res. 1967, 50, 53. https://doi.org/10.1016/0029-554X(67)90593-9
  2. Aggarwal, S. K.; Chourasiya, G.; Duggal, R. K.; Singh, C. P.; Rawat, A. S.; Jain, H. C. Nucl. Instrum. Meth. Phys. Res. 1984, 223, 266. https://doi.org/10.1016/0167-5087(84)90659-8
  3. Mitchell, R. F. Anal. Chem. 1960, 32, 326. https://doi.org/10.1021/ac60159a007
  4. Handley, T. H.; Cooper, J. H. Anal. Chem. 1969, 41, 381. https://doi.org/10.1021/ac60271a036
  5. Talvitie, N. A. Anal. Chem. 1972, 44, 280. https://doi.org/10.1021/ac60310a013
  6. Puphal, K. W.; Olsen, D. R. Anal. Chem. 1972, 44, 284. https://doi.org/10.1021/ac60310a014
  7. Dutton, J. W. R.; Lovett, M. B. Nature 1977, 267, 37. https://doi.org/10.1038/267037a0
  8. Joshi, S. R. J. Radioanal. Nucl. Chem. Article 1985, 90, 409. https://doi.org/10.1007/BF02060798
  9. Hindman, F. D. Anal. Chem. 1986, 58, 1238. https://doi.org/10.1021/ac00297a059
  10. Lee, M. H.; Lee, C. W. Instrum. Meth. Phys. Res. 2000, 447, 593. https://doi.org/10.1016/S0168-9002(99)01190-0

Cited by

  1. Sample pretreatment for the determination of gamma emitting nuclides in dry radioactive waste using a dry ashing and high-performance microwave digestion system vol.301, pp.2, 2014, https://doi.org/10.1007/s10967-014-3163-5
  2. Rapid quantification of alpha emitters in low- and intermediate-level dry radioactive waste vol.307, pp.1, 2016, https://doi.org/10.1007/s10967-015-4177-3
  3. 공기 중 우라늄 동위원소 분석을 위한 방사화학 전처리방법에 대한 비교 분석 연구 vol.40, pp.2, 2012, https://doi.org/10.14407/jrp.2015.40.2.101